ES2044085T3 - Proceso para la fabricacion de fluoroaromaticos. - Google Patents
Proceso para la fabricacion de fluoroaromaticos.Info
- Publication number
- ES2044085T3 ES2044085T3 ES89301659T ES89301659T ES2044085T3 ES 2044085 T3 ES2044085 T3 ES 2044085T3 ES 89301659 T ES89301659 T ES 89301659T ES 89301659 T ES89301659 T ES 89301659T ES 2044085 T3 ES2044085 T3 ES 2044085T3
- Authority
- ES
- Spain
- Prior art keywords
- resulting
- reaction
- agent
- added
- zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000006243 chemical reaction Methods 0.000 abstract 4
- 150000004982 aromatic amines Chemical class 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000012954 diazonium Substances 0.000 abstract 1
- 238000006193 diazotization reaction Methods 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-O diazynium Chemical compound [NH+]#N IJGRMHOSHXDMSA-UHFFFAOYSA-O 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B39/00—Halogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCESO QUE COMPRENDE EL AÑADIR A UNA AMINA AROMATICA EN PRSENCIA DE HF PARA UNA ZONA DE REACCION SIMULTANEMANTE CON UN AGENTE DIAZOLIZANTE ASI COMO PARA EFECTUAR LA DIAZOTIZACION DE LA AMINA AROMATICA, DESCOMPOSICION TERMICA DE LA SAL DE DIAZONIUM RESULTANTE SUSTANCIALMENTE SEGUN ESTA SE FORMA, Y ELIMINACION DEL COMPUESTO FLUOROAROMATICO RESULTANTE DE LA ZONA DE REACCION SUSTANCIALMENTE SEGUN SE FORMA. LA AMINA Y EL AGENTE DIATOMIZANTE SE AÑADEN A LA ZONA DE REACCION EN TALES CANTIDADES Y PROPORCIONAN SUSTANCIALMENTE SEGUN SE AÑADEN Y NO SE FORMEN CONCENTRACIONES SUSTANCIALES DE AGUA EN LA ZONA DE REACCION.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US16102488A | 1988-02-26 | 1988-02-26 | |
| US07/263,952 US4912268A (en) | 1988-02-26 | 1988-10-21 | Process for manufacture of fluoroaromatics |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2044085T3 true ES2044085T3 (es) | 1994-01-01 |
Family
ID=26857437
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES89301659T Expired - Lifetime ES2044085T3 (es) | 1988-02-26 | 1989-02-21 | Proceso para la fabricacion de fluoroaromaticos. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4912268A (es) |
| EP (1) | EP0330420B1 (es) |
| JP (1) | JPH01261339A (es) |
| DE (1) | DE68902658T2 (es) |
| ES (1) | ES2044085T3 (es) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3909486A1 (de) * | 1989-03-22 | 1990-09-27 | Basf Ag | Verfahren zur herstellung von aliphatisch substituierten fluorbenzolen |
| US5107046A (en) * | 1990-05-23 | 1992-04-21 | Mallinckrodt Specialty Chemicals Co., Inc. | Process for preparing aromatic fluorides |
| US5410125A (en) * | 1990-10-11 | 1995-04-25 | Harry Winston, S.A. | Methods for producing indicia on diamonds |
| DE69420029D1 (de) * | 1993-02-24 | 1999-09-16 | Du Pont | Verfahren zur herstellung von fluoroaromatischen verbindungen |
| DE10003320C2 (de) * | 2000-01-27 | 2002-04-11 | Bayer Ag | Verfahren zur Herstellung von 2,3,5,6-Tetrahalogen-xylylidenverbindungen |
| US9126905B2 (en) * | 2012-07-18 | 2015-09-08 | Basf Se | Process for manufacturing fluoroaromatics |
| CN108569948B (zh) * | 2017-03-09 | 2021-06-04 | 辽宁天予化工有限公司 | 一种2-氯-4-氟甲苯的制备方法 |
| CN112624896A (zh) * | 2020-12-18 | 2021-04-09 | 浙江解氏新材料股份有限公司 | 一种基于微通道反应器的间二氟苯的连续化合成方法 |
| CN113563156A (zh) * | 2021-07-28 | 2021-10-29 | 浙江解氏新材料股份有限公司 | 一种基于蜂窝填料的2-氯-4氟甲苯的合成方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE600706C (de) * | 1933-03-24 | 1934-07-30 | I G Farbenindustrie Akt Ges | Verfahren zur Herstellung aromatischer, im Kern fluorierter Verbindungen |
| US2563796A (en) * | 1948-05-26 | 1951-08-07 | Harshaw Chem Corp | Manufacture of aromatic diazonium fluorides and corresponding aromatic fluorides |
| US3160623A (en) * | 1960-12-23 | 1964-12-08 | Manufacture of aryl diazonium | |
| US3573214A (en) * | 1966-09-12 | 1971-03-30 | Merck & Co Inc | Process for preparing stable dimethyl sulfoxide-hydrogen fluoride mixture |
| US3471512A (en) * | 1966-09-12 | 1969-10-07 | Merck & Co Inc | Preparation of aminophenyl-nitroimidazoles |
| US3471511A (en) * | 1966-09-12 | 1969-10-07 | Merck & Co Inc | Preparation of 2-(fluorophenyl)-4(5)-nitroimidazoles |
| FR2084591A5 (en) * | 1970-03-20 | 1971-12-17 | Olin Corp | Meta-fluoroanilines from meta-aminoacetanilides |
| US3798228A (en) * | 1970-04-13 | 1974-03-19 | Olin Corp | Method for the preparation of difluoropyridines |
| US3950444A (en) * | 1973-03-05 | 1976-04-13 | Olin Corporation | Process for preparing ortho substituted aryl fluorides |
| US4075252A (en) * | 1975-10-31 | 1978-02-21 | Olin Corporation | Diazotization-fluorination in a medium of hydrogen fluoride-containing ammonium ions |
| US4096196A (en) * | 1975-10-31 | 1978-06-20 | Olin Corporation | Diazotization-fluorination in a medium of hydrogen fluoride containing tertiary amine compounds |
| US4145364A (en) * | 1977-11-30 | 1979-03-20 | Merck & Co., Inc. | Preparation of fluorinated anilines |
| DE3141659A1 (de) * | 1981-10-21 | 1983-05-05 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von in o-stellung substituierten fluoraromaten |
| US4423260A (en) * | 1982-01-27 | 1983-12-27 | The United States Of America As Represented By The Secretary Of The Air Force | Method for introducing fluorine into an aromatic ring |
| JPH08133074A (ja) * | 1994-11-04 | 1996-05-28 | Mitsubishi Heavy Ind Ltd | 空気取入れ装置 |
-
1988
- 1988-10-21 US US07/263,952 patent/US4912268A/en not_active Expired - Fee Related
-
1989
- 1989-02-21 EP EP89301659A patent/EP0330420B1/en not_active Expired
- 1989-02-21 ES ES89301659T patent/ES2044085T3/es not_active Expired - Lifetime
- 1989-02-21 DE DE8989301659T patent/DE68902658T2/de not_active Expired - Fee Related
- 1989-02-23 JP JP1045020A patent/JPH01261339A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| JPH01261339A (ja) | 1989-10-18 |
| DE68902658T2 (de) | 1993-02-04 |
| EP0330420B1 (en) | 1992-09-02 |
| DE68902658D1 (de) | 1992-10-08 |
| EP0330420A1 (en) | 1989-08-30 |
| US4912268A (en) | 1990-03-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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