EP1284322A1 - Sicherheitsmarkierungsmittel - Google Patents
Sicherheitsmarkierungsmittel Download PDFInfo
- Publication number
- EP1284322A1 EP1284322A1 EP02291986A EP02291986A EP1284322A1 EP 1284322 A1 EP1284322 A1 EP 1284322A1 EP 02291986 A EP02291986 A EP 02291986A EP 02291986 A EP02291986 A EP 02291986A EP 1284322 A1 EP1284322 A1 EP 1284322A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- luminescence
- components
- doped
- conversion
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 30
- 238000004020 luminiscence type Methods 0.000 claims abstract description 28
- 238000006243 chemical reaction Methods 0.000 claims abstract description 23
- 239000011159 matrix material Substances 0.000 claims abstract description 5
- AGVJBLHVMNHENQ-UHFFFAOYSA-N Calcium sulfide Chemical compound [S-2].[Ca+2] AGVJBLHVMNHENQ-UHFFFAOYSA-N 0.000 claims description 9
- 239000005083 Zinc sulfide Substances 0.000 claims description 8
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 8
- 229910052693 Europium Inorganic materials 0.000 claims description 7
- OGPBJKLSAFTDLK-UHFFFAOYSA-N europium atom Chemical compound [Eu] OGPBJKLSAFTDLK-UHFFFAOYSA-N 0.000 claims description 7
- QWVYNEUUYROOSZ-UHFFFAOYSA-N trioxido(oxo)vanadium;yttrium(3+) Chemical compound [Y+3].[O-][V]([O-])([O-])=O QWVYNEUUYROOSZ-UHFFFAOYSA-N 0.000 claims description 6
- 230000000630 rising effect Effects 0.000 claims description 4
- 229910052779 Neodymium Inorganic materials 0.000 claims description 2
- 239000002019 doping agent Substances 0.000 claims description 2
- QEFYFXOXNSNQGX-UHFFFAOYSA-N neodymium atom Chemical compound [Nd] QEFYFXOXNSNQGX-UHFFFAOYSA-N 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 230000005284 excitation Effects 0.000 description 7
- 230000005855 radiation Effects 0.000 description 6
- 229910052772 Samarium Inorganic materials 0.000 description 5
- KZUNJOHGWZRPMI-UHFFFAOYSA-N samarium atom Chemical compound [Sm] KZUNJOHGWZRPMI-UHFFFAOYSA-N 0.000 description 5
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 3
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000005098 photoluminescent agent Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- GFKJCVBFQRKZCJ-UHFFFAOYSA-N oxygen(2-);yttrium(3+);trisulfide Chemical compound [O-2].[O-2].[O-2].[S-2].[S-2].[S-2].[Y+3].[Y+3].[Y+3].[Y+3] GFKJCVBFQRKZCJ-UHFFFAOYSA-N 0.000 description 1
- 238000005424 photoluminescence Methods 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- -1 rare earth oxysulfides Chemical class 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052984 zinc sulfide Inorganic materials 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/40—Agents facilitating proof of genuineness or preventing fraudulent alteration, e.g. for security paper
- D21H21/44—Latent security elements, i.e. detectable or becoming apparent only by use of special verification or tampering devices or methods
- D21H21/48—Elements suited for physical verification, e.g. by irradiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M3/00—Printing processes to produce particular kinds of printed work, e.g. patterns
- B41M3/14—Security printing
- B41M3/144—Security printing using fluorescent, luminescent or iridescent effects
Definitions
- the present invention relates to a composition of safety marking with light cascade.
- the security marking compositions comprising photoluminescent elements have been used since many years to minimize the risk of reproduction by fraudsters of legal documents or economic documents, especially banknotes.
- a security marking composition comprising a organic matrix in which are incorporated at least a fluorescent component and at least one phosphorescent component forming between them a luminous cascade, that is, one of the components has a range of lengths of excitation waves that corresponds at least partially with the luminescence wavelength range of the other component.
- a security marking composition presents the advantage of realizing a true encoding of the light, the fraudster being unable to when submitting the document containing the composition to a determined wavelength, to establish a direct relationship between the observed final luminescence and the wavelength of the initial radiation.
- the composition described in this document therefore has a significant advantage compared to previous compositions.
- composition of security marking comprising an organic matrix in which at least two components are incorporated photoluminescents forming a luminous cascade, one at less components having a luminescence according to a upward conversion.
- Luminescence according to a conversion ascending (anti-Stokes effect or "Up-Conversion"), a luminescence in a range of lower wavelengths at the excitation wavelength of the component concerned, as opposed to luminescence according to a downward conversion (Stokes effect) for which the luminescence is produced in a range of lengths waves greater than the excitation wavelength as is usually the case for most components photoluminescents, in particular the components described in EP 265 323. It is thus multiplied the number of combinations made by the cascade and therefore increases the difficulty of determining the components entering the composition.
- the composition further comprises a luminous cascade of which the components all have a luminescence according to a conversion down.
- At least one of the components has luminescence according to upward and downward conversions.
- the security marking composition according to the invention comprises an organic matrix formed by example by a binder of acrylic resin, and a mixture photoluminescence representing about 20% by weight of the composition, the photoluminescent mixture comprising a part of zinc sulphide doped with silver, a part of sulphide of zinc doped with copper, a part of calcium sulphide doped with europium and samarium, and a part of vanadate of yttrium doped with neodymium.
- zinc sulphide doped with silver is a fluorescent component, that is, its luminescence ceases immediately after the cessation of the excitation, and has luminescence in a downward conversion, that is to say, it is excited by radiation in a range of wavelengths from around 200 nm at about 370 nm, and then emits a luminescence in a first range of wavelengths between about 400 nm and 500 nm.
- Yttrium vanadate is also a fluorescent component. He is excited by a radiation in a range of wavelengths ranging from about 250 nm to about 370 nm, and then emit luminescence in a range of wavelengths included between about 800 nm and 900 nm.
- Zinc sulphide doped with silver forms with calcium sulphide doped with europium and at the samarium, a first luminous cascade in which calcium sulphide emits luminescence according to a downward conversion by an excitation in a range of wavelengths between approximately 450 nm and 580 nm and emission in a range of lengths between about 600 nm and 700 nm, and the Yttrium vanadate forms with calcium sulphide a second luminous cascade in which the sulfide of calcium emits luminescence according to a rising conversion by excitation in the wavelength range covering the luminescence range of yttrium vanadate (800 to 900 nm), and a luminescent emission in the range of wavelengths between 600 nm and 700 nm.
- Copper-doped zinc sulphide is a component phosphorescent, that is, whose luminescent emission continues beyond the cessation of excitement, and emits luminescence according to a downconversion, the excitation being caused by radiation at a wavelength of the order of 370 nm and the emission luminescent being produced mainly for a length wave of the order of 500 nm.
- Zinc sulphide doped copper thus also forms a luminous cascade with calcium sulphide doped with europium and samarium but the two components of this luminous cascade then have a luminescence in a downward conversion.
- the composition according to the invention has a pink color when set under ultraviolet radiation it has a color white and when kept in the dark after cessation of ultraviolet radiation it presents a pale green color.
- the invention can be realized with a single luminous cascade of which one of the components has a luminescence according to a conversion descendant and the other a luminescence according to a upstream conversion, for example using only Yttrium vanadate, which has a luminescence according to a descending conversion and calcium sulphide which is then excited only in its upward conversion.
- a cascade with a first excited component in the ultraviolet and emitting in the infrared (the yttrium vanadate), and a second component excited in infrared and emitting in the visible range (sulphide calcium).
- composition according to the invention may also be carried out with rare earth oxysulfides which have a luminescence according to a downward or upward conversion depending on the dopant used.
- rare earth oxysulfides which have a luminescence according to a downward or upward conversion depending on the dopant used.
- Europium doped yttrium oxysulfide can be used which has a luminescence according to a rising conversion.
- composition includes both fluorescent and phosphorescent components, this can also be done with components exclusively fluorescent, for example a composition not containing copper-doped zinc sulfide.
- calcium sulphide can also be be doped exclusively with europium or samarium.
Landscapes
- Luminescent Compositions (AREA)
- Illuminated Signs And Luminous Advertising (AREA)
- Road Signs Or Road Markings (AREA)
- Paints Or Removers (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Dental Preparations (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0110806A FR2828698B1 (fr) | 2001-08-14 | 2001-08-14 | Composition de marquage de securite a cascade lumineuse |
| FR0110806 | 2001-08-14 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP1284322A1 true EP1284322A1 (de) | 2003-02-19 |
| EP1284322B1 EP1284322B1 (de) | 2006-04-05 |
Family
ID=8866524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP02291986A Expired - Lifetime EP1284322B1 (de) | 2001-08-14 | 2002-08-07 | Sicherheitsmarkierungsmittel |
Country Status (11)
| Country | Link |
|---|---|
| EP (1) | EP1284322B1 (de) |
| AT (1) | ATE322576T1 (de) |
| DE (1) | DE60210378T2 (de) |
| DK (1) | DK1284322T3 (de) |
| ES (1) | ES2257519T3 (de) |
| FR (1) | FR2828698B1 (de) |
| MA (1) | MA25711A1 (de) |
| MD (1) | MD2403C2 (de) |
| OA (1) | OA12478A (de) |
| PT (1) | PT1284322E (de) |
| TN (1) | TNSN02074A1 (de) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006099642A1 (de) * | 2005-03-21 | 2006-09-28 | Oesterreichische Banknoten- Und Sicherheitsdruck Gmbh | Sicherheitselement |
| EP1760134A1 (de) * | 2005-08-30 | 2007-03-07 | Viktor Ivanovich Petrik | Weiss-fluoreszierende Anti-Stokes-Zusammensetzungen und Methode zur Identifizierung und zum Schutz von Steuermarken, Banknoten, Wertpapieren, Dokumenten und Produkten |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010028818A1 (de) | 2010-05-10 | 2011-11-10 | Swiss Authentication Research And Development Ag | Kombination von Lumineszenzstoffen |
| EP3342601B1 (de) | 2017-01-02 | 2019-03-27 | Polska Wytwornia Papierow Wartosciowych S.A. | Sicherheitsdokument |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0265323A1 (de) * | 1986-10-10 | 1988-04-27 | Banque De France | Treuhänderischer Sicherheitsgegenstand, der eine visuelle oder optische Echtheitsprüfung erlaubt |
| US4897300A (en) * | 1987-08-19 | 1990-01-30 | Gao Gesellschaft Fuer Automation Und Organisation Mbh | Security paper |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE461359B (sv) * | 1987-06-30 | 1990-02-05 | Global Security Ab | Saett och anordning foer osynlig maerkning av sedlar eller vaerdehandlingar |
| DE3915638B4 (de) * | 1989-05-12 | 2006-06-08 | Giesecke & Devrient Gmbh | Sicherheitsdokument mit darin eingebettetem Sicherheitselement mit visuell und maschinell prüfbaren Kennzeichen und Sicherheitselement für ein Sicherheitsdokument |
| DE4114732A1 (de) * | 1991-05-06 | 1992-11-12 | Helmut Dr Bayer | Sicherheitskennzeichnung fuer papiere und andere materialien mit ebenen oberflaechen |
| US5639126A (en) * | 1995-06-06 | 1997-06-17 | Crane & Co., Inc. | Machine readable and visually verifiable security threads and security papers employing same |
| DE19735293C2 (de) * | 1997-08-14 | 2003-06-12 | Bundesdruckerei Gmbh | Wert- und Sicherheitserzeugnis mit Lumineszenzelement |
| RU2150749C1 (ru) * | 1999-02-09 | 2000-06-10 | Петрик Виктор Иванович | Средство защиты от подделки ценных бумаг и документов (варианты) |
| FR2813134B1 (fr) * | 2000-08-21 | 2004-01-16 | Banque De France | Procede d'authentification de documents sensibles |
| DE10056462A1 (de) * | 2000-11-14 | 2002-05-23 | Giesecke & Devrient Gmbh | Fluoreszenzstoff und Verfahren zu dessen Herstellung |
| DE20116951U1 (de) * | 2001-10-09 | 2001-12-13 | Khulusi, Gelan, 41542 Dormagen | Dispensierelement zur Überprüfung von Banknoten |
-
2001
- 2001-08-14 FR FR0110806A patent/FR2828698B1/fr not_active Expired - Fee Related
-
2002
- 2002-08-07 AT AT02291986T patent/ATE322576T1/de active
- 2002-08-07 DE DE60210378T patent/DE60210378T2/de not_active Expired - Lifetime
- 2002-08-07 MD MDA20020201A patent/MD2403C2/ro not_active IP Right Cessation
- 2002-08-07 EP EP02291986A patent/EP1284322B1/de not_active Expired - Lifetime
- 2002-08-07 ES ES02291986T patent/ES2257519T3/es not_active Expired - Lifetime
- 2002-08-07 DK DK02291986T patent/DK1284322T3/da active
- 2002-08-07 PT PT02291986T patent/PT1284322E/pt unknown
- 2002-08-09 MA MA26768A patent/MA25711A1/fr unknown
- 2002-08-12 TN TNTNSN02074A patent/TNSN02074A1/fr unknown
- 2002-08-14 OA OA1200200246A patent/OA12478A/fr unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0265323A1 (de) * | 1986-10-10 | 1988-04-27 | Banque De France | Treuhänderischer Sicherheitsgegenstand, der eine visuelle oder optische Echtheitsprüfung erlaubt |
| US4897300A (en) * | 1987-08-19 | 1990-01-30 | Gao Gesellschaft Fuer Automation Und Organisation Mbh | Security paper |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006099642A1 (de) * | 2005-03-21 | 2006-09-28 | Oesterreichische Banknoten- Und Sicherheitsdruck Gmbh | Sicherheitselement |
| US7656511B2 (en) | 2005-03-21 | 2010-02-02 | Oesterreichische Banknoten-Und Sicherheitsdruck Gmbh | Security element |
| AU2006227581B2 (en) * | 2005-03-21 | 2011-07-07 | Oesterreichische Banknoten- Und Sicherheitsdruck Gmbh | Security element |
| EP1760134A1 (de) * | 2005-08-30 | 2007-03-07 | Viktor Ivanovich Petrik | Weiss-fluoreszierende Anti-Stokes-Zusammensetzungen und Methode zur Identifizierung und zum Schutz von Steuermarken, Banknoten, Wertpapieren, Dokumenten und Produkten |
Also Published As
| Publication number | Publication date |
|---|---|
| DE60210378T2 (de) | 2006-10-19 |
| ES2257519T3 (es) | 2006-08-01 |
| FR2828698A1 (fr) | 2003-02-21 |
| ATE322576T1 (de) | 2006-04-15 |
| TNSN02074A1 (fr) | 2004-03-05 |
| MD2403C2 (ro) | 2004-09-30 |
| DE60210378D1 (de) | 2006-05-18 |
| EP1284322B1 (de) | 2006-04-05 |
| DK1284322T3 (da) | 2006-05-29 |
| PT1284322E (pt) | 2006-05-31 |
| MA25711A1 (fr) | 2003-04-01 |
| OA12478A (fr) | 2006-05-24 |
| FR2828698B1 (fr) | 2003-11-21 |
| MD2403B1 (en) | 2004-03-31 |
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