EP1897524B1 - Méthode et appareil pour la dynamisation de liquides - Google Patents

Méthode et appareil pour la dynamisation de liquides Download PDF

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Publication number
EP1897524B1
EP1897524B1 EP06018516A EP06018516A EP1897524B1 EP 1897524 B1 EP1897524 B1 EP 1897524B1 EP 06018516 A EP06018516 A EP 06018516A EP 06018516 A EP06018516 A EP 06018516A EP 1897524 B1 EP1897524 B1 EP 1897524B1
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EP
European Patent Office
Prior art keywords
vessel
potentisation
mixture
drain
injection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP06018516A
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German (de)
English (en)
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EP1897524A1 (fr
Inventor
Jacqueline Ryffel-Hausch
Denise Bürki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Spagyros AG
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Spagyros AG
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Publication date
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Priority to EP06018516A priority Critical patent/EP1897524B1/fr
Priority to AT06018516T priority patent/ATE550009T1/de
Publication of EP1897524A1 publication Critical patent/EP1897524A1/fr
Application granted granted Critical
Publication of EP1897524B1 publication Critical patent/EP1897524B1/fr
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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
    • A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/405—Methods of mixing liquids with liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/48—Mixing liquids with liquids; Emulsifying characterised by the nature of the liquids
    • B01F23/483—Mixing liquids with liquids; Emulsifying characterised by the nature of the liquids using water for diluting a liquid ingredient, obtaining a predetermined concentration or making an aqueous solution of a concentrate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75—Discharge mechanisms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75—Discharge mechanisms
    • B01F35/754—Discharge mechanisms characterised by the means for discharging the components from the mixer
    • B01F35/75465—Discharge mechanisms characterised by the means for discharging the components from the mixer using suction, vacuum, e.g. with a pipette
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/80—Forming a predetermined ratio of the substances to be mixed
    • B01F35/81—Forming mixtures with changing ratios or gradients

Definitions

  • the invention relates to a method for potentiating liquids according to claim 1, in which a first volume of a liquid to be diluted is added to a pot still, a second volume of a diluent liquid is injected into the pot and then a portion of the mixture formed is removed from the Potenziergefäss such that a first volume of the mixture remains in the pot, the pot still being kept immobile throughout the process.
  • Potentiation in the present context means a method for the production of medicaments in homeopathy.
  • This homeopathic basic substances are diluted gradually.
  • the dilution is usually carried out in a ratio of 1:10 (D-potency), 1: 100 (C-potency) or 1: 50,000 (Q / LM-potency) per exponentiation step.
  • the production by hand shaking according to the multi-glass method according to Hahnemann requires a time of 2 days with a C 200; Accordingly, of 10 days at a C 1000. Therefore, long ago machines were proposed, which do this work automatically.
  • the operating principle is as follows. In a container in which there is a certain residual amount of the liquid of preceding potency, a swirl is generated by the rapid injection of 99 times this residual amount of diluent liquid (water), which ensures sufficient mixing. The container is now emptied by tilting so far that again only the certain residual amount of liquid remains therein. The excess liquid drains off. The container returns to its original position and the next exponentiation step follows.
  • the Patent US4911897 describes an automatic device for dilution, loosening and movement of homeopathic medicines.
  • the operating principle of this device is similar to the Skinner machine, the device has a preparation vial, which is tilted for emptying.
  • Laid-Open Publication DE3409341 is a device for diluting mother tinctures (mother tinctures) described by the Korsakoff method.
  • the device has a metering device for supplying distilled water to a potenziergefäss, a Vakuumvornchtung for emptying the Potenziergefässes and a vibrator for the treatment of the mixture.
  • the known machines have the common disadvantage that they are equipped with a tilting device or a vibrating device, which increases the cost and the cost of manufacturing and maintaining such machines and also adversely affects their life, because these moving parts are subject to wear ,
  • the document WO2004 / 010919A1 describes a device for producing isopathic agents.
  • the device consists of a funnel, from which a connecting tube leads into a vortex chamber formed in a vessel. In the upper part of the vortex chamber, a drain pipe is arranged.
  • the document states that this device is designed for home use for diluting saliva.
  • the diluent is water which is to be added per dilution operation in an amount between one and fifty liters.
  • the invention is based on the object to further develop a method for potentiating liquid to the effect that the product can be produced at any time reproducible, consistently high quality and at an affordable price. Further, the process should be time-saving.
  • This solution according to the invention has the advantage that considerably less expenditure of time is required for the production of particularly so-called high potencies than in the known manual and mechanical methods, which in turn leads to a more cost-effective product.
  • Another advantage of this invention is the reproducibility achieved by meeting the legal requirements (validation of the manufacturing process). This results in a consistently high quality of the manufactured products.
  • the injection takes place in the form of a jet directed onto the surface of the mixture remaining in the pot still. This favors a complete mixing of the liquids.
  • the removal of the part of the mixture is effected by a pressure difference between the interior of the expectoration vessel and a discharge line for the part of the mixture.
  • Another aspect of the invention relates to a device for potentiating liquids according to claim 4, comprising a pot, an injection device for a diluting liquid and a drain for a mixture formed in the pot, wherein the pot can be designed and / or arranged the drain so that with immobility held Potenziergefäss only a portion of the mixture formed in the pot can be removed through the drain and a residual amount of the mixture remains in the pot.
  • This invention has for its object to propose a device which is simple in construction and inexpensive to manufacture, which operates reliably and with which, in particular, a high dilution can be achieved in stages, with good mixing of the liquid to be diluted with the diluting liquid during operation.
  • the device according to the invention is characterized in that the outflow is arranged in the region of the deepest point of the expectoration vessel during operation and that the injection device projects into the region of the deepest point of the expectoration vessel during operation.
  • This device offers over the known from the prior art machines the advantage that due to a precisely reproducible residual amount and a good mixing of the liquids, the products manufactured with it correspond to a high quality standard. Thanks to the simplicity of the device, this itself, but in particular the potentiated with her products is inexpensive to produce. In addition, the Device are easily disassembled into all their parts in contact with the product so that a cleaning in an autoclave, ref. The replacement of the items can be done.
  • An embodiment of the device provides that the outflow in the pot is at the lowest point in operation and this point adjacent to the pot can a trough is formed in which collects the remaining amount of the mixture.
  • Such a Potenziergefäss is relatively easy to produce and provides excellent accuracy and reproducibility of the residual amount.
  • the pot has approximately the shape of a pear and has in the upper, narrow area a neck with an injection device receiving opening and in the lower, wide area the drain and the trough.
  • a design ensures a thorough swirling of the fluids during the injection process and, after injection, a rapid and complete outflow of the mixture from the vessel walls.
  • such a device not only allows a very good mixing and high reproducibility, but also relatively short mixing cycles.
  • the drain is designed as a pipe penetrating the bottom of the pot, which projects beyond the inner wall on the inside of the pot, so that a space receiving the residual quantity is formed.
  • a Potenziergefäss is also relatively easy to produce and offers excellent accuracy and reproducibility of the residual amount.
  • the volume of the residual amount can be adjusted by a displacement of the tube or a processing of the projecting into the pot expansion end of the tube.
  • the drain is designed as a suction tube directed substantially downwardly in the suction tube, whose free end is arranged at a distance from the lowest point of the potentiometer, so that under the free end of the suction pipe, a residual quantity receiving space is formed.
  • This embodiment allows the use of a particularly simple expansion pot and the remaining amount is adjustable by simply moving the suction tube.
  • the injection device is designed as a tube or nozzle and is arranged so that at least one liquid jet emerging from the injection device strikes the surface of the residual quantity. This favors a complete mixing of the liquids.
  • Fig. 1 shows a schematic diagram of the method and the device according to the invention.
  • the reference numeral 1 designates a pot, with 2 is an injector and 3 with an outflow.
  • Fig. 2 shows a schematic diagram of an inventive device.
  • the oblique position of the arrow 2 symbolizing the injection device indicates that the positioning of the injection device with respect to the potentiator vessel has a significant influence on the complete mixing of the liquids.
  • the injection device 2 is preferably designed as an injection nozzle. Of course, if required, more than one injector can be arranged in the pot.
  • Fig. 3 shows a first embodiment of the device.
  • the Potenziergefäss 1 has here in the bottom of a trough 4 in which remains after draining the mixture through the drain 3 a well-defined volume of the mixture.
  • Fig. 4 another embodiment of the device is shown.
  • the outflow formed as a pipe 3 is passed through the bottom of the pot still and projects beyond it by a small amount.
  • FIG. 5 Another embodiment of the device is in Fig. 5 shown.
  • the pot still has no bottom opening for discharging the mixture.
  • the drain is designed here as a tube 3, which projects from above into the pot.
  • a vacuum can be applied either at the outlet 3 or an overpressure can be generated in the interior of the expander 1.
  • the opening 5 of the Potenziergefässes must be closed.
  • a gas for example air, can be supplied through a line (not shown) or through the injection device 2.
  • Fig. 6 a fourth embodiment of the device.
  • a well 4 is arranged here, which defines an exact volume of the remaining mixture.
  • the pear-shaped design of this potentiator promotes both a thorough turbulence of the liquid during the injection process as well as a rapid and complete draining of the mixture after completion of the injection process.
  • the injection device 2 is directed exactly to the trough 4, so that the jet of thinner liquid meets the surface of the substance to be diluted and this completely mixed with the diluent.
  • the removal of the mixture from the Potenziergefäss 1 is supported by vacuum or pressure in this embodiment, as in connection with Fig. 5 has been described.
  • a dosing device ensures exact and reproducible compliance with the volume of the thinner liquid fed through the injection device 2 to the expander 1.
  • the injected amount of liquid per Potenzier Colour is for example 1 to 2 ml, depending on the residual amount in the pot.
  • FIGS. 3, 4 and 6 is installed in the drain 3 preferably a valve, not shown, which is closed during the potentizing process and is opened to drain or suck the mixture.
  • the individual components of the device in particular those which come into direct contact with the starting material or the potentiated liquid must fit into an autoclave to destroy the subtle information and the conditions prevailing there (pressure 2.5 bar, 135 ° C, at least 30 minutes Treatment) survive without significant material fatigue. Any items excluded from this must be replaced instead within minutes.
  • the device preferably has a treatment plant, which is fed with tap water. With upstream reverse osmosis, deionizer and UV lamp to reach the Aqua purificata quality. All materials in contact with the liquid must be selected accordingly corrosion resistant.
  • a programmable control device controls all process steps taking place in the device.
  • a numerical digital display shows the current exponentiation step. Faults are indicated by a signaling or corresponding interface.
  • a logging device can be provided, so that the production process and possibly also malfunctions can be checked at any time.
  • the control device is configured such that if the energy or water supply fails, at least the current exponentiation step can be completed completely.
  • the device preferably consists of a single production cell.
  • Cross-contamination means the inadvertent mixing of parts of two different systems and the associated impurities. Cross-contamination worsens at best the effectiveness of a drug; in the worst case, the drug is so contaminated by dangerous influences (bacteria, etc.) that it represents a danger. In homoeopathic high potencies occurs through the cross-contamination, an energetic mixture. As a result, a homeopathic complex is formed instead of the desired pure single agent, which must be avoided at all costs. Homeopathic medicines are particularly susceptible to cross-contamination due to the small amounts of active ingredients involved and the very high number of production steps.
  • the production cell also ensures that it can be produced unaffected by most environmental influences (aerosols, odors, etc.).
  • the injection system is preferably designed in such a way that, when injecting the diluent liquid into the pot, any possible splashes of the liquid already in the pot still can not get back into the injection system. The same applies to the device for sucking off the excess potency liquid.
  • All electrical components are preferably surrounded by a grounded metal housing to expose the delicate drugs to as little external interference as possible.
  • Potenziergefäss 1 is given a first volume of a starting material. Thereafter, the injection device 2 is used, which was also treated new or in the manner described above, and directed to the surface of the previously introduced starting material.
  • the injection device 2 is connected to a preparation and metering device for the diluting liquid, for example distilled water.
  • the drain 3 of the Potenziergefässes 1 is connected with the interposition of a valve with a vacuum device. Now the device can be put into operation.
  • a second volume which is for example one hundred times the first volume, injected in a jet on the surface of the starting material, whereby a Aufwirbelung and intensive mixing of the liquids takes place. Thereafter, the largest part, for example, 99% of the mixture can be removed from the Potenziergefäss. So that after the injection process, the mixture can flow down from the walls of the expectoration vessel and collect in the lower area of the expectoration vessel, the control device opens said valve only after an adjustable break of, for example, 0.5 seconds. The extracted mixture is collected and / or fed to a sewer. With the amount of the mixture remaining in the well 4 corresponding to the first volume, the injection and aspiration steps are repeated until the desired dilution is achieved.
  • the duration of a potentiation step is, for example, about 3 to 4 seconds.
  • the controller is programmed to halt the process by two potency steps prior to the calculated final potency so that, for example, a durable ethanol potency can be manually produced.
  • the automatic stop by the control device is displayed, for example optically and / or acoustically.
  • the upstream of the injector parts such as nozzle nut and Einspitzklotz be autoclaved. All other parts in contact with the product such as the injection nozzle, pot and tube are discarded after use and replaced with new ones. These new parts are cleaned with 73% ethanol before use in the device.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Catching Or Destruction (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)

Claims (9)

  1. Procédé de dynamisation de liquides dans lequel un premier volume d'un liquide à diluer est introduit dans un récipient de dynamisation, un deuxième volume d'un liquide diluant est injecté dans le récipient de dynamisation et ensuite une partie du mélange résultant est enlevée du récipient de dynamisation de telle manière qu'un premier volume du mélange demeure dans le récipient de dynamisation, le récipient de dynamisation étant immobilisé pendant l'ensemble du procédé, caractérisé en ce que les étapes consistant à amener du liquide diluant et à enlever le mélange sont répétées jusqu'à ce que le mélange demeurant dans le récipient de dynamisation présente la dilution souhaitée, et en ce qu'entre l'injection du liquide diluant et l'enlèvement de ladite partie du mélange est intercalée une pause.
  2. Procédé selon la revendication 1, caractérisé en ce que l'injection est effectuée sous la forme d'un jet dirigé sur la surface du mélange demeurant dans le récipient de dynamisation.
  3. Procédé selon l'une des revendications précédentes, caractérisé en ce que l'enlèvement de ladite partie du mélange est accompli par une différence de pression entre l'intérieur du récipient de dynamisation et une conduite d'écoulement pour ladite partie du mélange.
  4. Dispositif de dynamisation de liquides, comprenant un récipient de dynamisation (1), un dispositif d'injection (2) d'un liquide diluant et un écoulement (3) pour un mélange
    formé dans le récipient de dynamisation, le récipient de dynamisation (1) étant conformé et/ou l'écoulement (3) agencé de telle manière que lorsque le récipient de dynamisation (1) est immobilisé, une partie seulement du mélange formé dans le récipient de dynamisation peut être enlevée par l'écoulement (3) et une quantité restante du mélange demeure dans le récipient de dynamisation (1), caractérisé en ce que l'écoulement (3) est agencé dans la zone du point le plus bas en cours de fonctionnement du récipient de dynamisation (1), et que le dispositif d'injection (2) s'étend jusque dans la zone du point le plus bas en cours de fonctionnement du récipient de dynamisation (1) .
  5. Dispositif selon la revendication 4, caractérisé en ce que l'écoulement (3) se trouve dans le récipient de dynamisation (1) au point le plus bas en cours de fonctionnement de celui-ci et à proximité de ce point est formé dans le récipient de dynamisation (1) une cavité (4) où s'accumule ladite quantité restante du mélange.
  6. Dispositif selon la revendication 5, caractérisé en ce que le récipient de dynamisation présente la forme d'une poire approximativement et comprend dans sa partie supérieure étroite un cou avec une ouverture (5) recevant le dispositif d'injection (2) et dans sa partie inférieure plus large ledit écoulement (3) et ladite cavité (4).
  7. Dispositif selon la revendication 4, caractérisé en ce que l'écoulement (3) est réalisé sous la forme d'un tube passant par le fond du récipient de dynamisation (1) et qui dépasse de la paroi intérieure à l'intérieur du récipient de dynamisation (1) de telle manière qu'un espace recevant ladite quantité restante est formé.
  8. Dispositif selon la revendication 4, caractérisé en ce que l'écoulement (3) est réalisé sous la forme d'un tube d'aspiration essentiellement dirigé vers le bas dans le récipient de dynamisation (1) et dont l'extrémité libre est agencée à un écart du point le plus bas du récipient de dynamisation de telle manière que sous l'extrémité libre du tube d'aspiration est formé un espace recevant ladite quantité restante.
  9. Dispositif selon l'une quelconque des revendications 4 à 8, caractérisé en ce que le dispositif d'injection est réalisé sous la forme d'un tube ou d'une buse et est agencé de telle manière qu'au moins un jet de liquide émanant du dispositif d'injection (2) tombe sur la surface de ladite quantité restante.
EP06018516A 2006-09-05 2006-09-05 Méthode et appareil pour la dynamisation de liquides Active EP1897524B1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP06018516A EP1897524B1 (fr) 2006-09-05 2006-09-05 Méthode et appareil pour la dynamisation de liquides
AT06018516T ATE550009T1 (de) 2006-09-05 2006-09-05 Verfahren und vorrichtung zum potenzieren von flüssigkeiten

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP06018516A EP1897524B1 (fr) 2006-09-05 2006-09-05 Méthode et appareil pour la dynamisation de liquides

Publications (2)

Publication Number Publication Date
EP1897524A1 EP1897524A1 (fr) 2008-03-12
EP1897524B1 true EP1897524B1 (fr) 2012-03-21

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Application Number Title Priority Date Filing Date
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Country Status (2)

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EP (1) EP1897524B1 (fr)
AT (1) ATE550009T1 (fr)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2435283A1 (fr) * 1978-09-08 1980-04-04 Durand Texte Gerard Dispositif pour diluer de facon discontinue, a une concentration determinee, un liquide dans un autre liquide
SE462317B (sv) * 1988-10-31 1990-06-11 Profor Ab Saett och anordning foer att kontinuerligt utspaeda en koncentrerad loesning
CZ12592U1 (cs) * 2002-07-10 2002-09-06 Jiří Mgr. Čehovský Autoizopatická baňka

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EP1897524A1 (fr) 2008-03-12
ATE550009T1 (de) 2012-04-15

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