EP4621078A1 - Four à vide avec trempe par eau - Google Patents

Four à vide avec trempe par eau

Info

Publication number
EP4621078A1
EP4621078A1 EP25164261.7A EP25164261A EP4621078A1 EP 4621078 A1 EP4621078 A1 EP 4621078A1 EP 25164261 A EP25164261 A EP 25164261A EP 4621078 A1 EP4621078 A1 EP 4621078A1
Authority
EP
European Patent Office
Prior art keywords
chamber
water
quenching
vacuum
furnace
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP25164261.7A
Other languages
German (de)
English (en)
Inventor
Maciej Korecki
Wieslaw Fujak
Marek Stankiewicz
Tomasz Sobiak
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Seco/Warwick SA
Original Assignee
Seco/Warwick SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Seco/Warwick SA filed Critical Seco/Warwick SA
Publication of EP4621078A1 publication Critical patent/EP4621078A1/fr
Pending legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B9/00Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity
    • F27B9/04Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity adapted for treating the charge in vacuum or special atmosphere
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0056Furnaces through which the charge is moved in a horizontal straight path
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/56General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering characterised by the quenching agents
    • C21D1/60Aqueous agents
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/62Quenching devices
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/62Quenching devices
    • C21D1/63Quenching devices for bath quenching
    • C21D1/64Quenching devices for bath quenching with circulating liquids
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/74Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/74Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
    • C21D1/773Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material under reduced pressure or vacuum
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0006Details, accessories not peculiar to any of the following furnaces
    • C21D9/0018Details, accessories not peculiar to any of the following furnaces for charging, discharging or manipulation of charge
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0062Heat-treating apparatus with a cooling or quenching zone
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00Arrangements for supplying or controlling air or other gases for drying solid materials or objects
    • F26B21/40Arrangements for supplying or controlling air or other gases for drying solid materials or objects using gases other than air
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00Drying solid materials or objects by processes involving the application of heat
    • F26B3/28Drying solid materials or objects by processes involving the application of heat by radiation, e.g. from the sun
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/042Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum for drying articles or discrete batches of material in a continuous or semi-continuous operation, e.g. with locks or other air tight arrangements for charging/discharging
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/02Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated of multiple-chamber type
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/04Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated adapted for treating the charge in vacuum or special atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D15/00Handling or treating discharged material; Supports or receiving chambers therefor
    • F27D15/02Cooling
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories or equipment specially adapted for furnaces of these types
    • F27B2005/062Cooling elements
    • F27B2005/068Cooling elements for external cooling
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B9/00Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity
    • F27B9/12Furnaces through which the charge is moved mechanically, e.g. of tunnel type; Similar furnaces in which the charge moves by gravity with special arrangements for preheating or cooling the charge
    • F27B2009/124Cooling

Definitions

  • the present invention relates to a vacuum furnace with water quenching, designed for the heat treatment of metals and alloys necessitating rapid quenching.
  • Vacuum heat treatment devices heat the charge in a vacuum, thereby preventing surface oxidation, and then cool the charge in an atmosphere of inert gases including nitrogen, argon, or helium, or in dedicated quenching oils.
  • Furnaces featuring oil quenching generally include a separate, sealed quenching chamber with an integrated oil tank for quenching.
  • Other known approaches utilize baths containing salt or polymer solutions for quenching.
  • the patent document CN216107091U describes a modular vacuum heat treatment production line that includes several dedicated modules for performing different operations within a single apparatus, such as quenching in gas, oil, water, or brine.
  • the line includes a hot material transfer module and a cold material transfer module, with the operating modules positioned on either side of these transfer modules.
  • the patent document CN213835455U describes a vacuum hardening furnace with temperature regulation and control, featuring a furnace body whose interior is protected by a heat-insulating plate, thus forming a heating chamber and a quenching chamber.
  • the quenching chamber features a tank containing a quenching medium at its bottom, which is cooled by an external circulation cooling device.
  • the circulating cooling device comprises a circulation pipeline, a heat exchanger, a heat exchange pipeline, and a chilled water unit.
  • a circulation pipeline connects the heat exchanger to the interior of the quenching tank, creating a closed loop.
  • the circulation pipeline connects to the circulation pump and the first group of valves, which controls the connection or disconnection of the pipeline.
  • the chilled water unit is connected to the heat exchanger via a heat exchange pipeline, forming a loop.
  • the heat exchange pipeline connects to the water pump and the second set of valves, which controls the connection or disconnection of the pipeline.
  • a temperature measuring element is placed in the quenching tank and is connected to a programmable logic controller (PLC) located within the furnace body. In addition to the temperature measuring element, the PLC is connected to the first valve group, the second valve group of the chilled water unit, and the heat exchanger.
  • PLC programmable logic controller
  • water serves as an effective quenching medium for carbon and low-alloy steels, even those exhibiting low hardenability.
  • a limitation of water as a quenching medium is its propensity for high reactivity with the surface of the metal workpiece. Furthermore, the high volatility of water leads to contamination of the protective atmosphere or hinders achieving the required vacuum level in the furnace.
  • the present invention seeks to provide a vacuum furnace design for the heat treatment of metals and alloys requiring rapid quenching, integrating the benefits of vacuum treatment and water quenching without the limitations previously described.
  • the vacuum furnace with water quenching comprises a loading and unloading chamber with a transport mechanism, a vacuum heating chamber equipped with thermal insulation and a graphite heating system, and a quenching chamber, all separated by vacuum-tight doors.
  • the vacuum furnace with water quenching is characterised in that it features a central loading and unloading chamber.
  • This chamber is equipped with a transport mechanism, a vacuum pumping system, and heat radiators for the rapid removal of water and moisture from the charge following the quenching process.
  • a vacuum heating chamber is located on one side of the loading and unloading chamber, and a water quenching chamber on the other.
  • the water quenching chamber is equipped with a heater and a water agitator to control the quenching water temperature, as well as an immersion system for the charge and a vacuum pumping system.
  • a protective atmosphere is maintained in the quenching chamber - inert gas or vacuum.
  • the vacuum furnace of the present invention facilitates heating the charge in a controlled protective vacuum and intensive water quenching within a single device, thereby minimizing the detrimental oxidation of the charge surface.
  • Fig. 1 is a schematic cross-sectional view of a vacuum furnace with water quenching
  • Fig. 2 is a cross-sectional view of an embodiment of a vacuum furnace with water quenching
  • Fig. 3 is a cross-sectional view of the water quenching chamber of the furnace.
  • the vacuum furnace with water quenching contains three chambers, separated by tight vacuum-tight doors 8.
  • the central chamber is the loading and unloading chamber 1, which is equipped with a transport mechanism 4, a vacuum pump system 12 and heat radiators 11 for the rapid removal of water and moisture from the charge following the quenching process
  • a vacuum heating chamber 2 equipped with graphite insulation 5, a graphite heating system 6 and a vacuum pump system 14 enabling the heating of the charge in a protective vacuum atmosphere, and on the other side there is a water quenching chamber 3.
  • a heater 9 and water agitators 10 are installed in the water quenching chamber 3 to regulate the quenching water temperature, as well as an immersion system 7 for transporting the charge and a vacuum pumping system 13, wherein a protective atmosphere, a vacuum or an inert gas atmosphere is maintained in the quenching chamber.
  • the charge In a vacuum furnace with water quenching, the charge is heated under vacuum, which provides a protective atmosphere. Subsequently, all furnace chambers 1, 2, 3 are purged with an inert gas, such as nitrogen or argon, before the charge is transported to the water tank within the quenching chamber 3 by a transport mechanism 4.
  • an inert gas such as nitrogen or argon
  • the quenching chamber 3 the charge is immersed in water by means of an immersion system 7.
  • the charge is rapidly quenched in water and then, after the water has drained, it is transported in a protective gas atmosphere to the loading and unloading chamber 1 for rapid removal of residual moisture.
  • the loading and unloading chamber 1 acts as a vacuum dryer.
  • a vacuum pumping system 12 evacuates the gaseous atmosphere, and then the heat emitters 11 are activated, ensuring rapid drying of the load from residual water and moisture.
  • the transport chamber is purged with gas, and the charge is ready for unloading.

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Furnace Details (AREA)
  • Muffle Furnaces And Rotary Kilns (AREA)
  • Tunnel Furnaces (AREA)
EP25164261.7A 2024-03-20 2025-03-17 Four à vide avec trempe par eau Pending EP4621078A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL448051A PL448051A1 (pl) 2024-03-20 2024-03-20 Piec próżniowy z chłodzeniem w wodzie

Publications (1)

Publication Number Publication Date
EP4621078A1 true EP4621078A1 (fr) 2025-09-24

Family

ID=94944789

Family Applications (1)

Application Number Title Priority Date Filing Date
EP25164261.7A Pending EP4621078A1 (fr) 2024-03-20 2025-03-17 Four à vide avec trempe par eau

Country Status (2)

Country Link
EP (1) EP4621078A1 (fr)
PL (1) PL448051A1 (fr)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011026653A (ja) * 2009-07-24 2011-02-10 Daido Steel Co Ltd 焼入装置
JP2012012637A (ja) * 2010-06-29 2012-01-19 Furutekku Kk 熱処理加工方法、熱処理加工物及び熱処理加工装置
US20130153547A1 (en) * 2010-07-02 2013-06-20 Kazuhiko Katsumata Multi-chamber heat treatment device
CN104451044A (zh) * 2014-12-31 2015-03-25 湖南顶立科技有限公司 一种真空淬火方法
CN204874589U (zh) * 2015-06-03 2015-12-16 中山凯旋真空技术工程有限公司 高真空水淬固溶炉系统
JP2016089251A (ja) * 2014-11-10 2016-05-23 中外炉工業株式会社 熱処理設備
US20170254592A1 (en) * 2015-04-02 2017-09-07 Ihi Corporation Thermal treatment device
CN213835455U (zh) 2020-11-16 2021-07-30 江苏华苏工业炉制造有限公司 一种具有温度调控的真空淬火炉
CN216107091U (zh) 2021-09-06 2022-03-22 法垄热工技术(上海)有限公司 一种新型模块化真空热处理产线
WO2023105846A1 (fr) * 2021-12-10 2023-06-15 Jfeスチール株式会社 Dispositif de production de bande d'acier, installation de recuit continu et procédé de production

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3484085A (en) * 1967-03-27 1969-12-16 Midland Ross Corp Drop bottom furnace and quench chamber
US20050104266A1 (en) * 2003-11-13 2005-05-19 Iq Technologies, Inc. Vacuum furnace with pressurized intensive water quench tank
CN2781304Y (zh) * 2005-01-17 2006-05-17 陈虞才 钕铁硼永磁体用多功能三室烧结炉

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011026653A (ja) * 2009-07-24 2011-02-10 Daido Steel Co Ltd 焼入装置
JP2012012637A (ja) * 2010-06-29 2012-01-19 Furutekku Kk 熱処理加工方法、熱処理加工物及び熱処理加工装置
US20130153547A1 (en) * 2010-07-02 2013-06-20 Kazuhiko Katsumata Multi-chamber heat treatment device
JP2016089251A (ja) * 2014-11-10 2016-05-23 中外炉工業株式会社 熱処理設備
CN104451044A (zh) * 2014-12-31 2015-03-25 湖南顶立科技有限公司 一种真空淬火方法
US20170254592A1 (en) * 2015-04-02 2017-09-07 Ihi Corporation Thermal treatment device
CN204874589U (zh) * 2015-06-03 2015-12-16 中山凯旋真空技术工程有限公司 高真空水淬固溶炉系统
CN213835455U (zh) 2020-11-16 2021-07-30 江苏华苏工业炉制造有限公司 一种具有温度调控的真空淬火炉
CN216107091U (zh) 2021-09-06 2022-03-22 法垄热工技术(上海)有限公司 一种新型模块化真空热处理产线
WO2023105846A1 (fr) * 2021-12-10 2023-06-15 Jfeスチール株式会社 Dispositif de production de bande d'acier, installation de recuit continu et procédé de production

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Publication number Publication date
PL448051A1 (pl) 2025-09-22

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