EP3008048A4 - Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf) - Google Patents

Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Info

Publication number: EP3008048A4
Authority: EP; European Patent Office
Prior art keywords: hydroxymethylfurfural; hmf; preparation
Prior art date: 2013-06-12
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Withdrawn

Application number

EP14810780.8A

Other languages

English (en)

French (fr)

Other versions

EP3008048A2 (de

Inventor

Dr Benoit Blank

Dr Alois Kindler

Dr Peter Bassler

Dr Markus Piepenbrink

Ortmund Lang

Carmen Feldner

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

BASF SE

Original Assignee

BASF SE

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2013-06-12

Filing date

2014-06-11

Publication date

2016-12-14

2014-06-11 Application filed by BASF SE filed Critical BASF SE

2014-06-11 Priority to EP14810780.8A priority Critical patent/EP3008048A4/de

2016-04-20 Publication of EP3008048A2 publication Critical patent/EP3008048A2/de

2016-12-14 Publication of EP3008048A4 publication Critical patent/EP3008048A4/de

Status Withdrawn legal-status Critical Current

Links

NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 title 1
RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 title 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Furan Compounds (AREA)
Catalysts (AREA)

EP14810780.8A 2013-06-12 2014-06-11 Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf) Withdrawn EP3008048A4 (de)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
EP14810780.8A EP3008048A4 (de)	2013-06-12	2014-06-11	Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
EP13171627.6A EP2813494A1 (de)	2013-06-12	2013-06-12	Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)
EP14810780.8A EP3008048A4 (de)	2013-06-12	2014-06-11	Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)
PCT/IB2014/062121 WO2014199306A2 (de)	2013-06-12	2014-06-11	Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Publications (2)

Publication Number	Publication Date
EP3008048A2 EP3008048A2 (de)	2016-04-20
EP3008048A4 true EP3008048A4 (de)	2016-12-14

Family

ID=48577625

Family Applications (2)

Application Number	Title	Priority Date	Filing Date
EP13171627.6A Withdrawn EP2813494A1 (de)	2013-06-12	2013-06-12	Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)
EP14810780.8A Withdrawn EP3008048A4 (de)	2013-06-12	2014-06-11	Verfahren zur herstellung von 5-hydroxymethylfurfural (hmf)

Family Applications Before (1)

Application Number	Title	Priority Date	Filing Date
EP13171627.6A Withdrawn EP2813494A1 (de)	2013-06-12	2013-06-12	Verfahren zur Herstellung von 5-Hydroxymethylfurfural (HMF)

Country Status (8)

Country	Link
US (1)	US9260402B2 (de)
EP (2)	EP2813494A1 (de)
JP (1)	JP2016523852A (de)
KR (1)	KR20160018703A (de)
CN (1)	CN105452231A (de)
CA (1)	CA2914308A1 (de)
RU (1)	RU2016100205A (de)
WO (1)	WO2014199306A2 (de)

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EP3077453B1 (de)	2013-12-06	2018-03-28	Basf Se	Weichmacher-zusammensetzung, die tetrahydrofuranderivate und 1,2-cyclohexandicarbonsäureester enthält
WO2016094878A1 (en)	2014-12-12	2016-06-16	Virdia, Inc.	Methods for converting cellulose to furanic products
WO2016206909A1 (de)	2015-06-24	2016-12-29	Basf Se	Verfahren zur herstellung von 5-hydroxymethylfurfural und huminen
WO2016207025A1 (de)	2015-06-24	2016-12-29	Basf Se	Verfahren zum herstellen und abtrennen von hmf
WO2016207365A1 (de) *	2015-06-24	2016-12-29	Basf Se	Verfahren zur kontinuierlichen herstellung von 5-hydroxymethyl-furfural (hmf) in einer reaktoranordnung
WO2017184545A1 (en) *	2016-04-18	2017-10-26	Rennovia, Inc.	Conversion of fructose-containing feedstocks to hmf-containing product
US11274089B2 (en)	2016-06-27	2022-03-15	Nihon Shokuhin Kako Co., Ltd.	5-hydroxymethyl-2-furfural production method
JP6293333B2 (ja) *	2016-06-27	2018-03-14	日本食品化工株式会社	５−ヒドロキシメチル−２−フルフラールの製造方法
EP3366468B1 (de) *	2017-02-27	2022-04-06	AVA Biochem AG	Verfahren zur herstellung thermisch härtbarer harze sowie durch das verfahren erhältliche harze
EP3366712A1 (de)	2017-02-27	2018-08-29	AVALON Industries AG	Neue hmf-oligomere
EP3366714B1 (de) *	2017-02-27	2022-03-30	AVA Biochem AG	Verfahren zur herstellung thermisch härtbarer phenolharze sowie durch das verfahren erhältliche phenolharze
CN107501215B (zh) *	2017-09-18	2020-10-30	中国农业大学	一种连续化制备5-羟甲基糠醛及其衍生物的方法和装置
EP3498699A1 (de)	2017-12-13	2019-06-19	Basf Se	Chromatographieverfahren zur reinigung von furfuralderivaten
TWI664291B (zh) *	2018-11-14	2019-07-01	遠東新世紀股份有限公司	自含有葡萄糖之原料製備5-羥甲基糠醛的方法
RU187166U1 (ru) *	2018-11-15	2019-02-21	Нина Владимировна Смирнова	Лабораторно-исследовательский стенд для изучения процессов дегидратации углеводов
CN109651308A (zh) *	2019-02-15	2019-04-19	陈茁	一种5-羟甲基糠醛的纯化方法
WO2020214419A1 (en) *	2019-04-15	2020-10-22	Stora Enso Oyj	Process for the recovery of solvent and isolation of humin materials and compositions thereof
CN110368985B (zh) *	2019-07-04	2022-05-31	浙江工业大学	一种用于5-hmf合成的催化剂及5-hmf的制备方法
CN110586114A (zh) *	2019-09-19	2019-12-20	天津大学	一种铜铬铝水滑石催化剂的制备方法及催化氧化5-羟甲基糠醛的应用
CN119462576A (zh) *	2024-11-26	2025-02-18	中国科学技术大学	制备5,5'-氧基双亚甲基-2-糠醛的方法及装置

Citations (1)

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Publication number	Priority date	Publication date	Assignee	Title
CN102399203A (zh) *	2011-12-19	2012-04-04	浙江大学	一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法

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US4400468A (en)	1981-10-05	1983-08-23	Hydrocarbon Research Inc.	Process for producing adipic acid from biomass
DE3601281A1 (de)	1986-01-17	1987-07-23	Sueddeutsche Zucker Ag	Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
FR2663933B1 (fr)	1990-06-27	1994-06-17	Beghin Say Sa	Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
FR2664273B1 (fr)	1990-06-27	1994-04-29	Beghin Say Sa	Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
FR2670209B1 (fr) *	1990-12-07	1995-04-28	Commissariat Energie Atomique	Procede de preparation d'hydroxymethyl-5 furfural par catalyse heterogene.
DE10202838A1 (de)	2002-01-24	2003-08-07	Basf Ag	Verfahren zur Abtrennung von Säuren aus chemischen Reaktionsgemischen mit Hilfe von ionischen Flüssigkeiten
FR2858618B1 (fr) *	2003-08-07	2006-02-24	Sucreries Et Raffineries D Ers	Procede et reacteur de fabrication d'hydroxymethylfurfural
EP1834950A1 (de)	2006-03-10	2007-09-19	Avantium International B.V.	Verfahren zur Herstellung von Alkoxymethylfurfuralen und deren Verwenung
EP1834951A1 (de)	2006-03-10	2007-09-19	Avantium International B.V.	Verfahren zur Herstellung von organischen 5-Hydroxymethylfurfuralsäureestern und ihre Verwendung
BRPI0806908A2 (pt)	2007-01-23	2014-04-29	Basf Se	Processos para a prepração de um produto de glicose a partir de um material lignocelulósico, e para a preparação de um produto de metabolismo microbiano, produto de glicose, e, produto de lignina
CN101617055A (zh)	2007-01-23	2009-12-30	巴斯夫欧洲公司	通过对使用含多原子阴离子的离子液体从含木素纤维素的材料得到的纤维素进行酶促水解来制备葡萄糖的方法
CN101812039B (zh) *	2010-05-14	2012-09-26	天津大学	一种利用离子液体催化生成5－羟甲基糠醛的方法
BR112014011672A2 (pt)	2011-11-23	2017-05-30	Segetis Inc	processo para preparar ácido levulínico

2013
- 2013-06-12 EP EP13171627.6A patent/EP2813494A1/de not_active Withdrawn
2014
- 2014-06-11 KR KR1020167000350A patent/KR20160018703A/ko not_active Withdrawn
- 2014-06-11 CN CN201480044683.9A patent/CN105452231A/zh active Pending
- 2014-06-11 CA CA2914308A patent/CA2914308A1/en not_active Abandoned
- 2014-06-11 EP EP14810780.8A patent/EP3008048A4/de not_active Withdrawn
- 2014-06-11 RU RU2016100205A patent/RU2016100205A/ru not_active Application Discontinuation
- 2014-06-11 US US14/302,046 patent/US9260402B2/en not_active Expired - Fee Related
- 2014-06-11 WO PCT/IB2014/062121 patent/WO2014199306A2/de not_active Ceased
- 2014-06-11 JP JP2016518622A patent/JP2016523852A/ja not_active Withdrawn

Patent Citations (1)

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Publication number	Priority date	Publication date	Assignee	Title
CN102399203A (zh) *	2011-12-19	2012-04-04	浙江大学	一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法

Non-Patent Citations (1)

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Title
ZUONJUN WI ET AL: "Entrainer-intensified vacuum reactive distillation process for the separation of 5-hydroxymethylfurfural from the dehydration of carbohydrates catalyzed by a metal salt-ionic liquid", GREEN CHEMISTRY, vol. 14, 7 March 2012 (2012-03-07), pages 1220 - 1226, XP002712463 *

Also Published As

Publication number	Publication date
CN105452231A (zh)	2016-03-30
US20140371473A1 (en)	2014-12-18
JP2016523852A (ja)	2016-08-12
WO2014199306A2 (de)	2014-12-18
WO2014199306A3 (de)	2015-04-23
RU2016100205A (ru)	2017-07-17
RU2016100205A3 (de)	2018-04-26
EP2813494A1 (de)	2014-12-17
CA2914308A1 (en)	2014-12-18
US9260402B2 (en)	2016-02-16
KR20160018703A (ko)	2016-02-17
EP3008048A2 (de)	2016-04-20

Legal Events

Date	Code	Title	Description
2016-03-18	PUAI	Public reference made under article 153(3) epc to a published international application that has entered the european phase	Free format text: ORIGINAL CODE: 0009012
2016-04-20	17P	Request for examination filed	Effective date: 20160112
2016-04-20	AK	Designated contracting states	Kind code of ref document: A2 Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR
2016-04-20	AX	Request for extension of the european patent	Extension state: BA ME
2016-09-21	DAX	Request for extension of the european patent (deleted)
2016-11-02	R17P	Request for examination filed (corrected)	Effective date: 20160112
2016-12-14	A4	Supplementary search report drawn up and despatched	Effective date: 20161110
2016-12-14	RIC1	Information provided on ipc code assigned before grant	Ipc: B01D 3/00 20060101ALI20161104BHEP Ipc: C07D 307/48 20060101AFI20161104BHEP Ipc: C07D 307/46 20060101ALI20161104BHEP
2017-07-25	GRAP	Despatch of communication of intention to grant a patent	Free format text: ORIGINAL CODE: EPIDOSNIGR1
2017-08-23	INTG	Intention to grant announced	Effective date: 20170726
2018-04-27	STAA	Information on the status of an ep patent application or granted ep patent	Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN
2018-05-30	18D	Application deemed to be withdrawn	Effective date: 20171206

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