ES2032564T3 - Peliculas de polietileno de alta densidad (hdpe) con orientacion biaxial diferenciada. - Google Patents

Peliculas de polietileno de alta densidad (hdpe) con orientacion biaxial diferenciada.

Info

Publication number
ES2032564T3
ES2032564T3 ES198888308746T ES88308746T ES2032564T3 ES 2032564 T3 ES2032564 T3 ES 2032564T3 ES 198888308746 T ES198888308746 T ES 198888308746T ES 88308746 T ES88308746 T ES 88308746T ES 2032564 T3 ES2032564 T3 ES 2032564T3
Authority
ES
Spain
Prior art keywords
films
high density
density polyethylene
hdpe
differentiated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198888308746T
Other languages
English (en)
Inventor
Pang-Chia Lu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mobil Oil AS
Original Assignee
Mobil Oil AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mobil Oil AS filed Critical Mobil Oil AS
Application granted granted Critical
Publication of ES2032564T3 publication Critical patent/ES2032564T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/32—Layered products comprising a layer of synthetic resin comprising polyolefins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C55/00—Shaping by stretching, e.g. drawing through a die; Apparatus therefor
    • B29C55/02—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets
    • B29C55/023—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets using multilayered plates or sheets
    • B29C55/026—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets using multilayered plates or sheets of preformed plates or sheets coated with a solution, a dispersion or a melt of thermoplastic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C55/00—Shaping by stretching, e.g. drawing through a die; Apparatus therefor
    • B29C55/02—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets
    • B29C55/10—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets multiaxial
    • B29C55/12—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets multiaxial biaxial
    • B29C55/14—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets multiaxial biaxial successively
    • B29C55/143—Shaping by stretching, e.g. drawing through a die; Apparatus therefor of plates or sheets multiaxial biaxial successively firstly parallel to the direction of feed and then transversely thereto
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00—Layered products comprising a layer of synthetic resin
    • B32B27/30—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • B32B27/306—Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising vinyl acetate or vinyl alcohol (co)polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/04—Homopolymers or copolymers of ethene
    • C08L23/06—Polyethylene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2023/00—Use of polyalkenes or derivatives thereof as moulding material
    • B29K2023/04—Polymers of ethylene
    • B29K2023/06—PE, i.e. polyethylene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2995/00—Properties of moulding materials, reinforcements, fillers, preformed parts or moulds
    • B29K2995/0037—Other properties
    • B29K2995/0065—Permeability to gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2270/00—Resin or rubber layer containing a blend of at least two different polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
    • B32B2307/30—Properties of the layers or laminate having particular thermal properties
    • B32B2307/31—Heat sealable
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
    • B32B2307/50—Properties of the layers or laminate having particular mechanical properties
    • B32B2307/514—Oriented
    • B32B2307/518—Oriented bi-axially
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2323/00—Polyalkenes
    • B32B2323/04—Polyethylene
    • B32B2323/043—HDPE, i.e. high density polyethylene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2439/00—Containers; Receptacles
    • B32B2439/70—Food packaging
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2323/04—Homopolymers or copolymers of ethene
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31855—Of addition polymer from unsaturated monomers
    • Y10T428/31909—Next to second addition polymer from unsaturated monomers
    • Y10T428/31913—Monoolefin polymer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Laminated Bodies (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)
  • Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
  • Wrappers (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

PELICULAS DE POLIETILENO DE ALTA DENSIDAD, CONTENIENDO PREFERIBLEMENTE MEZCLAS DE RESINAS HDPE O CERA MICROCRISTALINA SE ORIENTAN PARA UNA RELACION DE DEFORMACION SOBRE 2 EN LA DIRECCION DE LA MAQUINA, Y SOBRE 6 O MAS EN LA DIRECCION TRANSVERSAL PARA DAR PELICULAS QUE TENGAN UNAS BUENAS CARACTERISTICAS DE PLEGADO Y CARACTERISTICAS DE TRANSMISION DE VAPOR DE AGUA HACIENDOLAS A ESTAS MUY CONVENIENTES PARA CUANDO SE RECUBREN CON UNA CAPA HERMETICA AL CALOR POR EJEMPLO UN IONOMERO.
ES198888308746T 1987-09-28 1988-09-21 Peliculas de polietileno de alta densidad (hdpe) con orientacion biaxial diferenciada. Expired - Lifetime ES2032564T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/101,894 US4870122A (en) 1987-09-28 1987-09-28 HdPE films with imbalanced biaxial orientation

Publications (1)

Publication Number Publication Date
ES2032564T3 true ES2032564T3 (es) 1993-02-16

Family

ID=22287034

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198888308746T Expired - Lifetime ES2032564T3 (es) 1987-09-28 1988-09-21 Peliculas de polietileno de alta densidad (hdpe) con orientacion biaxial diferenciada.

Country Status (12)

Country Link
US (1) US4870122A (es)
EP (1) EP0310290B1 (es)
JP (1) JP2573672B2 (es)
KR (1) KR960015092B1 (es)
CN (1) CN1014899B (es)
AT (1) ATE77398T1 (es)
AU (1) AU603702B2 (es)
CA (1) CA1312435C (es)
DE (1) DE3872140T2 (es)
ES (1) ES2032564T3 (es)
GR (1) GR3004943T3 (es)
PH (1) PH25026A (es)

Families Citing this family (55)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4880706A (en) * 1987-10-05 1989-11-14 Mobil Oil Corp. Biaxially oriented multilayer barrier films
JPH0759641B2 (ja) * 1987-12-28 1995-06-28 出光石油化学株式会社 ブテン−１重合体系フィルムおよびその積層フィルム
DE4041453A1 (de) * 1990-12-21 1992-06-25 Huels Troisdorf Formmasse und verfahren zum kalandrieren von folien auf basis von polyethylen
US5223346A (en) * 1991-10-23 1993-06-29 Mobil Oil Corporation Hdpe/polypropylene film laminates
US5194318A (en) * 1991-10-25 1993-03-16 Mobil Oil Corporation Multilayer film with metallized surface
US5302442A (en) * 1992-03-09 1994-04-12 Mobil Oil Corporation Heat sealable base films
US5346763A (en) * 1993-04-21 1994-09-13 Mobil Oil Corporation Multilayer film structure
WO1995006556A1 (en) * 1993-09-02 1995-03-09 Quantum Chemical Corporation Biaxially-oriented polypropylene film with improved gas barrier
ZA949549B (en) * 1993-12-01 1996-05-30 Mobil Oil Corp Oriented HDPE films with skin layers
US5725962A (en) * 1993-12-01 1998-03-10 Mobil Oil Corporation Oriented HDPE films with metallized skin layer
JPH09506050A (ja) * 1993-12-01 1997-06-17 モービル・オイル・コーポレーション スキン層を有する延伸ｈｄｐｅフィルム
US5500283A (en) * 1993-12-01 1996-03-19 Mobil Oil Corporation Coated hope film and its method of manufacture
US6495231B2 (en) 1994-06-27 2002-12-17 Exxonmobil Oil Corporation Epoxy coated multilayer structure for use in the production of security documents
US6294267B1 (en) 1994-06-27 2001-09-25 Exxonmobil Oil Corporation Core printed security documents
US5698333A (en) * 1994-06-27 1997-12-16 Mobil Oil Corporation Multilayer film structures for use in the production of banknotes or the like
US5935696A (en) * 1997-06-11 1999-08-10 Mobil Oil Corporation Multilayer film structures for use in the production of banknotes or the like
ZA955144B (en) * 1994-06-27 1996-12-23 Mobil Oil Corp Cross-laminated multilayer film structures for use in the production of banknotes or the like
US5879028A (en) * 1998-04-23 1999-03-09 Mobil Oil Corporation Weakened oriented high density polyethylene film for multilayer security document lamination
GB9416183D0 (en) * 1994-08-10 1994-09-28 Mobil Plastics Europ Inc Oriented HDPE laminates for easy direct onal opening and reclosable bags
US6419966B1 (en) * 1994-12-22 2002-07-16 Exxonmobil Chemical Patents Inc. Polyethylene articles with improved resistance to water vapor transmission
US20030199657A1 (en) * 1994-12-22 2003-10-23 Davis Donna Sue Polyethylene articles with improved resistance to water vapor transmission
US5527608A (en) * 1994-12-27 1996-06-18 Mobil Oil Corporation Oriented multilayer heat sealable packaging film capable of withstanding high altitude effects
US6764751B2 (en) 1996-10-03 2004-07-20 Exxonmobil Oil Corporation Coated multilayer polyethylene film
US5885721A (en) * 1996-10-03 1999-03-23 Mobil Oil Corporation Multilaminar high density polyethylene film with high biaxial orientation
US6689857B1 (en) * 1996-10-03 2004-02-10 Exxonmobil Oil Corporation High density polyethylene film with high biaxial orientation
US6017615A (en) * 1997-08-25 2000-01-25 Huntsman Polymers Corporation Film product comprising novel polyolefins
US6387529B1 (en) * 1997-12-24 2002-05-14 Exxon Mobil Oil Corporation Biaxially oriented HDPE multilayer film
US6228505B1 (en) * 1998-05-15 2001-05-08 Mobil Oil Corporation Medium density polyethylene film having unidirectional tear
US6168826B1 (en) 1998-12-23 2001-01-02 Mobil Oil Corporation Biaxially oriented polyethylene film with improved optics and sealability properties
US6391425B1 (en) 1999-03-30 2002-05-21 Exxonmobil Oil Corporation Polyolefin film with embossed surface
AU4818399A (en) * 1999-06-03 2000-12-28 Printpack Illinois, Inc. Machine direction oriented high molecular weight, high density polyethylene films with enhanced water vapor transmission properties
US6391411B1 (en) 1999-06-03 2002-05-21 Printpack Illinois, Inc. Machine direction oriented high molecular weight, high density polyethylene films with enhanced water vapor transmission properties
EP1214203B1 (en) 1999-08-04 2003-07-02 Applied Extrusion Technologies, Inc. Holographic transfer film
US6677029B2 (en) 1999-12-20 2004-01-13 Applied Extrusion Technologies, Inc. Holographic films
US6764752B2 (en) * 2000-07-13 2004-07-20 Toray Plastics (America), Inc. Biaxially oriented polypropylene metallized film for packaging
US6758000B2 (en) 2001-01-10 2004-07-06 Avery Dennison Corporation Livestock security tag assembly
US6756095B2 (en) 2001-01-10 2004-06-29 Avery Dennison Corporation Heat-sealable laminate
US6641914B2 (en) 2001-05-29 2003-11-04 Exxonmobil Oil Corporation HDPE label film
US6919113B2 (en) 2001-07-18 2005-07-19 Avery Dennison Corporation Multilayered film
US6773653B2 (en) 2001-10-05 2004-08-10 Avery Dennison Corporation In-mold labeling method
US6887923B2 (en) * 2002-12-11 2005-05-03 Equistar Chemicals, L.P. Processing aids for enhanced machine direction orientation rates and property enhancement of polyolefin films using hydrocarbon waxes
US8034461B2 (en) * 2005-02-09 2011-10-11 Equistar Chemicals, Lp Preparation of multilayer polyethylene thin films
KR101170703B1 (ko) 2005-12-29 2012-08-07 옴야 디벨로프먼트 아게 탄산칼슘 장벽 필름 및 그 용도
CA2594472A1 (en) * 2007-07-23 2009-01-23 Nova Chemicals Corporation Multilayer barrier film
CN102083624A (zh) * 2008-05-28 2011-06-01 比密斯公司 由乙烯乙酸乙烯共聚物制成的气密层
CA2688092C (en) * 2009-12-10 2016-07-12 Nova Chemicals Corporation Multilayer film structure
EP3272500B1 (en) * 2010-12-28 2019-06-26 Asahi Kasei Kabushiki Kaisha Polyolefin-based porous film
KR102883861B1 (ko) 2019-10-23 2025-11-11 노바 케미컬즈 (인터내셔널) 소시에테 아노님 2축 배향 mdpe 필름
US20210379866A1 (en) 2020-05-29 2021-12-09 Inteplast Group Corporation Laminated film
CA3102574A1 (en) 2020-06-29 2021-12-29 Nova Chemicals Corporation Ethylene copolymer for biaxial orientation
WO2022154053A1 (ja) * 2021-01-18 2022-07-21 藤森工業株式会社 積層体および包装袋
CN117320880A (zh) * 2021-04-19 2023-12-29 诺瓦化学品(国际)股份有限公司 双轴取向膜
CA3213023A1 (en) * 2021-04-19 2022-10-27 Nova Chemicals Corporation Biaxially oriented film
US20250026106A1 (en) * 2021-11-25 2025-01-23 Dow Global Technologies Llc Biaxially oriented polyolefin films
WO2024025675A1 (en) 2022-07-27 2024-02-01 Jindal Films Americas Llc Pressure-sensitive-adhesive release film for oriented hdpe

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GB849389A (en) * 1957-10-09 1960-09-28 Phillips Petroleum Co Blend of microcrystalline wax and olefin polymer and method for production thereof
US3179720A (en) * 1962-10-22 1965-04-20 Hercules Powder Co Ltd Polyethylene blends
US3340328A (en) * 1962-12-13 1967-09-05 Continental Oil Co Blends of polyethylenes having improved properties
US3998914A (en) * 1972-02-01 1976-12-21 Du Pont Of Canada Limited Film from a blend of high density polyethylene and a low density ethylene polymer
JPS4918140A (es) * 1972-06-09 1974-02-18
US3976612A (en) * 1972-11-30 1976-08-24 Idemitsu, Kosan Kabushiki-Kaisha (Idemitsu Kosan Co., Ltd.) Polyethylene composition
AU523866B2 (en) * 1978-04-18 1982-08-19 Du Pont Canada Inc. Manufacture of film
EP0111602B1 (en) * 1982-12-16 1986-05-14 Idemitsu Petrochemical Co. Ltd. Packaging bags

Also Published As

Publication number Publication date
GR3004943T3 (es) 1993-04-28
CN1014899B (zh) 1991-11-27
AU2280388A (en) 1989-04-06
EP0310290B1 (en) 1992-06-17
EP0310290A1 (en) 1989-04-05
CA1312435C (en) 1993-01-12
DE3872140T2 (de) 1992-12-03
DE3872140D1 (de) 1992-07-23
KR960015092B1 (ko) 1996-10-24
US4870122A (en) 1989-09-26
PH25026A (en) 1991-01-28
KR890005186A (ko) 1989-05-13
CN1032424A (zh) 1989-04-19
JP2573672B2 (ja) 1997-01-22
JPH01127316A (ja) 1989-05-19
AU603702B2 (en) 1990-11-22
ATE77398T1 (de) 1992-07-15

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