ES2042234T3 - Extraccion de productos naturales asistida por microondas. - Google Patents
Extraccion de productos naturales asistida por microondas.Info
- Publication number
- ES2042234T3 ES2042234T3 ES199090401290T ES90401290T ES2042234T3 ES 2042234 T3 ES2042234 T3 ES 2042234T3 ES 199090401290 T ES199090401290 T ES 199090401290T ES 90401290 T ES90401290 T ES 90401290T ES 2042234 T3 ES2042234 T3 ES 2042234T3
- Authority
- ES
- Spain
- Prior art keywords
- extraction
- products
- microwaves
- natural products
- solvents
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000605 extraction Methods 0.000 title abstract 7
- 229930014626 natural product Natural products 0.000 title abstract 2
- 239000002904 solvent Substances 0.000 abstract 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 240000002234 Allium sativum Species 0.000 abstract 1
- 239000012620 biological material Substances 0.000 abstract 1
- 235000004611 garlic Nutrition 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000005855 radiation Effects 0.000 abstract 1
- 238000004326 stimulated echo acquisition mode for imaging Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N1/4055—Concentrating samples by solubility techniques
- G01N2001/4061—Solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Abstract
LA EXTRACCION DE PRODUCTOS NATURALES A PARTIR DE MATERIAL BIOLOGICO SE AUMENTA Y ACELERA CUANDO SE PONE EN CONTACTO CON UN EXTRACTANTE Y SE EXPONE SIMULTANEAMENTE A UNA RADIACION DE MICROONDAS. NORMALMENTE EL DISOLVENTE ELEGIDO ES TRANSPARENTE A LAS MICROONDAS Y PERMANECE A LA TEMPERATURA AMBIENTE; SIN EMBARGO, PUEDE NO SER MAS QUE PARCIALMENTE TRANSPARENTE SI ES TOLERABLE UN RECALENTAMIENTO. DEBE ESTAR PRESENTE UNA CANTIDAD SUFICIENTE DE DISOLVENTE PARA PERMITIR LA EXTRACCION APUNTADA. LOS PRODUCTOS DE LA EXTRACCION SE RECUPERAN POR PROCEDIMIENTOS NORMALS. LOS MATERIALES UTILIZADOS PARA LA EXTRACCION SON MENTA, UMBELIFERA ESCOCESA, FOLLAJE DE CEDRO Y AJO. LOS DISOLVENTES PUEDEN SER HEXANO, DICLOROMETANO O ETANOL. LAS EXTRACCIONES SE PUEDEN LLEVAR A CABO EN DOS ETAPAS O MAS CON DIFERENTES DISOLVENTES EN CADA ETAPA. CIERTOS PRODUCTOS DE EXTRACCION SON NUEVOS Y MUY DISTINTOS DE LOS PRODUCTOS OBTENIDOS POR ARRASTRE CON VAPOR.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA000600322A CA1336968C (en) | 1989-05-16 | 1989-05-16 | Microwave-assisted natural products extraction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2042234T3 true ES2042234T3 (es) | 1993-12-01 |
Family
ID=4140083
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES199090401290T Expired - Lifetime ES2042234T3 (es) | 1989-05-16 | 1990-05-15 | Extraccion de productos naturales asistida por microondas. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5002784A (es) |
| EP (1) | EP0398798B1 (es) |
| CA (1) | CA1336968C (es) |
| ES (1) | ES2042234T3 (es) |
| MA (1) | MA21844A1 (es) |
Families Citing this family (65)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE69024961T2 (de) * | 1990-11-16 | 1996-08-14 | United Kingdom Government | Mikrowellenaussonderung von flüchtigen Ölen und Vorrichtung dafür |
| CA2060931C (en) * | 1992-02-10 | 1996-12-17 | J. R. Jocelyn Pare | Microwave-assisted generation of volatiles, of supercritical fluid, and apparatus therefor |
| US5732476A (en) * | 1992-02-10 | 1998-03-31 | Pare; J.R. Jocelyn | Microwave-assisted separations using volatiles, and apparatus therefor |
| US5884417A (en) * | 1992-02-10 | 1999-03-23 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Microwave-assisted separations using volatiles |
| US5519947A (en) * | 1992-02-10 | 1996-05-28 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Microwave-assisted generation of volatiles, of supercritical fluid, and apparatus therefor |
| US5675909A (en) * | 1992-02-10 | 1997-10-14 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of Environment | Microwave-assisted separations using volatiles |
| DE4226811A1 (de) * | 1992-08-13 | 1994-02-17 | Sueddeutsche Kalkstickstoff | Verfahren zur Stabilisierung von Hopfenprodukten |
| US5853726A (en) * | 1992-09-16 | 1998-12-29 | Chevereau; Pierre | Method for extracting and fixing aromas on non-aqueous substrate, machine for implementing the method, and product thereby |
| FR2694300B1 (fr) * | 1992-09-16 | 1994-10-14 | Pierre Chevereau | Procédé d'extraction et de fixation d'arômes sur un substrat non aqueux, machine pour mettre en Óoeuvre le procédé et produit obtenu selon le procédé. |
| AT397464B (de) * | 1992-10-07 | 1994-04-25 | Koch Heinrich P Dr | Verfahren zur gewinnung eines therapeutischen pflanzenextraktes |
| US7001629B1 (en) | 1993-05-11 | 2006-02-21 | Archimex | Method and plant for solvent-free microwave extraction of natural products |
| FR2705035B1 (fr) * | 1993-05-11 | 1995-08-04 | Archimex Pibs | Procédé et installation d'extraction sans solvant de produits naturels par micro-ondes. |
| FR2740991B1 (fr) * | 1995-11-13 | 1998-05-22 | Phybiotex Sa | Nouveaux extraits de plantes, leur procede de fabrication et leur utilisation dans les produits cosmetiques |
| US5784682A (en) * | 1996-02-16 | 1998-07-21 | Birken; Stephen M. | System for separating constituents from a base material |
| US6061926A (en) * | 1997-11-05 | 2000-05-16 | Her Majesty The Queen In Right Of Canada, As Represented By The Minister Of The Environment | Controlled energy density microwave-assisted processes |
| US5891501A (en) * | 1997-11-25 | 1999-04-06 | Mckellip; Lewis L. | Method for extraction of essential oils from plant material |
| FR2772598B1 (fr) * | 1997-12-24 | 2000-01-21 | Gattefosse Ets Sa | Composition cosmetique ou dermopharmaceutique comprenant une base et au moins un element actif d'origine vegetale, procede de fabrication et utilisation |
| DE19838377C2 (de) * | 1998-08-24 | 2000-10-26 | Fiegert Seibt Edda | Verfahren und Vorrichtung zur Extraktherstellung aus pflanzlichem Material |
| KR100388110B1 (ko) * | 2000-05-04 | 2003-06-18 | 해태제과식품주식회사 | 효모 균주에서 아스타산틴 색소 추출방법 및 추출된 색소 |
| KR100411364B1 (ko) * | 2000-08-04 | 2003-12-18 | 해태제과식품주식회사 | 녹조류에서 아스타산틴 색소 추출방법 및 추출된 색소 |
| AU2002226380B2 (en) * | 2000-12-20 | 2006-10-12 | Dsm Ip Assets B.V. | Tissue treatment |
| US20070178219A1 (en) * | 2002-09-19 | 2007-08-02 | Eric Boudreaux | Method for Reducing Acrylamide Formation |
| US7811618B2 (en) | 2002-09-19 | 2010-10-12 | Frito-Lay North America, Inc. | Method for reducing asparagine in food products |
| US20050074538A1 (en) * | 2002-09-19 | 2005-04-07 | Elder Vincent Allen | Method for reducing acrylamide formation in thermally processed foods |
| US7393550B2 (en) * | 2003-02-21 | 2008-07-01 | Frito-Lay North America, Inv. | Method for reducing acrylamide formation in thermally processed foods |
| DE50300039D1 (de) * | 2003-01-21 | 2004-09-02 | Milestone Srl | Lösungsmittelfreie Mikrowellen-Extraktion von flüchtigen Naturstoffen |
| US8110240B2 (en) | 2003-02-21 | 2012-02-07 | Frito-Lay North America, Inc. | Method for reducing acrylamide formation in thermally processed foods |
| CA2472896A1 (en) * | 2004-07-02 | 2006-01-02 | Her Majesty The Queen In Right Of Canada As Represented By The Minister Of Environment | Microwave assisted processes and equipment therefore |
| US20060019002A1 (en) * | 2004-07-26 | 2006-01-26 | Harvest Food Co., Ltd. | Method for processing, storing and transporting garlic |
| US20060159810A1 (en) * | 2005-01-20 | 2006-07-20 | Marialuci Almeida | Method for producing a food product |
| CN100479899C (zh) * | 2006-12-07 | 2009-04-22 | 华南理工大学 | 一种连续式微波固-液萃取装置 |
| EP1955749B1 (en) * | 2007-01-22 | 2010-03-17 | Milestone S.r.l. | Microwave hydrodiffusion for isolation of natural products |
| DE602007005342D1 (de) * | 2007-01-22 | 2010-04-29 | Milestone Srl | Mikrowellenintegrierter Soxhlet-Aufsatz |
| JP5119397B2 (ja) * | 2007-02-26 | 2013-01-16 | 国立大学法人徳島大学 | スダチチンおよびノビレチンの製造方法 |
| US8486684B2 (en) | 2007-08-13 | 2013-07-16 | Frito-Lay North America, Inc. | Method for increasing asparaginase activity in a solution |
| CN101196446B (zh) * | 2007-12-18 | 2010-05-19 | 天津市农业科学院中心实验室 | 微波萃取等离子体质谱法测定土壤中有效硼含量的方法 |
| US8284248B2 (en) | 2009-08-25 | 2012-10-09 | Frito-Lay North America, Inc. | Method for real time detection of defects in a food product |
| US8158175B2 (en) | 2008-08-28 | 2012-04-17 | Frito-Lay North America, Inc. | Method for real time measurement of acrylamide in a food product |
| US9095145B2 (en) | 2008-09-05 | 2015-08-04 | Frito-Lay North America, Inc. | Method and system for the direct injection of asparaginase into a food process |
| RU2370272C1 (ru) * | 2008-11-25 | 2009-10-20 | Государственное образовательное учреждение высшего профессионального образования "Красноярский государственный торгово-экономический институт" | Способ получения биологически активного препарата из древесной зелени пихты сибирской |
| US9215886B2 (en) * | 2008-12-05 | 2015-12-22 | Frito-Lay North America, Inc. | Method for making a low-acrylamide content snack with desired organoleptical properties |
| FR2943684B1 (fr) * | 2009-03-30 | 2011-04-22 | Castera Anne Rossignol | Procede d'extraction de composes non volatils. |
| US8282789B2 (en) * | 2009-05-18 | 2012-10-09 | Bing-Nan Lee | Microwave apparatus and method of extracting essential oils, essence, and pigments with gas flow |
| US8282788B2 (en) * | 2009-05-18 | 2012-10-09 | Bing-Nan Lee | Extraction apparatus and method of extracting essential oils, essence, and pigments from odorous raw material by microwave heating under sub-critical conditions |
| US9839661B2 (en) * | 2010-05-11 | 2017-12-12 | Kemin Industries, Inc. | Plant material drying methods |
| WO2012051670A1 (en) | 2010-10-21 | 2012-04-26 | Byron Food Science Pty Limited | Method for preserving plant material |
| AU2013100380A4 (en) * | 2010-10-21 | 2013-05-02 | Botanical Food Company Pty Ltd | Preserved Plant Material |
| FR2986534B1 (fr) | 2012-02-07 | 2014-06-27 | Univ D'avignon Et Des Pays De Vaucluse | Procede d'enrichissement d'un corps gras en carotenoides |
| US9421477B2 (en) * | 2013-08-12 | 2016-08-23 | Green Extraction Technologies | Biomass fractionation and extraction apparatus |
| ES3034200T3 (en) | 2013-10-04 | 2025-08-13 | Natural Extraction Sys Llc | Method and apparatus for extracting botanical oils |
| FR3017308B1 (fr) | 2014-02-10 | 2022-06-17 | Idco | Dispositif et procede d'extraction de produits biologiques par micro-ondes et ultrasons |
| RO130896A0 (ro) * | 2015-01-19 | 2016-02-26 | Mariana Pătraşcu | Reactor continuu pentru extracţia asistată de microunde şi ultrasunete a compuşilor biologic activi din plante |
| CA2925827A1 (en) | 2016-04-05 | 2017-10-05 | Atlantic Cancer Research Institute | Microwave-assisted medical technologies and apparatus therfor |
| DE102016206677A1 (de) * | 2016-04-20 | 2017-10-26 | Gcr Global Commodity Resources Ug (Haftungsbeschränkt) | Verfahren zur Gewinnung ätherischer Öle und/oder von Bestandteilen ätherischer Öle aus feuchtem Extraktionsgut |
| JP6962678B2 (ja) * | 2016-10-27 | 2021-11-05 | サッポロビール株式会社 | ホップ抽出物含有飲料の製造方法、及び、ホップ抽出物含有飲料の香味向上方法 |
| AU2017368264A1 (en) * | 2016-12-01 | 2019-05-23 | Natural Extraction Systems, LLC | Rapid botanical oil distillation device utilizing microwave agent |
| MX2019006498A (es) | 2016-12-05 | 2019-08-01 | Sinnovatek Inc | Sistema y metodo para la extraccion continua asistida por microondas de agentes bioactivos de la biomasa. |
| JP2020203958A (ja) * | 2017-08-18 | 2020-12-24 | ライオン株式会社 | シソ科メンタ属植物由来の抽出物とその製造方法 |
| WO2021159038A1 (en) | 2020-02-07 | 2021-08-12 | Natural Extraction Systems, LLC | Methods to refine cannabinoids |
| US12420214B2 (en) | 2018-08-10 | 2025-09-23 | Natural Extraction Systems, LLC | Methods to produce products comprising cannabinoids |
| US10669248B2 (en) | 2018-08-10 | 2020-06-02 | Natural Extraction Systems, LLC | Methods to chemically modify cannabinoids |
| US10822320B2 (en) | 2018-08-10 | 2020-11-03 | Natural Extraction Systems, LLC | Methods to purify cannabinoids |
| US12606535B2 (en) | 2020-02-09 | 2026-04-21 | Natural Extraction Systems, LLC | Gas phase methods to extract natural products |
| CN112940862A (zh) * | 2021-01-28 | 2021-06-11 | 江西宗轩生物科技有限公司 | 玫瑰鲜花液分离浓缩工艺 |
| CN117680038B (zh) * | 2024-02-04 | 2024-06-28 | 北京露华本草生物科技有限公司 | 一种基于微波加热的植物原露析取设备及其工艺 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2925328A (en) * | 1955-09-07 | 1960-02-16 | Brev Alce Soc D Expl Des | Apparatus for extracting aromatic products such as essential oils, extracts and the like, from their natural supports |
| US3025220A (en) * | 1956-12-12 | 1962-03-13 | Kunz | Preparation of perfumes |
| FR1201108A (fr) * | 1958-08-04 | 1959-12-28 | Sibra | Procédé de préparation de dispersions stables d'anéthol dans l'eau et produits conformes à ceux obtenus |
| US3870053A (en) * | 1972-06-06 | 1975-03-11 | Brown & Williamson Tobacco Corp | Enhancement of flavor and aroma by microwave treatment |
| DD139342A1 (de) * | 1977-09-19 | 1979-12-27 | Gertraude Huebner | Verfahren zur herstellung von auszuegen,insbesondere fuer die spirituosenindustrie |
| DE3114593C1 (de) * | 1981-04-10 | 1982-12-09 | Fried. Krupp Gmbh, 4300 Essen | Verfahren zur Gewinnung von Aroma- und Farbstoffen aus Paprika |
-
1989
- 1989-05-16 CA CA000600322A patent/CA1336968C/en not_active Expired - Lifetime
-
1990
- 1990-05-07 US US07/519,588 patent/US5002784A/en not_active Expired - Lifetime
- 1990-05-14 MA MA22110A patent/MA21844A1/fr unknown
- 1990-05-15 ES ES199090401290T patent/ES2042234T3/es not_active Expired - Lifetime
- 1990-05-15 EP EP90401290A patent/EP0398798B1/fr not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0398798A3 (en) | 1990-12-27 |
| EP0398798A2 (fr) | 1990-11-22 |
| US5002784A (en) | 1991-03-26 |
| CA1336968C (en) | 1995-09-12 |
| EP0398798B1 (fr) | 1993-07-14 |
| MA21844A1 (fr) | 1990-12-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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