EP3046169A4 - Lithiumsulfid-eisen-kohlenstoff-verbundkörper - Google Patents

Lithiumsulfid-eisen-kohlenstoff-verbundkörper Download PDF

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Publication number
EP3046169A4
EP3046169A4 EP14843674.4A EP14843674A EP3046169A4 EP 3046169 A4 EP3046169 A4 EP 3046169A4 EP 14843674 A EP14843674 A EP 14843674A EP 3046169 A4 EP3046169 A4 EP 3046169A4
Authority
EP
European Patent Office
Prior art keywords
iron
carbon composite
composite body
lithium sulfide
sulfide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP14843674.4A
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English (en)
French (fr)
Other versions
EP3046169A1 (de
EP3046169B1 (de
EP3046169A8 (de
Inventor
Tomonari Takeuchi
Atsushi Sakuda
Hiroyuki Kageyama
Hikari Sakaebe
Kuniaki Tatsumi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
National Institute of Advanced Industrial Science and Technology
Original Assignee
National Institute of Advanced Industrial Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by National Institute of Advanced Industrial Science and Technology filed Critical National Institute of Advanced Industrial Science and Technology
Publication of EP3046169A1 publication Critical patent/EP3046169A1/de
Publication of EP3046169A8 publication Critical patent/EP3046169A8/de
Publication of EP3046169A4 publication Critical patent/EP3046169A4/de
Application granted granted Critical
Publication of EP3046169B1 publication Critical patent/EP3046169B1/de
Not-in-force legal-status Critical Current
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/581—Chalcogenides or intercalation compounds thereof
    • H01M4/5815—Sulfides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/22—Alkali metal sulfides or polysulfides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/009—Compounds containing iron, with or without oxygen or hydrogen, and containing two or more other elements
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562—Solid materials
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/058—Construction or manufacture
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/42—Methods or arrangements for servicing or maintenance of secondary cells or secondary half-cells
    • H01M10/44—Methods for charging or discharging
    • H01M10/446—Initial charging measures
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H01M4/043—Processes of manufacture in general involving compressing or compaction
    • H01M4/0433—Molding
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H01M4/0438—Processes of manufacture in general by electrochemical processing
    • H01M4/044—Activating, forming or electrochemical attack of the supporting material
    • H01M4/0445—Forming after manufacture of the electrode, e.g. first charge, cycling
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/362—Composites
    • H01M4/364—Composites as mixtures
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/38—Selection of substances as active materials, active masses, active liquids of elements or alloys
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/027—Negative electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2220/00—Batteries for particular applications
    • H01M2220/20—Batteries in motive systems, e.g. vehicle, ship, plane
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2220/00—Batteries for particular applications
    • H01M2220/30—Batteries in portable systems, e.g. mobile phone, laptop
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0065—Solid electrolytes
    • H01M2300/0068—Solid electrolytes inorganic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T10/00—Road transport of goods or passengers
    • Y02T10/60—Other road transportation technologies with climate change mitigation effect
    • Y02T10/70—Energy storage systems for electromobility, e.g. batteries

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  • Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Composite Materials (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
EP14843674.4A 2013-09-13 2014-09-10 Lithiumsulfid-eisen-kohlenstoff-verbundkörper Not-in-force EP3046169B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2013190215 2013-09-13
PCT/JP2014/073871 WO2015037598A1 (ja) 2013-09-13 2014-09-10 硫化リチウム－鉄－炭素複合体

Publications (4)

Publication Number Publication Date
EP3046169A1 EP3046169A1 (de) 2016-07-20
EP3046169A8 EP3046169A8 (de) 2016-09-14
EP3046169A4 true EP3046169A4 (de) 2017-05-31
EP3046169B1 EP3046169B1 (de) 2018-08-29

Family

ID=52665700

Family Applications (1)

Application Number Title Priority Date Filing Date
EP14843674.4A Not-in-force EP3046169B1 (de) 2013-09-13 2014-09-10 Lithiumsulfid-eisen-kohlenstoff-verbundkörper

Country Status (6)

Country Link
US (1) US10290870B2 (de)
EP (1) EP3046169B1 (de)
JP (1) JP6150233B2 (de)
KR (1) KR102225165B1 (de)
CN (1) CN105518913B (de)
WO (1) WO2015037598A1 (de)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10424779B1 (en) 2016-09-07 2019-09-24 Google Llc Lithium-ion cells and methods of manufacture
US10707531B1 (en) 2016-09-27 2020-07-07 New Dominion Enterprises Inc. All-inorganic solvents for electrolytes
JP6978887B2 (ja) * 2017-10-10 2021-12-08 古河機械金属株式会社 無機材料の製造方法
CN109037672B (zh) * 2018-09-13 2020-07-17 广东邦普循环科技有限公司 一种动力电池用镍钴锰酸锂材料的制备方法
CN110931783B (zh) * 2019-12-06 2021-05-28 华南师范大学 一种硫化锂/纳米金属正极复合材料及其制备方法与应用
CN111740170B (zh) * 2020-08-18 2020-11-17 浙江艾罗网络能源技术有限公司 一种线缆结构全固态锂硫电池及其制备方法
CN111977703B (zh) * 2020-08-21 2023-09-05 天目湖先进储能技术研究院有限公司 Li2O、Li2CO3包覆过渡金属硫化物基正极材料及制备方法和应用
JP7400765B2 (ja) * 2021-04-01 2023-12-19 トヨタ自動車株式会社 全固体電池の製造方法
WO2023167132A1 (ja) * 2022-03-03 2023-09-07 国立研究開発法人産業技術総合研究所 硫化リチウム－鉄－炭素複合体
JP7797056B2 (ja) * 2022-11-04 2026-01-13 国立研究開発法人産業技術総合研究所 鉄含有多硫化リチウム
KR20250063831A (ko) * 2023-10-27 2025-05-09 삼성에스디아이 주식회사 양극 혼합제, 이를 포함하는 양극을 포함하는 고체 이차전지 및 그 제조방법
CN118352479B (zh) * 2024-06-18 2024-09-13 浙江省白马湖实验室有限公司 一种自支撑锂离子硫电池正极的制备方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3907589A (en) * 1974-01-18 1975-09-23 Us Energy Cathode for a secondary electrochemical cell
WO2010084808A1 (ja) * 2009-01-22 2010-07-29 独立行政法人産業技術総合研究所 硫化鉄リチウム複合体の製造方法
US20110223481A1 (en) * 2007-08-24 2011-09-15 National Institute Of Advanced Industrial Science And Technology Process for producing metal sulfide
JP2013075816A (ja) * 2011-09-13 2013-04-25 Nippon Chem Ind Co Ltd 硫化リチウム、その製造方法及び無機固体電解質の製造方法

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US4006034A (en) * 1976-03-11 1977-02-01 The United States Of America As Represented By The United States Energy Research And Development Administration Method of preparing an electrochemical cell in uncharged state
JP4747482B2 (ja) 2003-07-29 2011-08-17 三菱化学株式会社 リチウム二次電池用正極材料、リチウム二次電池用正極及びリチウム二次電池
KR101099225B1 (ko) * 2004-02-13 2011-12-27 산요덴키가부시키가이샤 비수성 전해질 2차 전지용 양극 및 그의 제조 방법 및비수성 전해질 2차 전지 및 그의 제조 방법
JP2005228586A (ja) * 2004-02-13 2005-08-25 Sanyo Electric Co Ltd 非水電解質二次電池およびその製造方法
JP2009283344A (ja) * 2008-05-23 2009-12-03 Idemitsu Kosan Co Ltd リチウム電池用負極合材、リチウム電池用負極、リチウム電池、装置およびリチウム電池用負極合材の製造方法
JP5299971B2 (ja) * 2009-10-27 2013-09-25 独立行政法人産業技術総合研究所 リチウムイオン二次電池用電極活物質及びその製造方法
JP5660538B2 (ja) * 2011-07-21 2015-01-28 独立行政法人産業技術総合研究所 全固体二次電池用電極体、全固体二次電池、全固体二次電池用電極体の製造方法、全固体二次電池の製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3907589A (en) * 1974-01-18 1975-09-23 Us Energy Cathode for a secondary electrochemical cell
US20110223481A1 (en) * 2007-08-24 2011-09-15 National Institute Of Advanced Industrial Science And Technology Process for producing metal sulfide
WO2010084808A1 (ja) * 2009-01-22 2010-07-29 独立行政法人産業技術総合研究所 硫化鉄リチウム複合体の製造方法
JP2013075816A (ja) * 2011-09-13 2013-04-25 Nippon Chem Ind Co Ltd 硫化リチウム、その製造方法及び無機固体電解質の製造方法

Non-Patent Citations (1)

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Title
See also references of WO2015037598A1 *

Also Published As

Publication number Publication date
EP3046169A1 (de) 2016-07-20
CN105518913A (zh) 2016-04-20
JPWO2015037598A1 (ja) 2017-03-02
CN105518913B (zh) 2018-05-25
KR102225165B1 (ko) 2021-03-09
EP3046169B1 (de) 2018-08-29
KR20160055213A (ko) 2016-05-17
US10290870B2 (en) 2019-05-14
WO2015037598A1 (ja) 2015-03-19
JP6150233B2 (ja) 2017-06-21
EP3046169A8 (de) 2016-09-14
US20160268606A1 (en) 2016-09-15

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