EP4366771A4 - Procédé de préparation d'acide 2-nitro-4-méthylsulfonylbenzoïque pur - Google Patents
Procédé de préparation d'acide 2-nitro-4-méthylsulfonylbenzoïque purInfo
- Publication number
- EP4366771A4 EP4366771A4 EP22837192.8A EP22837192A EP4366771A4 EP 4366771 A4 EP4366771 A4 EP 4366771A4 EP 22837192 A EP22837192 A EP 22837192A EP 4366771 A4 EP4366771 A4 EP 4366771A4
- Authority
- EP
- European Patent Office
- Prior art keywords
- nitro
- pure
- preparation
- methylsulfonylbenzoic acid
- methylsulfonylbenzoic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C317/00—Sulfones; Sulfoxides
- C07C317/44—Sulfones; Sulfoxides having sulfone or sulfoxide groups and carboxyl groups bound to the same carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
- C07C303/08—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with halogenosulfonic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
- C07C315/04—Preparation of sulfones; Preparation of sulfoxides by reactions not involving the formation of sulfone or sulfoxide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
- C07C315/06—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IN202121030817 | 2021-07-09 | ||
| PCT/IN2022/050623 WO2023281536A1 (fr) | 2021-07-09 | 2022-07-08 | Procédé de préparation d'acide 2-nitro-4-méthylsulfonylbenzoïque pur |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EP4366771A1 EP4366771A1 (fr) | 2024-05-15 |
| EP4366771A4 true EP4366771A4 (fr) | 2025-06-25 |
Family
ID=84800431
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP22837192.8A Pending EP4366771A4 (fr) | 2021-07-09 | 2022-07-08 | Procédé de préparation d'acide 2-nitro-4-méthylsulfonylbenzoïque pur |
Country Status (3)
| Country | Link |
|---|---|
| EP (1) | EP4366771A4 (fr) |
| CN (1) | CN117794567A (fr) |
| WO (1) | WO2023281536A1 (fr) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116589384A (zh) * | 2023-04-19 | 2023-08-15 | 贵州微化科技有限公司 | 一种利用微通道反应器合成3-硝基-4-甲基苯磺酰氯的方法 |
| CN118420495A (zh) * | 2024-04-30 | 2024-08-02 | 金华双宏化工有限公司 | 连续制备3-硝基-4-甲基苯磺酰氯的方法 |
| CN119930484A (zh) * | 2025-02-20 | 2025-05-06 | 辽宁龙田化工科技有限公司 | 一种4-甲砜基甲苯衍生物的合成方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103121961A (zh) * | 2013-02-05 | 2013-05-29 | 江苏中旗作物保护股份有限公司 | 除草剂甲基磺草酮中间体2-硝基-4-甲磺酰基甲苯合成方法 |
| CN103772243A (zh) * | 2013-12-30 | 2014-05-07 | 北京英力精化技术发展有限公司 | 一种甲基磺草酮的制备方法 |
| CN106699616A (zh) * | 2016-11-17 | 2017-05-24 | 北京颖泰嘉和生物科技股份有限公司 | 一种新的2‑硝基‑4‑甲磺酰基苯甲酸的纯化方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5136043A (en) * | 1989-06-17 | 1992-08-04 | Hoechst Aktiengesellschaft | Process for the preparation of aromatic sulfonyl chlorides |
| DE4235155A1 (de) * | 1992-10-19 | 1994-04-21 | Basf Ag | Verfahren zur Herstellung von Methylsulfonylbenzoesäuren |
-
2022
- 2022-07-08 WO PCT/IN2022/050623 patent/WO2023281536A1/fr not_active Ceased
- 2022-07-08 EP EP22837192.8A patent/EP4366771A4/fr active Pending
- 2022-07-08 CN CN202280054627.8A patent/CN117794567A/zh active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103121961A (zh) * | 2013-02-05 | 2013-05-29 | 江苏中旗作物保护股份有限公司 | 除草剂甲基磺草酮中间体2-硝基-4-甲磺酰基甲苯合成方法 |
| CN103772243A (zh) * | 2013-12-30 | 2014-05-07 | 北京英力精化技术发展有限公司 | 一种甲基磺草酮的制备方法 |
| CN106699616A (zh) * | 2016-11-17 | 2017-05-24 | 北京颖泰嘉和生物科技股份有限公司 | 一种新的2‑硝基‑4‑甲磺酰基苯甲酸的纯化方法 |
Non-Patent Citations (1)
| Title |
|---|
| See also references of WO2023281536A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| EP4366771A1 (fr) | 2024-05-15 |
| CN117794567A (zh) | 2024-03-29 |
| WO2023281536A1 (fr) | 2023-01-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE INTERNATIONAL PUBLICATION HAS BEEN MADE |
|
| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: REQUEST FOR EXAMINATION WAS MADE |
|
| 17P | Request for examination filed |
Effective date: 20240105 |
|
| AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR |
|
| DAV | Request for validation of the european patent (deleted) | ||
| DAX | Request for extension of the european patent (deleted) | ||
| REG | Reference to a national code |
Ref country code: DE Ref legal event code: R079 Free format text: PREVIOUS MAIN CLASS: A61K0039390000 Ipc: C07C0303080000 |
|
| A4 | Supplementary search report drawn up and despatched |
Effective date: 20250528 |
|
| RIC1 | Information provided on ipc code assigned before grant |
Ipc: C07C 315/06 20060101ALI20250522BHEP Ipc: C07C 317/14 20060101ALI20250522BHEP Ipc: C07C 317/44 20060101ALI20250522BHEP Ipc: C07C 315/04 20060101ALI20250522BHEP Ipc: C07C 315/00 20060101ALI20250522BHEP Ipc: C07C 309/86 20060101ALI20250522BHEP Ipc: C07C 303/08 20060101AFI20250522BHEP |