ES2031132T3 - Procedimiento. - Google Patents

Procedimiento.

Info

Publication number
ES2031132T3
ES2031132T3 ES198787306805T ES87306805T ES2031132T3 ES 2031132 T3 ES2031132 T3 ES 2031132T3 ES 198787306805 T ES198787306805 T ES 198787306805T ES 87306805 T ES87306805 T ES 87306805T ES 2031132 T3 ES2031132 T3 ES 2031132T3
Authority
ES
Spain
Prior art keywords
alkyl alcohol
secondary esterification
esterification zone
maleate
zone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198787306805T
Other languages
English (en)
Inventor
John Wilson Kippax
Colin Rathmell
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Johnson Matthey Davy Technologies Ltd
Original Assignee
Davy Mckee London Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Davy Mckee London Ltd filed Critical Davy Mckee London Ltd
Application granted granted Critical
Publication of ES2031132T3 publication Critical patent/ES2031132T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/593—Dicarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/60—Maleic acid esters; Fumaric acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/62—Halogen-containing esters
    • C07C69/65—Halogen-containing esters of unsaturated acids
    • C07C69/657—Maleic acid esters; Fumaric acid esters; Halomaleic acid esters; Halofumaric acid esters
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/02—Laboratory distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/13—Spirits

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Glass Compositions (AREA)
  • Iron Core Of Rotating Electric Machines (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fittings On The Vehicle Exterior For Carrying Loads, And Devices For Holding Or Mounting Articles (AREA)
  • Toys (AREA)

Abstract

PROCEDIMIENTO PARA LA PRODUCCION DE UN MALEATO DE DIALQUILO POR REACCION DE UN ANHIDRIDO MALEICO CON UN ALCOHOL ALIFATICO EN UNA ZONA DE MONOESTERIFICACION PARA FORMAR MALEATO DE MONOALQUILO, SEGUIDA DE LA REACCION DE ESTE CON MAS ALCOHOL PARA FORMAR MALEATO DE DIALQUILO. EL PROCEDIMIENTO INCLUYE LAS ETAPAS DE SUMINISTRAR UNA PRIMERA APORTACION DE LIQUIDO QUE CONTIENE MALEATO DE MONOALQUILO A UNA ZONA DE ESTERIFICACION SECUNDARIA QUE CONTIENE UNA CARGA DE UN CATALIZADOR DE ESTERIFICACION SOLIDO, SUMINISTRAR UNA SEGUNDA APORTACION QUE CONTIENE ALCOHOL ALIFATICO A LA ZONA DE ESTERIFICACION SECUNDARIA, MANTENIENDO ESTA A UNA TEMPERATURA SUFICIENTEMENTE ELEVADA PARA FORMAR O MANNTENER EN ELLA UNA CORRIENTE DE VAPOR QUE CONTIENEN EL ALCOHOL, PONER EN INTIMI CONTACTO LA PRIMERA APORTACION DE LIQUIDO EN LA ZONA DE ESTERIFICACION SECUNDARIA EN PRESENCIA DEL CATALIZADOR CON LA CORRIENTE DE ALIMENTACION DE VAPOR, RECUPERAR DE LA ZONA DE ESTERIFICACION SECUNDARIA UNA CORRIENTE EFLUENTE DE VAPOR, QUECONTIENE ADEMAS DE VAPOR DE ALCOHOL, AGUA EN FORMA DE VAPOR PRODUCIDO EN LA ZONA DE ESTERIFICACION SECUNDARIA POR LA ESTERIFICACION DEL MALEATO DE MONOALQUILO CON EL ALCOHOL, Y RECUPERAR DE DICHA ZONA UNA CORRIENTE DE PRODUCTO LIQUIDO QUE CONTIENE EL AMLEATO DE DIALQUILO.
ES198787306805T 1986-08-01 1987-07-31 Procedimiento. Expired - Lifetime ES2031132T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB868618888A GB8618888D0 (en) 1986-08-01 1986-08-01 Process

Publications (1)

Publication Number Publication Date
ES2031132T3 true ES2031132T3 (es) 1992-12-01

Family

ID=10602120

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198787306805T Expired - Lifetime ES2031132T3 (es) 1986-08-01 1987-07-31 Procedimiento.

Country Status (15)

Country Link
US (1) US4795824A (es)
EP (1) EP0255399B1 (es)
JP (1) JPH0813784B2 (es)
KR (2) KR950013081Y1 (es)
CN (1) CN1025329C (es)
AT (1) ATE73441T1 (es)
AU (1) AU592464B2 (es)
CA (1) CA1294630C (es)
DE (1) DE3777275D1 (es)
ES (1) ES2031132T3 (es)
GB (1) GB8618888D0 (es)
GR (1) GR3004365T3 (es)
IN (1) IN170126B (es)
MX (1) MX168898B (es)
NZ (1) NZ221286A (es)

Families Citing this family (44)

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US4740272A (en) * 1987-03-31 1988-04-26 Davy Mckee (London) Limited Separation of monoalkyl maleate from dialkyl maleate
BR9007037A (pt) * 1989-01-17 1991-10-22 Davy Mckee London Processo para a producao de alcoois graxos
JP2921977B2 (ja) * 1989-01-17 1999-07-19 デイヴイ・プロセス・テクノロジー・リミテッド プロセス及び装置
AT400033B (de) * 1992-03-10 1995-09-25 Biochemie Gmbh Neues verfahren zur isolierung und reinigung von clavulansäure und zur herstellung von pharmakologisch verträglichen salzen derselben
DE4423355A1 (de) * 1994-07-04 1996-01-11 Bayer Ag Verfahren zur Herstellung von Maleinsäuredialkylestern
AT403375B (de) * 1995-11-15 1998-01-26 Biochemie Gmbh Verfahren zur fällung von alkalisalzen der clavulansäure
TW366335B (en) * 1996-03-29 1999-08-11 Kvaerner Process Tech Ltd Process for the purification of butane-1,4-diol
ZA973972B (en) * 1996-05-14 1998-03-23 Kvaerner Process Tech Ltd A process for the production of at least one C4 compound selected from butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran.
GB9724004D0 (en) 1997-11-13 1998-10-21 Kvaerner Process Tech Ltd Process
ES2158645T3 (es) 1998-03-23 2001-09-01 Basf Ag Procedimiento para la preparacion de 1,4-butanodiol, butirolactona y tetrahidrofurano.
EP1108702A1 (en) * 1999-12-13 2001-06-20 Kvaerner Process Technology Limited Process for the co-production of aliphatic diols and cyclic ethers
US6355817B1 (en) 2000-07-15 2002-03-12 Exxonmobil Chemical Patents Inc. Optimized catalyst addition to enhance esterification catalyst performance
GB0117090D0 (en) * 2001-07-12 2001-09-05 Kvaerner Process Tech Ltd Process
US7435336B2 (en) 2002-10-10 2008-10-14 China Petroleum & Chenical Corporation Process for carrying out gas-liquid countercurrent processing
GB0325530D0 (en) * 2003-10-31 2003-12-03 Davy Process Techn Ltd Process
GB0421928D0 (en) * 2004-10-01 2004-11-03 Davy Process Techn Ltd Process
JP2007153814A (ja) * 2005-12-06 2007-06-21 Mitsubishi Chemicals Corp ジカルボン酸ジエステルの製造方法
WO2008062433A2 (en) * 2006-08-22 2008-05-29 Dorf Ketal Chemicals (I) Private Limited Method of removal of calcium from hydrocarbon feedstock
CN101314564A (zh) * 2007-06-01 2008-12-03 上海焦化有限公司 马来酸二甲酯的制备方法
BRPI0905734B1 (pt) * 2008-01-24 2017-11-14 Dorf Ketal Chemicals I Method for removal of metals from raw materials using carboxylic acid esters
JP5093354B2 (ja) 2008-09-11 2012-12-12 トヨタ自動車株式会社 ディスクブレーキ装置
US8901344B2 (en) * 2008-12-16 2014-12-02 Basf Se Production of carboxylic acid esters by stripping with alcohol vapor
WO2012038242A1 (de) 2010-09-24 2012-03-29 Basf Se Verfahren zur gewinnung von tetrahydrofuran
US9186599B2 (en) 2010-09-24 2015-11-17 Basf Se Process for isolating tetrahydrofuran
US10226748B2 (en) * 2011-06-27 2019-03-12 Rachel Burton Reactor system
GB201115617D0 (en) 2011-09-09 2011-10-26 Davy Process Techn Ltd Proacess
CN103360253B (zh) * 2012-04-01 2015-07-15 中国石油化工股份有限公司 生产马来酸二甲酯的方法
CN103360252B (zh) * 2012-04-01 2015-04-08 中国石油化工股份有限公司 马来酸二甲酯的生产方法
GB201216653D0 (en) * 2012-09-18 2012-10-31 Davy Process Techn Ltd Process
FR3012139B1 (fr) 2013-10-18 2016-08-26 Arkema France Unite d'esterification pour la production de methacrylate de methyle brut, procede d'esterification utilisant ladite unite et installation comprenant ladite unite
GB201321611D0 (en) 2013-12-06 2014-01-22 Johnson Matthey Davy Technologies Ltd Process
GB201321627D0 (en) 2013-12-06 2014-01-22 Johnson Matthey Davy Technologies Ltd Process
GB201507234D0 (en) 2015-04-28 2015-06-10 Johnson Matthey Davy Technologies Ltd Process
CN106187683B (zh) * 2016-07-05 2018-07-24 中石化上海工程有限公司 1，4-丁二醇的生产方法
CN106083523B (zh) * 2016-07-05 2018-07-27 中石化上海工程有限公司 生产1，4-丁二醇的方法
KR102151747B1 (ko) * 2018-11-23 2020-09-03 지에스칼텍스 주식회사 알킬 카르복실산 에스테르의 제조 방법 및 알킬 카르복실산 에스테르의 제조 장치
CN111848394A (zh) * 2020-07-22 2020-10-30 深圳飞扬兴业科技有限公司 一种马来酸二元醇单叔丁醚双酯的合成方法及其应用
CN112961058B (zh) * 2021-02-08 2022-05-10 宁波窦氏化学科技有限公司 一种制备马来酸二醇酯的工艺方法
CN114181038B (zh) 2021-12-24 2022-10-11 常州瑞华化工工程技术股份有限公司 一种顺酐直接加氢生产1,4-丁二醇并联产丁二酸酐的方法
GB202203264D0 (en) 2022-03-09 2022-04-20 Johnson Matthey Davy Technologies Ltd Process for producing a refined 1,4-butanediol stream
CN114933531A (zh) * 2022-06-07 2022-08-23 中建安装集团有限公司 一种悬浮催化精馏制备顺丁烯二酸二甲酯的方法及装置
GB202302059D0 (en) 2023-02-14 2023-03-29 Johnson Matthey Davy Technologies Ltd Process for producing dialkyl succinate
CN116178150A (zh) * 2023-03-13 2023-05-30 深圳飞扬骏研新材料股份有限公司 一种连续生产低反式含量马来酸二乙酯的方法
CN116272736B (zh) * 2023-03-25 2026-01-16 深圳飞扬骏研新材料股份有限公司 一种马来酸二乙酯的连续生产方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2230226C3 (de) * 1972-06-21 1975-11-20 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung von Dicarbonsäurediestern unter weitgehender Abwasserreinigung
US3862147A (en) * 1972-08-25 1975-01-21 Petro Tex Chem Corp Maleic anhydride process
US4032458A (en) * 1975-08-08 1977-06-28 Petro-Tex Chemical Corporation Production of 1,4-butanediol
US4314947A (en) * 1978-12-21 1982-02-09 Basf Aktiengesellschaft Process for completing the esterification of carboxylic acids with alcohols
ZA816748B (en) * 1980-10-01 1982-10-27 Hoechst Ag Process for the preparation of an ethyl ester
DE3106819A1 (de) * 1981-02-24 1982-09-09 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von 1,4-butandiol
GB8331793D0 (en) * 1983-11-29 1984-01-04 Davy Mckee Ltd Process
DE3346134A1 (de) * 1983-12-21 1985-07-04 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen abscheidung von maleinsaeureanhydrid aus gasfoermigen reaktionsgemischen

Also Published As

Publication number Publication date
CA1294630C (en) 1992-01-21
EP0255399A2 (en) 1988-02-03
AU7638887A (en) 1988-02-04
IN170126B (es) 1992-02-15
MX168898B (es) 1993-06-14
ATE73441T1 (de) 1992-03-15
DE3777275D1 (de) 1992-04-16
EP0255399B1 (en) 1992-03-11
JPS6399039A (ja) 1988-04-30
AU592464B2 (en) 1990-01-11
US4795824A (en) 1989-01-03
GR3004365T3 (es) 1993-03-31
KR880002797A (ko) 1988-05-11
KR880022642U (ko) 1988-12-27
CN1025329C (zh) 1994-07-06
KR950013081Y1 (en) 1995-10-24
EP0255399A3 (en) 1988-12-14
NZ221286A (en) 1989-08-29
GB8618888D0 (en) 1986-09-10
CN87105388A (zh) 1988-03-09
JPH0813784B2 (ja) 1996-02-14

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