ES2023788T3 - Procedimiento para la preparacion de 1,4-diazabiciclo (2.2.2.)-octano, a partir de piperazina. - Google Patents

Procedimiento para la preparacion de 1,4-diazabiciclo (2.2.2.)-octano, a partir de piperazina.

Info

Publication number
ES2023788T3
ES2023788T3 ES198888113766T ES88113766T ES2023788T3 ES 2023788 T3 ES2023788 T3 ES 2023788T3 ES 198888113766 T ES198888113766 T ES 198888113766T ES 88113766 T ES88113766 T ES 88113766T ES 2023788 T3 ES2023788 T3 ES 2023788T3
Authority
ES
Spain
Prior art keywords
piperazine
preparation
diazabiciclo
octano
procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198888113766T
Other languages
English (en)
Other versions
ES2023788A4 (es
Inventor
Josef Dr. Disteldorf
Norbert Dr. Finke
Werner Dr. Hubel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huels AG
Original Assignee
Huels AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huels AG filed Critical Huels AG
Publication of ES2023788A4 publication Critical patent/ES2023788A4/es
Application granted granted Critical
Publication of ES2023788T3 publication Critical patent/ES2023788T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/08—Bridged systems

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

EL OBJETO DE LA PRESENTE PATENTE ES LA PRODUCCION DE 1,4-DIAZABICICLO(2,2,2)-OCTANO (TEDA) PARTIENDO DE PRODUCTOS CICLICOS. SE ENCONTRO SORPRENDENTEMENTE QUE LA PIPERACINA A TEMPERATURAAS ELEVADAS REACCIONA EN PRESENCIA DE ZEOLITAS PARA CONVERTIRSE EN TEDA Y QUE, DE ESTA FORMA, TAMBIEN SE PUEDEN TRASPONER A TEDA, CON UN ALTO GRADO DE SELECTIVIDAD, MEZCLAS DE AMBOS COMPONENTES QUE SON TECNICAMENTE DIFICILES DE SEPARAR. TEDA ENCUENTRA APLICACION SOBRE TODO COMO CATALIZADOR PARA LA OBTENCION DE POLIURETANOS.
ES198888113766T 1987-10-17 1988-08-24 Procedimiento para la preparacion de 1,4-diazabiciclo (2.2.2.)-octano, a partir de piperazina. Expired - Lifetime ES2023788T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19873735214 DE3735214A1 (de) 1987-10-17 1987-10-17 Verfahren zur herstellung von 1,4-diazabicyclo(2.2.2)-octan aus piperazin

Publications (2)

Publication Number Publication Date
ES2023788A4 ES2023788A4 (es) 1992-02-16
ES2023788T3 true ES2023788T3 (es) 1993-07-16

Family

ID=6338555

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198888113766T Expired - Lifetime ES2023788T3 (es) 1987-10-17 1988-08-24 Procedimiento para la preparacion de 1,4-diazabiciclo (2.2.2.)-octano, a partir de piperazina.

Country Status (5)

Country Link
EP (1) EP0312734B1 (es)
JP (1) JPH01132587A (es)
AT (1) ATE71098T1 (es)
DE (2) DE3735214A1 (es)
ES (1) ES2023788T3 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5120860A (en) * 1987-12-18 1992-06-09 Union Carbide Chemicals & Plastics Technology Corporation Process for the production of aziridines
DE3823160A1 (de) * 1988-07-08 1990-01-11 Basf Ag Verfahren zur herstellung von 1,4-diazabicyclo-2,2,2-octanen
DE3903622A1 (de) * 1989-02-08 1990-08-09 Basf Ag Verfahren zur herstellung von 1,4-diazabicyclo-2,2,2-octan
DE3934459A1 (de) * 1989-10-14 1991-04-18 Bayer Ag Verfahren zur herstellung von triethylendiamin und piperazin
US5162531A (en) * 1990-09-20 1992-11-10 Union Carbide Chemicals & Plastics Technology Corporation Mixed metal oxide catalytic process for the preparation of triethylenediamines
US5731449A (en) * 1996-09-23 1998-03-24 Air Products And Chemicals, Inc. Triethylendiamine synthesis with base-treated zeolites as catalysts
US5756741A (en) * 1996-11-15 1998-05-26 Air Products And Chemicals, Inc. Process for the production of triethylenediamine
US5741906A (en) * 1996-11-15 1998-04-21 Air Products And Chemicals, Inc. Production of triethylenediamine using surface acidity deactivated zeolite catalysts
US6084096A (en) * 1998-04-09 2000-07-04 Air Products And Chemicals, Inc. Triethylenediamine and piperazine synthesis using zeolite catalysts modified with a silicon-containing compound
DE19930736C2 (de) 1999-07-05 2001-07-05 Performance Chemicals Handels Verfahren zur Herstellung von Triethylendiamin unter Einsatz von Ethylendiamin
DE10061863A1 (de) 2000-12-12 2002-06-13 Basf Ag Verfahren zur Herstellung von Triethylendiamin (TEDA)
DE10132499A1 (de) * 2001-07-05 2003-01-23 Basf Ag Verfahren zur selektiven Synthese von Triethylendiamin
CN108997356B (zh) * 2018-07-18 2021-08-20 西安近代化学研究所 一种催化乙撑亚胺与2-甲基哌嗪合成2-甲基三乙烯二胺的方法
CN108912120B (zh) * 2018-07-18 2021-01-05 西安近代化学研究所 一种三乙烯二胺联产n-氨乙基哌嗪的制备方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3772293A (en) * 1971-12-13 1973-11-13 Air Prod & Chem Single step synthesis of trietylene diamine
US4582904A (en) * 1982-05-24 1986-04-15 Air Products And Chemicals, Inc. Amine production via condensation reactions using rare earth metal hydrogen phosphates as catalysts
EP0158319A3 (en) * 1984-04-10 1988-05-25 Union Carbide Corporation Synthesis of 1-azabicyclo(2.2.2) octanes or 1,4-diazabicyclo(2-2.2)octanes

Also Published As

Publication number Publication date
EP0312734A1 (de) 1989-04-26
ES2023788A4 (es) 1992-02-16
EP0312734B1 (de) 1992-01-02
ATE71098T1 (de) 1992-01-15
JPH01132587A (ja) 1989-05-25
DE3867417D1 (de) 1992-02-13
DE3735214A1 (de) 1989-04-27

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