EP1127273A1 - Sensoranordnung zur ermittlung physikalischer eigenschaften von flüssigkeiten - Google Patents
Sensoranordnung zur ermittlung physikalischer eigenschaften von flüssigkeitenInfo
- Publication number
- EP1127273A1 EP1127273A1 EP99957946A EP99957946A EP1127273A1 EP 1127273 A1 EP1127273 A1 EP 1127273A1 EP 99957946 A EP99957946 A EP 99957946A EP 99957946 A EP99957946 A EP 99957946A EP 1127273 A1 EP1127273 A1 EP 1127273A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- sensor arrangement
- arrangement according
- substrate
- measurement
- measuring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 20
- 230000000704 physical effect Effects 0.000 title claims abstract description 7
- 239000000758 substrate Substances 0.000 claims abstract description 20
- 239000004020 conductor Substances 0.000 claims abstract description 5
- 238000010897 surface acoustic wave method Methods 0.000 claims abstract description 4
- 239000010410 layer Substances 0.000 claims description 25
- 238000005259 measurement Methods 0.000 claims description 17
- 238000001465 metallisation Methods 0.000 claims description 12
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 9
- 239000003990 capacitor Substances 0.000 claims description 5
- 230000001419 dependent effect Effects 0.000 claims description 5
- 229910052697 platinum Inorganic materials 0.000 claims description 5
- 239000012790 adhesive layer Substances 0.000 claims description 4
- 238000009529 body temperature measurement Methods 0.000 claims description 4
- 238000011156 evaluation Methods 0.000 claims description 4
- 239000010705 motor oil Substances 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 3
- 230000005284 excitation Effects 0.000 claims description 2
- 238000012883 sequential measurement Methods 0.000 claims description 2
- 230000008878 coupling Effects 0.000 description 3
- 238000010168 coupling process Methods 0.000 description 3
- 238000005859 coupling reaction Methods 0.000 description 3
- WSMQKESQZFQMFW-UHFFFAOYSA-N 5-methyl-pyrazole-3-carboxylic acid Chemical compound CC1=CC(C(O)=O)=NN1 WSMQKESQZFQMFW-UHFFFAOYSA-N 0.000 description 2
- 238000006388 chemical passivation reaction Methods 0.000 description 2
- GQYHUHYESMUTHG-UHFFFAOYSA-N lithium niobate Chemical compound [Li+].[O-][Nb](=O)=O GQYHUHYESMUTHG-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000003057 platinum Chemical class 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/02—Analysing fluids
- G01N29/036—Analysing fluids by measuring frequency or resonance of acoustic waves
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/16—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by measuring damping effect upon oscillatory body
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R27/00—Arrangements for measuring resistance, reactance, impedance, or electric characteristics derived therefrom
- G01R27/02—Measuring real or complex resistance, reactance, impedance, or other two-pole characteristics derived therefrom, e.g. time constant
- G01R27/22—Measuring resistance of fluids
Definitions
- the invention relates to a sensor arrangement for determining physical properties of liquids according to the preamble of the main claim.
- SAW Surface Acoustic Wave
- An important area here is the measurement of electrical quantities, such as the dielectric constant and / or the conductivity, the measurement of mechanical quantities, such as the density and / or the viscosity.
- the known sensor arrangement is based on a measurement principle which is described, for example, in the article "A study of love-wave acoustic sensors", J.Du, GL Harding, PROgilvy and M.Lake in the specialist journal Sen- sors and Actuators A56 (1996), pages 211 to 219.
- a sensor is implemented that works with horizontally polarized acoustic shear waves, so-called leakage waves or surface skimming bulk waves (SSBW waves) or love waves.
- SSBW waves surface skimming bulk waves
- interdigital transducers which are also known per se from the prior art mentioned above, so that the desired sensor signal can be obtained from the propagation behavior on a propagation or measurement path.
- the sensor arrangement is used to determine the quality of engine or lubricating oils in a motor vehicle or comparable machines, it is often necessary to obtain a large number of measurement variables in order to evaluate them as input variables for corresponding control units. Above all, the viscosity, the temperature, the electrical conductivity and the dielectric constant of the oil are important for a useful statement, e.g. to monitor the oil change intervals.
- the sensor arrangement mentioned at the outset for determining physical properties of liquids is advantageously further developed according to the invention with the characterizing features of the main claim.
- a compact sensor arrangement is advantageously created, with which an integration of different individual measurement sensors on a substrate plate is made possible with low-cost production.
- the electro-acoustic transducers which generate and detect the surface acoustic waves with predetermined wave modes are advantageously arranged together with further measuring arrangements.
- a corresponding measured value is determined from the propagation behavior of the acoustic waves along a propagation path in the manner known per se.
- the basic sensor element is, for example, a substrate made of certain quartz, lithium tantalate and lithium niobate sections which are particularly suitable for the acoustic shear modes described at the beginning.
- a temperature-dependent resistor is advantageously attached adjacent to the substrate as a measuring arrangement for temperature measurement.
- the conductor track structure on the substrate is produced from a metallization layer, advantageously from platinum, whereby both the temperature-dependent resistance and the transmission and reception conductor track structures of the electro-acoustic transducer can be produced from this platinum layer, so that only a single metallization layer on the substrate is necessary is. Platinum is extremely chemically resistant, so that cover layers can be dispensed with under certain circumstances.
- a dielectric layer applied above the metallization layer on the substrate can, however, also be arranged as an acoustic waveguide layer for the electro-acoustic transducers in addition to the chemical passivation. It is also possible to use titanium or silicon or other intermediate layers as an adhesive layer between the substrate and the electro-acoustic wall learners as well as between the electro-acoustic transducers and other layers above.
- an arrangement for electrical conductivity measurement can advantageously also be produced from the metallization layer by means of uncovered electrodes.
- the conductivity measurement is carried out in a simple manner with a direct current or an alternating current which flows through the liquid.
- an arrangement for measuring the dielectric constant can advantageously be created from the same metallization layer by means of a capacitor structure.
- the capacitor structure can be in the form of an interdigital capacitor and, if appropriate, can be covered by an additional insulating layer; However, it is also possible to use it uncovered for better coupling to the liquid to be measured, wherein the chemical resistance of the metallization layer can be exploited.
- all measuring arrangements for determining the individual physical quantities can be contacted individually in a simple manner, and thus all four measuring methods can be carried out on a corresponding evaluation electronics for sequential measurement with a single substrate, which can be used particularly for construction forms which are favorable for production. Furthermore, the good heat coupling on the substrate is also advantageous, since the temperature of the various measuring sensors is available with particularly small deviations during signal evaluation, so that very precise compensation methods can be used.
- the schematic view according to the single figure shows the main component of the proposed sensor arrangement, namely a substrate plate 1 polished on one side from a piezoelectric material, in which horizontally polarized acoustic shear modes can be excited by an interdigital transducer 3 that can be contacted via electrical connections 2 and in an interdigital transducer 4 as an electro -acoustic transducers are detectable.
- the measuring arrangement described above with the electro-acoustic transducers for measuring the viscosity of a measuring liquid via the propagation of a surface wave and the measuring arrangements described below are structured from a metallization layer, preferably from platinum, and optionally adhesive layers.
- a dielectric layer (not shown here) can also be arranged above the electro-acoustic transducers 3 and 4 as an acoustic waveguide layer, which also enables chemical passivation.
- electrodes 5 for conductivity measurement are present on the substrate 1 and are supplied with a direct or alternating current.
- conductivity measurement could also be dispensed with in many application stalls.
- the temperature measurement is carried out here via a resistance meander 6, which is likewise structured from the metallization layer.
- the arrangement of the resistance meander 6 can also lie outside the propagation distance between the transducers 3 and 4, in a modification of the shape shown.
- a capacitor structure 7 which, for better coupling to the liquid to be measured, is either uncovered or provided with a cover layer 8 shown here in broken lines in order to improve the chemical resistance.
- the measurement of the dielectric constant and the conductivity can possibly also be carried out with the electro-acoustic transducers for determining the viscosity of the liquid a different excitation frequency than the frequency required to generate the surface wave is selected.
- the measuring liquid e.g.
- the engine oil of a motor vehicle flows past the substrate surface and possibly the cover layer to determine the physical properties, and the measurement signals obtained are taken at the contact points and an evaluation device (not shown here) for generating the necessary control and / or display signals, e.g. for the quality of the engine oil.
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Acoustics & Sound (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19850799 | 1998-11-04 | ||
| DE19850799A DE19850799A1 (de) | 1998-11-04 | 1998-11-04 | Sensoranordnung zur Ermittlung physikalischer Eigenschaften von Flüssigkeiten |
| PCT/DE1999/003458 WO2000026661A1 (de) | 1998-11-04 | 1999-10-28 | Sensoranordnung zur ermittlung physikalischer eigenschaften von flüssigkeiten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP1127273A1 true EP1127273A1 (de) | 2001-08-29 |
Family
ID=7886644
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP99957946A Withdrawn EP1127273A1 (de) | 1998-11-04 | 1999-10-28 | Sensoranordnung zur ermittlung physikalischer eigenschaften von flüssigkeiten |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP1127273A1 (de) |
| JP (1) | JP2003502617A (de) |
| KR (1) | KR20010090813A (de) |
| AU (1) | AU749057B2 (de) |
| DE (1) | DE19850799A1 (de) |
| WO (1) | WO2000026661A1 (de) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10152777A1 (de) * | 2001-10-29 | 2003-05-15 | Hydac Electronic Gmbh | Vorrichtung und Verfahren zur Bestimmung der Qualität eines Mediums, insbesondere eines Schmier- und/oder Kühlmittels |
| CN100335878C (zh) * | 2002-06-08 | 2007-09-05 | Lg伊诺特有限公司 | 使用狭缝声波的saw传感器装置及其方法 |
| DE102004049580A1 (de) * | 2004-10-12 | 2006-04-13 | Robert Bosch Gmbh | Verfahren zur Erfassung von Zustandsparametern einer Flüssigkeit |
| DE102006015111A1 (de) * | 2006-03-31 | 2007-10-04 | Schaeffler Kg | Dreh-, Schwenk- oder Axiallager mit einem Schmierfett-Sensor |
| DE102009055738A1 (de) * | 2009-11-26 | 2011-06-09 | Continental Automotive Gmbh | Verfahren zur Bestimmung des Zustandes eines Reduktionsmittels in einem Reduktionsmitteltank |
| JP5779191B2 (ja) * | 2009-12-21 | 2015-09-16 | ヴェマ・システム・アーエスWema System As | 品質センサ機器 |
| GB2476317B (en) * | 2009-12-21 | 2014-02-12 | Wema System As | Quality sensor apparatus |
| FR2962224B1 (fr) | 2010-07-02 | 2013-05-10 | Sartorius Stedim Biotech Sa | Dispositif capteur d'un parametre lie a un phenomene electrique d'un contenu biopharmaceutique et conteneur biopharmaceutique comportant un tel dispositif capteur. |
| DE102013009370A1 (de) | 2013-06-05 | 2014-12-11 | Hochschule Karlsruhe | Vorrichtung zur Messung von Fluideigenschaften und deren Verwendung |
| EP3156620B1 (de) | 2015-10-13 | 2018-09-12 | Plastic Omnium Advanced Innovation and Research | Verfahren zur bestimmung der konzentration eines chemischen mittels in einer lösung basierend auf der geschwindigkeit einer druckwelle und system dafür |
| DE102015016887A1 (de) * | 2015-12-22 | 2017-06-22 | Dürr Somac GmbH | Vorrichtung zur Messung des Wassergehaltes in Bremsflüssigkeiten |
| EP3513154B1 (de) | 2016-09-13 | 2021-03-17 | Passerro GmbH | Verfahren und vorrichtung zur bestimmung und/oder überwachung der durchschlagspannung eines transformatorenöls |
| NO343381B1 (en) | 2017-10-05 | 2019-02-18 | Sentec As | Level sensor assembly |
| DE102018210387B4 (de) * | 2018-06-26 | 2023-03-23 | Robert Bosch Gmbh | Sensorvorrichtung und Verfahren zum Detektieren von Gasen |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19706486A1 (de) * | 1997-02-19 | 1998-08-20 | Fraunhofer Ges Forschung | Vorrichtung und Verfahren zum Bestimmen des Alterungszustands flüssiger Medien |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5130257A (en) * | 1988-09-29 | 1992-07-14 | Hewlett-Packard Company | Chemical sensor utilizing a surface transverse wave device |
| US5741961A (en) * | 1993-08-18 | 1998-04-21 | Sandia Corporation | Quartz resonator fluid density and viscosity monitor |
| DE19710358C2 (de) * | 1997-03-13 | 2000-11-30 | Bosch Gmbh Robert | Mikrostrukturierter Sensor |
-
1998
- 1998-11-04 DE DE19850799A patent/DE19850799A1/de not_active Withdrawn
-
1999
- 1999-10-28 KR KR1020017005559A patent/KR20010090813A/ko not_active Withdrawn
- 1999-10-28 JP JP2000579991A patent/JP2003502617A/ja active Pending
- 1999-10-28 WO PCT/DE1999/003458 patent/WO2000026661A1/de not_active Ceased
- 1999-10-28 AU AU15490/00A patent/AU749057B2/en not_active Ceased
- 1999-10-28 EP EP99957946A patent/EP1127273A1/de not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19706486A1 (de) * | 1997-02-19 | 1998-08-20 | Fraunhofer Ges Forschung | Vorrichtung und Verfahren zum Bestimmen des Alterungszustands flüssiger Medien |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2003502617A (ja) | 2003-01-21 |
| WO2000026661A1 (de) | 2000-05-11 |
| KR20010090813A (ko) | 2001-10-19 |
| AU1549000A (en) | 2000-05-22 |
| AU749057B2 (en) | 2002-06-20 |
| DE19850799A1 (de) | 2000-05-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
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| 17P | Request for examination filed |
Effective date: 20010605 |
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| AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AT BE CH CY DE DK ES FI FR GB GR IE IT LI LU MC NL PT SE Kind code of ref document: A1 Designated state(s): CH DE FR GB LI |
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| 17Q | First examination report despatched |
Effective date: 20020507 |
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| RTI1 | Title (correction) |
Free format text: SENSOR ARRANGEMENT FOR DETERMINING PHYSICAL PROPERTIES OF A LIQUID |
|
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
| 18D | Application deemed to be withdrawn |
Effective date: 20020918 |
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| RBV | Designated contracting states (corrected) |
Designated state(s): CH DE FR GB LI |