ES2042234T3 - Extraccion de productos naturales asistida por microondas. - Google Patents

Extraccion de productos naturales asistida por microondas.

Info

Publication number
ES2042234T3
ES2042234T3 ES199090401290T ES90401290T ES2042234T3 ES 2042234 T3 ES2042234 T3 ES 2042234T3 ES 199090401290 T ES199090401290 T ES 199090401290T ES 90401290 T ES90401290 T ES 90401290T ES 2042234 T3 ES2042234 T3 ES 2042234T3
Authority
ES
Spain
Prior art keywords
extraction
products
microwaves
natural products
solvents
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES199090401290T
Other languages
English (en)
Inventor
Jocelyn J.R. Pare
Michel Sigouin
Jacques Lapointe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Canada Minister of Environment
Original Assignee
Canada Minister of Environment
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Canada Minister of Environment filed Critical Canada Minister of Environment
Application granted granted Critical
Publication of ES2042234T3 publication Critical patent/ES2042234T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40Concentrating samples
    • G01N1/4055Concentrating samples by solubility techniques
    • G01N2001/4061Solvent extraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Fats And Perfumes (AREA)

Abstract

LA EXTRACCION DE PRODUCTOS NATURALES A PARTIR DE MATERIAL BIOLOGICO SE AUMENTA Y ACELERA CUANDO SE PONE EN CONTACTO CON UN EXTRACTANTE Y SE EXPONE SIMULTANEAMENTE A UNA RADIACION DE MICROONDAS. NORMALMENTE EL DISOLVENTE ELEGIDO ES TRANSPARENTE A LAS MICROONDAS Y PERMANECE A LA TEMPERATURA AMBIENTE; SIN EMBARGO, PUEDE NO SER MAS QUE PARCIALMENTE TRANSPARENTE SI ES TOLERABLE UN RECALENTAMIENTO. DEBE ESTAR PRESENTE UNA CANTIDAD SUFICIENTE DE DISOLVENTE PARA PERMITIR LA EXTRACCION APUNTADA. LOS PRODUCTOS DE LA EXTRACCION SE RECUPERAN POR PROCEDIMIENTOS NORMALS. LOS MATERIALES UTILIZADOS PARA LA EXTRACCION SON MENTA, UMBELIFERA ESCOCESA, FOLLAJE DE CEDRO Y AJO. LOS DISOLVENTES PUEDEN SER HEXANO, DICLOROMETANO O ETANOL. LAS EXTRACCIONES SE PUEDEN LLEVAR A CABO EN DOS ETAPAS O MAS CON DIFERENTES DISOLVENTES EN CADA ETAPA. CIERTOS PRODUCTOS DE EXTRACCION SON NUEVOS Y MUY DISTINTOS DE LOS PRODUCTOS OBTENIDOS POR ARRASTRE CON VAPOR.
ES199090401290T 1989-05-16 1990-05-15 Extraccion de productos naturales asistida por microondas. Expired - Lifetime ES2042234T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CA000600322A CA1336968C (en) 1989-05-16 1989-05-16 Microwave-assisted natural products extraction

Publications (1)

Publication Number Publication Date
ES2042234T3 true ES2042234T3 (es) 1993-12-01

Family

ID=4140083

Family Applications (1)

Application Number Title Priority Date Filing Date
ES199090401290T Expired - Lifetime ES2042234T3 (es) 1989-05-16 1990-05-15 Extraccion de productos naturales asistida por microondas.

Country Status (5)

Country Link
US (1) US5002784A (es)
EP (1) EP0398798B1 (es)
CA (1) CA1336968C (es)
ES (1) ES2042234T3 (es)
MA (1) MA21844A1 (es)

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DE69024961T2 (de) * 1990-11-16 1996-08-14 United Kingdom Government Mikrowellenaussonderung von flüchtigen Ölen und Vorrichtung dafür
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US5732476A (en) * 1992-02-10 1998-03-31 Pare; J.R. Jocelyn Microwave-assisted separations using volatiles, and apparatus therefor
US5884417A (en) * 1992-02-10 1999-03-23 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment Microwave-assisted separations using volatiles
US5519947A (en) * 1992-02-10 1996-05-28 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment Microwave-assisted generation of volatiles, of supercritical fluid, and apparatus therefor
US5675909A (en) * 1992-02-10 1997-10-14 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Environment Microwave-assisted separations using volatiles
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US5853726A (en) * 1992-09-16 1998-12-29 Chevereau; Pierre Method for extracting and fixing aromas on non-aqueous substrate, machine for implementing the method, and product thereby
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US7001629B1 (en) 1993-05-11 2006-02-21 Archimex Method and plant for solvent-free microwave extraction of natural products
FR2705035B1 (fr) * 1993-05-11 1995-08-04 Archimex Pibs Procédé et installation d'extraction sans solvant de produits naturels par micro-ondes.
FR2740991B1 (fr) * 1995-11-13 1998-05-22 Phybiotex Sa Nouveaux extraits de plantes, leur procede de fabrication et leur utilisation dans les produits cosmetiques
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US6061926A (en) * 1997-11-05 2000-05-16 Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment Controlled energy density microwave-assisted processes
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DE19838377C2 (de) * 1998-08-24 2000-10-26 Fiegert Seibt Edda Verfahren und Vorrichtung zur Extraktherstellung aus pflanzlichem Material
KR100388110B1 (ko) * 2000-05-04 2003-06-18 해태제과식품주식회사 효모 균주에서 아스타산틴 색소 추출방법 및 추출된 색소
KR100411364B1 (ko) * 2000-08-04 2003-12-18 해태제과식품주식회사 녹조류에서 아스타산틴 색소 추출방법 및 추출된 색소
AU2002226380B2 (en) * 2000-12-20 2006-10-12 Dsm Ip Assets B.V. Tissue treatment
US20070178219A1 (en) * 2002-09-19 2007-08-02 Eric Boudreaux Method for Reducing Acrylamide Formation
US7811618B2 (en) 2002-09-19 2010-10-12 Frito-Lay North America, Inc. Method for reducing asparagine in food products
US20050074538A1 (en) * 2002-09-19 2005-04-07 Elder Vincent Allen Method for reducing acrylamide formation in thermally processed foods
US7393550B2 (en) * 2003-02-21 2008-07-01 Frito-Lay North America, Inv. Method for reducing acrylamide formation in thermally processed foods
DE50300039D1 (de) * 2003-01-21 2004-09-02 Milestone Srl Lösungsmittelfreie Mikrowellen-Extraktion von flüchtigen Naturstoffen
US8110240B2 (en) 2003-02-21 2012-02-07 Frito-Lay North America, Inc. Method for reducing acrylamide formation in thermally processed foods
CA2472896A1 (en) * 2004-07-02 2006-01-02 Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Environment Microwave assisted processes and equipment therefore
US20060019002A1 (en) * 2004-07-26 2006-01-26 Harvest Food Co., Ltd. Method for processing, storing and transporting garlic
US20060159810A1 (en) * 2005-01-20 2006-07-20 Marialuci Almeida Method for producing a food product
CN100479899C (zh) * 2006-12-07 2009-04-22 华南理工大学 一种连续式微波固-液萃取装置
EP1955749B1 (en) * 2007-01-22 2010-03-17 Milestone S.r.l. Microwave hydrodiffusion for isolation of natural products
DE602007005342D1 (de) * 2007-01-22 2010-04-29 Milestone Srl Mikrowellenintegrierter Soxhlet-Aufsatz
JP5119397B2 (ja) * 2007-02-26 2013-01-16 国立大学法人徳島大学 スダチチンおよびノビレチンの製造方法
US8486684B2 (en) 2007-08-13 2013-07-16 Frito-Lay North America, Inc. Method for increasing asparaginase activity in a solution
CN101196446B (zh) * 2007-12-18 2010-05-19 天津市农业科学院中心实验室 微波萃取等离子体质谱法测定土壤中有效硼含量的方法
US8284248B2 (en) 2009-08-25 2012-10-09 Frito-Lay North America, Inc. Method for real time detection of defects in a food product
US8158175B2 (en) 2008-08-28 2012-04-17 Frito-Lay North America, Inc. Method for real time measurement of acrylamide in a food product
US9095145B2 (en) 2008-09-05 2015-08-04 Frito-Lay North America, Inc. Method and system for the direct injection of asparaginase into a food process
RU2370272C1 (ru) * 2008-11-25 2009-10-20 Государственное образовательное учреждение высшего профессионального образования "Красноярский государственный торгово-экономический институт" Способ получения биологически активного препарата из древесной зелени пихты сибирской
US9215886B2 (en) * 2008-12-05 2015-12-22 Frito-Lay North America, Inc. Method for making a low-acrylamide content snack with desired organoleptical properties
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US8282789B2 (en) * 2009-05-18 2012-10-09 Bing-Nan Lee Microwave apparatus and method of extracting essential oils, essence, and pigments with gas flow
US8282788B2 (en) * 2009-05-18 2012-10-09 Bing-Nan Lee Extraction apparatus and method of extracting essential oils, essence, and pigments from odorous raw material by microwave heating under sub-critical conditions
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US9421477B2 (en) * 2013-08-12 2016-08-23 Green Extraction Technologies Biomass fractionation and extraction apparatus
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FR3017308B1 (fr) 2014-02-10 2022-06-17 Idco Dispositif et procede d'extraction de produits biologiques par micro-ondes et ultrasons
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JP6962678B2 (ja) * 2016-10-27 2021-11-05 サッポロビール株式会社 ホップ抽出物含有飲料の製造方法、及び、ホップ抽出物含有飲料の香味向上方法
AU2017368264A1 (en) * 2016-12-01 2019-05-23 Natural Extraction Systems, LLC Rapid botanical oil distillation device utilizing microwave agent
MX2019006498A (es) 2016-12-05 2019-08-01 Sinnovatek Inc Sistema y metodo para la extraccion continua asistida por microondas de agentes bioactivos de la biomasa.
JP2020203958A (ja) * 2017-08-18 2020-12-24 ライオン株式会社 シソ科メンタ属植物由来の抽出物とその製造方法
WO2021159038A1 (en) 2020-02-07 2021-08-12 Natural Extraction Systems, LLC Methods to refine cannabinoids
US12420214B2 (en) 2018-08-10 2025-09-23 Natural Extraction Systems, LLC Methods to produce products comprising cannabinoids
US10669248B2 (en) 2018-08-10 2020-06-02 Natural Extraction Systems, LLC Methods to chemically modify cannabinoids
US10822320B2 (en) 2018-08-10 2020-11-03 Natural Extraction Systems, LLC Methods to purify cannabinoids
US12606535B2 (en) 2020-02-09 2026-04-21 Natural Extraction Systems, LLC Gas phase methods to extract natural products
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CN117680038B (zh) * 2024-02-04 2024-06-28 北京露华本草生物科技有限公司 一种基于微波加热的植物原露析取设备及其工艺

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DE3114593C1 (de) * 1981-04-10 1982-12-09 Fried. Krupp Gmbh, 4300 Essen Verfahren zur Gewinnung von Aroma- und Farbstoffen aus Paprika

Also Published As

Publication number Publication date
EP0398798A3 (en) 1990-12-27
EP0398798A2 (fr) 1990-11-22
US5002784A (en) 1991-03-26
CA1336968C (en) 1995-09-12
EP0398798B1 (fr) 1993-07-14
MA21844A1 (fr) 1990-12-31

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