ES2030058T3 - Procedimiento de adsorcion con oscilacion de presion para producir una corriente de gas enriquecido. - Google Patents

Procedimiento de adsorcion con oscilacion de presion para producir una corriente de gas enriquecido.

Info

Publication number
ES2030058T3
ES2030058T3 ES198787302493T ES87302493T ES2030058T3 ES 2030058 T3 ES2030058 T3 ES 2030058T3 ES 198787302493 T ES198787302493 T ES 198787302493T ES 87302493 T ES87302493 T ES 87302493T ES 2030058 T3 ES2030058 T3 ES 2030058T3
Authority
ES
Spain
Prior art keywords
adsorption zone
adsorption
column
zone
pressure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198787302493T
Other languages
English (en)
Inventor
Toan P. Vo
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Calgon Carbon Corp
Original Assignee
Calgon Carbon Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Calgon Carbon Corp filed Critical Calgon Carbon Corp
Application granted granted Critical
Publication of ES2030058T3 publication Critical patent/ES2030058T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0476—Vacuum pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/104—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/116—Molecular sieves other than zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25—Coated, impregnated or composite adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/12—Oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/102—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40001—Methods relating to additional, e.g. intermediate, treatment of process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028—Depressurization
    • B01D2259/4003—Depressurization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B01D2259/40037—Equalization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40043—Purging
    • B01D2259/4005—Nature of purge gas
    • B01D2259/40052—Recycled product or process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40043—Purging
    • B01D2259/4005—Nature of purge gas
    • B01D2259/40056—Gases other than recycled product or process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40064—Five
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/402—Further details for adsorption processes and devices using two beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/414—Further details for adsorption processes and devices using different types of adsorbents
    • B01D2259/4141—Further details for adsorption processes and devices using different types of adsorbents within a single bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26—Drying gases or vapours
    • B01D53/261—Drying gases or vapours by adsorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • External Artificial Organs (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

PROCESO PARA LA PRODUCCION DE UNA CORRIENTE CONTINUA DE GAS ENRIQUECIDO EN UNA PRIMERA Y UNA SEGUNDA ZONAS DE ADSORCION QUE CONSTA DE LAS SIGUIENTES FASES: A) PASAR SERIAL Y CONCURRENTEMENTE UNA MEZCLA GASEOSA CONTENIENDO EL GAS A ENRIQUECER A TRAVES DE UNA PRIMERA ZONA DE ADSORCION CON UNA COLUMNA DE ADSORCION PRIMARIA Y UNA COLUMNA AUXILIAR BAJO PRESION PARA PRODUCIR UNA CORRIENTE DE GAS ENRIQUECIDO; B) HACER DISCONTINUO EL FLUJO DE MEZCLA GASEOSA IGUALANDO LA PRESION EN LA PRIMERA ZONA DE ADSORCION CON LA PRESION EN LA COLUMNA PRIMARIA DE LA SEGUNDA ZONA, IGUALANDO SIMULTANEAMENTE (I) LA COLUMNA AUXILIAR DESDE SU SALIDA A LA SALIDA DE LA COLUMNA PRIMARIA DE LA SEGUNDA ZONA DE ADSORCION, E IGUALANDO SIMULTANEAMENTE DESDE LA ADMISION DE LA COLUMNA PRIMARIA DE LA PRIMERA ZONA DE ADSORCION A LA ADMISION DE LA COLUMNA PRIMARIA DE LA SEGUNDA ZONA DE ADSORCION, Y (II) PRESIONIZANDO LA COLUMNA AUXILIAR DE LA SEGUNDA ZONA DE ADSORCION A LA MISMA PRESION DE LA COLUMNA PRIMARIA DE LA SEGUNDA ZONADE ADSORCION; C) PURGAR LA PRIMERA ZONA DE ADSORCION EN CONTRAPOSICION A LA PRESION ATMOSFERICA; D) PURGAR LA PRIMERA ZONA DE ADSORCION; E) AL MISMO TIEMPO QUE LOS PASOS C) Y D), PRESIONIZAR LA SEGUNDA ZONA DE ADSORCION CON UNA MEZCLA DE GAS A LA PRESION DE ADSORCION Y PRODUCIR GAS ENRIQUECIDO EN LA SALIDA DE DICHA SEGUNDA ZONA DE ADSORCION; F) PRESIONIZAR LA COLUMNA AUXILIAR DE LA PRIMERA ZONA CON GAS ENRIQUECIDO E IGUALAR LA COLUMNA PRIMARIA DE LA PRIMERA ZONA DE ADSORCION CON LA PRESION DE LA SEGUNDA ZONA, Y REPETIR LOS PASOS A) A E).
ES198787302493T 1986-04-04 1987-03-23 Procedimiento de adsorcion con oscilacion de presion para producir una corriente de gas enriquecido. Expired - Lifetime ES2030058T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/848,309 US4715867A (en) 1986-04-04 1986-04-04 Auxiliary bed pressure swing adsorption molecular sieve

Publications (1)

Publication Number Publication Date
ES2030058T3 true ES2030058T3 (es) 1992-10-16

Family

ID=25302939

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198787302493T Expired - Lifetime ES2030058T3 (es) 1986-04-04 1987-03-23 Procedimiento de adsorcion con oscilacion de presion para producir una corriente de gas enriquecido.

Country Status (7)

Country Link
US (1) US4715867A (es)
EP (1) EP0248510B1 (es)
JP (1) JPH01104325A (es)
AT (1) ATE72769T1 (es)
CA (1) CA1305435C (es)
DE (1) DE3776815D1 (es)
ES (1) ES2030058T3 (es)

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GB8718129D0 (en) * 1987-07-30 1987-09-03 Boc Group Plc Separation of gas mixtures
JP2562326B2 (ja) * 1987-08-07 1996-12-11 住友精化株式会社 空気から高濃度酸素を取得する方法
JPH04502581A (ja) * 1989-10-27 1992-05-14 ポール・コーポレーション 気体からの成分を収着する装置および方法
DE3941487C1 (es) * 1989-12-15 1991-04-25 Bergwerksverband Gmbh, 4300 Essen, De
US5090973A (en) * 1990-10-23 1992-02-25 The Boc Group, Inc. Psa employing high purity purging
JPH05221A (ja) * 1991-06-24 1993-01-08 Kanebo Ltd 混合気体の分離装置
US5403385A (en) * 1994-02-08 1995-04-04 Alberta Research Council Serial flow pressure swing adsorption process for gas separation
US5738709A (en) * 1996-12-20 1998-04-14 Air Products And Chemicals, Inc. Nitrogen PSA with intermediate pressure transfer
US5900532A (en) * 1997-02-20 1999-05-04 Nippon Sanso Corporation Method of removing siloxanes from silicon compound gases and apparatus therefor
CA2433156A1 (en) * 2000-12-26 2002-07-04 Sumitomo Seika Chemicals Co., Ltd. Method and device for separating object gas
US6751958B1 (en) 2001-09-06 2004-06-22 Honeywell International Inc. Physical chemistry compression
SE523278C2 (sv) * 2001-10-11 2004-04-06 Ifoe Ceramics Ab Förfarande och anordning för framställning av syre eller syreberikad luft
KR100488411B1 (ko) * 2003-07-16 2005-05-11 엘지전자 주식회사 기체 분리 장치
JP4898194B2 (ja) 2005-11-14 2012-03-14 大陽日酸株式会社 圧力変動吸着式ガス分離方法及び分離装置
US7491261B2 (en) * 2005-06-27 2009-02-17 Wearair Oxygen, Inc. Process and apparatus for generating and delivering an enriched gas fraction
US7722698B2 (en) 2008-02-21 2010-05-25 Delphi Technologies, Inc. Method of determining the purity of oxygen present in an oxygen-enriched gas produced from an oxygen delivery system
US8075676B2 (en) * 2008-02-22 2011-12-13 Oxus America, Inc. Damping apparatus for scroll compressors for oxygen-generating systems
US20090212962A1 (en) * 2008-02-22 2009-08-27 Delphi Technologies, Inc. Oxygen Generating System with Self-Contained Electronic Diagnostics and Fault-Tolerant Operation
US8343259B2 (en) * 2010-03-29 2013-01-01 Wearair Oxygen, Inc. Moisture mitigation in PSA air fractionation
KR101559902B1 (ko) * 2013-08-12 2015-10-14 (주)세프라텍 흡착성 투과 폴리머 중공사막을 이용한 가스 흡탈착 분리 시스템
FR3017804B1 (fr) * 2014-02-24 2018-01-26 Nitrocraft Dispositif de purification avec colonnes d'adsorption en serie
JP6325437B2 (ja) * 2014-12-26 2018-05-16 株式会社クラレ 窒素ガス分離方法および窒素ガス分離装置
JP6290114B2 (ja) * 2015-01-29 2018-03-07 株式会社アドバン理研 ガス製造装置およびガス製造処理方法
CN107281895B (zh) * 2016-04-01 2020-03-17 四川天采科技有限责任公司 一种吡咯烷精制脱水的全温程变压吸附方法
JP6595639B2 (ja) * 2018-02-07 2019-10-23 株式会社アドバン理研 ガス製造装置
EP3885027A4 (en) * 2018-11-19 2022-08-31 Sumitomo Seika Chemicals Co., Ltd. GAS SEPARATION DEVICE AND GAS SEPARATION PROCESS
CN111989149A (zh) * 2020-04-14 2020-11-24 成都盈辰科技有限公司 一种移动式变压吸附氧气生产装置的方法
US11717784B1 (en) 2020-11-10 2023-08-08 Solid State Separation Holdings, LLC Natural gas adsorptive separation system and method
CN113041782B (zh) * 2021-03-15 2021-12-17 西南化工研究设计院有限公司 一种气体变压吸附分离提纯系统及其分离提纯方法
WO2025093617A1 (en) * 2023-10-31 2025-05-08 Gases Research Innovation And Technology, S.L. Process for separating multicomponent gas mixtures without off-gas

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Also Published As

Publication number Publication date
JPH01104325A (ja) 1989-04-21
EP0248510B1 (en) 1992-02-26
US4715867A (en) 1987-12-29
JPH0257972B2 (es) 1990-12-06
CA1305435C (en) 1992-07-21
EP0248510A2 (en) 1987-12-09
ATE72769T1 (de) 1992-03-15
EP0248510A3 (en) 1988-06-01
DE3776815D1 (de) 1992-04-02

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