EP1213372A3 - Verfahren und Anordnung zur galvanischen Abscheidung von Nickel, Kobalt, Nickellegierungen oder Kobaltlegierungen mit periodischen Strompulsen und Verwendung des Verfahrens - Google Patents

Verfahren und Anordnung zur galvanischen Abscheidung von Nickel, Kobalt, Nickellegierungen oder Kobaltlegierungen mit periodischen Strompulsen und Verwendung des Verfahrens Download PDF

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Publication number
EP1213372A3
EP1213372A3 EP01128897A EP01128897A EP1213372A3 EP 1213372 A3 EP1213372 A3 EP 1213372A3 EP 01128897 A EP01128897 A EP 01128897A EP 01128897 A EP01128897 A EP 01128897A EP 1213372 A3 EP1213372 A3 EP 1213372A3
Authority
EP
European Patent Office
Prior art keywords
cobalt
nickel
alloys
anode
cathode
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP01128897A
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English (en)
French (fr)
Other versions
EP1213372B1 (de
EP1213372A2 (de
Inventor
Rüdiger Ewald
Peter Filke
Michael Heckmann
Wolfgang Keinath
Günter Langel
Anton Schmidt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Airbus DS GmbH
Original Assignee
Astrium GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Astrium GmbH filed Critical Astrium GmbH
Publication of EP1213372A2 publication Critical patent/EP1213372A2/de
Publication of EP1213372A3 publication Critical patent/EP1213372A3/de
Application granted granted Critical
Publication of EP1213372B1 publication Critical patent/EP1213372B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D17/00Constructional parts, or assemblies thereof, of cells for electrolytic coating
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D17/00Constructional parts, or assemblies thereof, of cells for electrolytic coating
    • C25D17/008Current shielding devices
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D17/00Constructional parts, or assemblies thereof, of cells for electrolytic coating
    • C25D17/10Electrodes, e.g. composition, counter electrode
    • C25D17/12Shape or form
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00Electroplating: Baths therefor
    • C25D3/02Electroplating: Baths therefor from solutions
    • C25D3/12Electroplating: Baths therefor from solutions of nickel or cobalt
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D3/00Electroplating: Baths therefor
    • C25D3/02Electroplating: Baths therefor from solutions
    • C25D3/56Electroplating: Baths therefor from solutions of alloys
    • C25D3/562Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of iron or nickel or cobalt
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/18Electroplating using modulated, pulsed or reversing current

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Electrical Discharge Machining, Electrochemical Machining, And Combined Machining (AREA)
  • Electroplating And Plating Baths Therefor (AREA)

Abstract

Beschrieben wird ein Verfahren zur galvanischen Abscheidung von Nickel, Kobalt, Nickellegierungen oder Kobaltlegierungen in einem galvanischen Bad (1) unter Verwendung eines Nickelverbindungen oder Kobaltverbindungen enthaltenden Elektrolyten, wobei zur Abscheidung mindestens eine Anode (3,3a,3b) und mindestens eine Kathode des Bades (1) mit periodischen Strompulsen (Pulse Plating) beaufschlagt wird. Das Verhältnis IA/IC aus Anodenstromdichte IA zu Kathodenstromdichte IC wird dazu größer als 1 und kleiner als 1,5 gewählt, und das Ladungsverhältnis QA/QC=(TA·IA)/(TC·IC) der während eines Anodenpulses der Dauer TA transportierten Ladung QA zu der während eines Kathodenpulses der Dauer TC transportierten Ladung QC beträgt zwischen 30 und 45. Ein Bad zur Durchführung des Verfahrens weist insbesondere konturierte Anoden (3,3a,3b), Stromblenden (5), eine Reinigungseinrichtung (6) für den Elektrolyten und eine Umwälzeinrichtung (13) mit einer Rückführung des Elektrolyten durch Düsen (7) auf.
EP01128897A 2000-12-07 2001-12-05 Verfahren und Anordnung zur galvanischen Abscheidung von Nickel, Kobalt, Nickellegierungen oder Kobaltlegierungen mit periodischen Strompulsen und Verwendung des Verfahrens Expired - Lifetime EP1213372B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10061186 2000-12-07
DE10061186A DE10061186C1 (de) 2000-12-07 2000-12-07 Verfahren und Anordnung zur galvanischen Abscheidung von Nickel, Kobalt, Nickellegierungen oder Kobaltlegierungen mit periodischen Strompulsen und Verwendung des Verfahrens

Publications (3)

Publication Number Publication Date
EP1213372A2 EP1213372A2 (de) 2002-06-12
EP1213372A3 true EP1213372A3 (de) 2004-02-04
EP1213372B1 EP1213372B1 (de) 2011-02-09

Family

ID=7666361

Family Applications (1)

Application Number Title Priority Date Filing Date
EP01128897A Expired - Lifetime EP1213372B1 (de) 2000-12-07 2001-12-05 Verfahren und Anordnung zur galvanischen Abscheidung von Nickel, Kobalt, Nickellegierungen oder Kobaltlegierungen mit periodischen Strompulsen und Verwendung des Verfahrens

Country Status (6)

Country Link
US (1) US6790332B2 (de)
EP (1) EP1213372B1 (de)
JP (1) JP4285932B2 (de)
AT (1) ATE498026T1 (de)
DE (2) DE10061186C1 (de)
RU (1) RU2281990C2 (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10237381B4 (de) * 2002-08-12 2005-06-23 Eads Space Transportation Gmbh Brennkammerstruktur und Verfahren zu deren Herstellung
US7306710B2 (en) * 2002-11-08 2007-12-11 Pratt & Whitney Rocketdyne, Inc. Apparatus and method for electroplating a metallic film on a rocket engine combustion chamber component
DE10259362A1 (de) * 2002-12-18 2004-07-08 Siemens Ag Verfahren zum Abscheiden einer Legierung auf ein Substrat
US20060037865A1 (en) * 2004-08-19 2006-02-23 Rucker Michael H Methods and apparatus for fabricating gas turbine engines
GB0811016D0 (en) * 2008-06-17 2008-07-23 Smart Stabilizer Systems Ltd Steering component and steering assembly
FR2935147B1 (fr) * 2008-08-25 2010-09-17 Snecma Dispositif et procede pour l'application d'un revetement sur une piece par electro deposition.
US8425751B1 (en) 2011-02-03 2013-04-23 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Systems and methods for the electrodeposition of a nickel-cobalt alloy
DE102013010025A1 (de) * 2013-06-17 2014-12-18 Muhr Und Bender Kg Verfahren zum Herstellen eines Erzeugnisses aus flexibel gewalztem Bandmaterial
CN103526246A (zh) * 2013-09-26 2014-01-22 沈阳化工大学 一种发动机转子表面复合Al-Ni镀层的方法
CN103556192B (zh) * 2013-10-09 2016-03-30 北京航空航天大学 一种采用双向脉冲电源制备具有高力学性能电铸镍层的方法
GB2528873A (en) * 2014-07-31 2016-02-10 Mohammad Sakhawat Hussain Direct high speed nickel plating on difficult to plate metals
RU2617470C1 (ru) * 2015-12-28 2017-04-25 Федеральное государственное бюджетное образовательное учреждение высшего образования "Российский химико-технологический университе имени Д. И. Менделеева (РХТУ им. Д. И. Менделеева) Способ электроосаждения покрытий никель-фосфор
CN105862093B (zh) * 2016-05-26 2018-03-06 安庆师范大学 一种离子液体中电镀Ni‑Cr‑PTFE复合镀层的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2470775A (en) * 1947-07-09 1949-05-24 Westinghouse Electric Corp Electroplating nickel and cobalt with periodic reverse current
US3915835A (en) * 1973-11-05 1975-10-28 Ford Motor Co Method of improving plating distribution of elnisil coatings
DE2558423A1 (de) * 1975-12-23 1977-06-30 Messerschmitt Boelkow Blohm Verfahren zum galvanischen abscheiden von nickel aus einem nickelsulfamatbad
EP0835335A1 (de) * 1995-06-21 1998-04-15 Peter Torben Tang Elektroplattierungsverfahren zur herstellung von beschichtungen aus nickel, kobalt, nickel- oder kobaltlegierungen

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3726768A (en) * 1971-04-23 1973-04-10 Atomic Energy Commission Nickel plating baths containing aromatic sulfonic acids
SU1110825A1 (ru) * 1983-03-15 1984-08-30 Днепропетровский Ордена Трудового Красного Знамени Институт Инженеров Железнодорожного Транспорта Им.М.И.Калинина Способ нанесени никелевых покрытий
DE19545231A1 (de) * 1995-11-21 1997-05-22 Atotech Deutschland Gmbh Verfahren zur elektrolytischen Abscheidung von Metallschichten
RU2089675C1 (ru) * 1996-10-24 1997-09-10 Шевелкин Валерий Иванович Способ никелирования деталей из стали, меди и медных сплавов
US6071398A (en) * 1997-10-06 2000-06-06 Learonal, Inc. Programmed pulse electroplating process
US6210555B1 (en) * 1999-01-29 2001-04-03 Faraday Technology Marketing Group, Llc Electrodeposition of metals in small recesses for manufacture of high density interconnects using reverse pulse plating

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2470775A (en) * 1947-07-09 1949-05-24 Westinghouse Electric Corp Electroplating nickel and cobalt with periodic reverse current
US3915835A (en) * 1973-11-05 1975-10-28 Ford Motor Co Method of improving plating distribution of elnisil coatings
DE2558423A1 (de) * 1975-12-23 1977-06-30 Messerschmitt Boelkow Blohm Verfahren zum galvanischen abscheiden von nickel aus einem nickelsulfamatbad
EP0835335A1 (de) * 1995-06-21 1998-04-15 Peter Torben Tang Elektroplattierungsverfahren zur herstellung von beschichtungen aus nickel, kobalt, nickel- oder kobaltlegierungen

Also Published As

Publication number Publication date
RU2281990C2 (ru) 2006-08-20
DE10061186C1 (de) 2002-01-17
EP1213372B1 (de) 2011-02-09
JP2002226991A (ja) 2002-08-14
DE50115791D1 (de) 2011-03-24
US6790332B2 (en) 2004-09-14
ATE498026T1 (de) 2011-02-15
US20020084190A1 (en) 2002-07-04
JP4285932B2 (ja) 2009-06-24
EP1213372A2 (de) 2002-06-12

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