ES2047961T4 - Procedimiento para la fabricacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina. - Google Patents

Procedimiento para la fabricacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina.

Info

Publication number
ES2047961T4
ES2047961T4 ES91104288T ES91104288T ES2047961T4 ES 2047961 T4 ES2047961 T4 ES 2047961T4 ES 91104288 T ES91104288 T ES 91104288T ES 91104288 T ES91104288 T ES 91104288T ES 2047961 T4 ES2047961 T4 ES 2047961T4
Authority
ES
Spain
Prior art keywords
procedure
ciclohexilamina
trimetil
aminometil
manufacture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES91104288T
Other languages
English (en)
Other versions
ES2047961T3 (es
Inventor
Franz Dr Merger
Claus-Ulrich Dr Priester
Tom Dr Witzel
Gerhard Dr Koppenhoefer
Wolfgang Dr Harder
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2047961T3 publication Critical patent/ES2047961T3/es
Publication of ES2047961T4 publication Critical patent/ES2047961T4/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

LA INVENCION TRATA DE UN PROCEDIMIENTO: QUE SE UTILIZA PARA OBTENER A (A) Y CONSISTE EN; TRATAR AL 3-CIANO-3,5,5-TRIMETILCICLOHEXANONA CON AMONIACO EN EXCESO, EN PRESENCIA DE CATALIZADORES DE OXIDOS METALICOS ACIDOS, ENTRE 20 Y 150 C Y A UNA PRESION ENTRE 15 Y 500 BAR E HIDROGENAR AL PRODUCTO RESULTANTE CON HIDROGENO, EN PRESENCIA DE AMONIACO EN EXCESO Y DE CATALIZADORES METALICOS CONTENIENDO METALES NOBLES Y OTROS METALES COMO COBALTO, NIQUEL Y RUTENIO Y OTROS PORTADORES BASICOS Y NEUTROS, ENTRE 60 Y 150 C Y A UNA PRESENTE 50 Y 300 BAR. SIENDO A EL 3-AMINOMETILO-3,5,5 -TRIMETILO-CICLOHEXILAMINO.
ES91104288T 1990-03-30 1991-03-20 Procedimiento para la fabricacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina. Expired - Lifetime ES2047961T4 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4010227A DE4010227A1 (de) 1990-03-30 1990-03-30 Verfahren zur herstellung von 3-aminomethyl-3,5,5-trimethyl-cyclohexylamin

Publications (2)

Publication Number Publication Date
ES2047961T3 ES2047961T3 (es) 1994-03-01
ES2047961T4 true ES2047961T4 (es) 1995-09-16

Family

ID=6403401

Family Applications (1)

Application Number Title Priority Date Filing Date
ES91104288T Expired - Lifetime ES2047961T4 (es) 1990-03-30 1991-03-20 Procedimiento para la fabricacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina.

Country Status (6)

Country Link
US (1) US5371292A (es)
EP (1) EP0449089B1 (es)
JP (1) JP2965727B2 (es)
CA (1) CA2039328C (es)
DE (2) DE4010227A1 (es)
ES (1) ES2047961T4 (es)

Families Citing this family (47)

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Publication number Priority date Publication date Assignee Title
EP0482347B1 (de) * 1990-10-23 1993-06-09 Degussa Aktiengesellschaft Bis(3-cyano-3,5,5-trimethyl-cyclohexyliden)-azin, Verfahren zu seiner Herstellung und Weiterverarbeitung zu 3-(Aminomethyl)-3,5,5-trimethylcyclohexylamin
EP0534449A3 (en) * 1991-09-25 1993-06-02 Mitsubishi Kasei Corporation Process for the preparation of 3-aminomethyl-3,5,5-trialkylcyclohexylamine
US5406000A (en) * 1993-01-12 1995-04-11 Elf/Atochem North America, Inc. Process for the production of 3-aminomethyl-3,5,5-trialkylcyclohexylamine
CA2115025A1 (en) * 1993-02-08 1994-08-09 Atsushi Furutani Process for producing amines
CA2115024A1 (en) * 1993-04-27 1994-10-28 Atsushi Furutani Process for producing amines
DE4426472A1 (de) * 1993-07-27 1995-02-02 Du Pont Herstellung von Isophorondiamin
DE4343890A1 (de) * 1993-12-22 1995-06-29 Degussa Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE4343891A1 (de) * 1993-12-22 1995-06-29 Degussa Verfahren zur Beeinflussung des cis-/trans-Isomerenverhältnisses von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin bei dessen Herstellung aus 3-Cyano-3,5,5-trimethylcyclohexanon
DE4407325B4 (de) * 1994-03-04 2006-06-29 Basf Ag Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE19507398C1 (de) * 1995-03-03 1996-09-12 Basf Ag Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE19540191C1 (de) * 1995-10-30 1996-11-21 Degussa Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin, unter Verwendung eines Festbett-Hydrierkatalysators auf der Basis von Kobalt nach Raney
DE19627265A1 (de) * 1996-07-06 1998-01-08 Degussa Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Oxoverbindungen
DE19709260A1 (de) * 1997-03-06 1998-09-10 Basf Ag Verfahren zur Herstellung von 4-Amino-2,2,6,6-tetramethyl-piperidin
DE19747913C1 (de) * 1997-10-30 1999-02-11 Degussa Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Iminen oder Nitrilen, insbesondere zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin (Isophorondiamin) aus 3-Cyano-3,5,5-trimethylcyclohexanimin (Isophoronnitril-imin) durch Hydrierung in Gegenwart eines quaternären Ammoniumhydroxids
DE19756400A1 (de) * 1997-12-18 1999-06-24 Basf Ag Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin mit einem cic/trans-Isomerenverhältnis von mindestens 70/30
DE19933611A1 (de) 1999-07-17 2001-01-18 Aventis Res & Tech Gmbh & Co Verfahren zur Herstellung von Aminen durch homogen katalysierte reduktive Aminierung von Carbonylverbindungen
DE10065030A1 (de) 2000-12-23 2002-07-04 Degussa Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE10142635A1 (de) * 2001-08-31 2003-03-20 Basf Ag Verfahren zur Herstellung von Isophorondiamin (IPDA, 3-Aminomethyl-3,5,5,-trimethylcyclohexylamin)
DE10145119A1 (de) * 2001-09-13 2003-04-03 Basf Ag Verfahren zur Herstellung von Aminen
DE502004005974D1 (de) 2003-09-10 2008-03-06 Basf Ag Verfahren zur herstellung von xylylendiamin durch kontinuierliche hydrierung von flüssigem phthalodinitril
TW200710069A (en) * 2005-06-30 2007-03-16 Dow Global Technologies Inc Process for the reductive amination of aldehydes and ketones via the formation of macrocyclic polyimine intermediates
JP4938802B2 (ja) * 2006-02-14 2012-05-23 ビーエーエスエフ ソシエタス・ヨーロピア モノエチレングリコール（ｍｅｇ）からのエチレンアミン及びエタノールアミンの製造方法
JP5124486B2 (ja) * 2006-02-14 2013-01-23 ビーエーエスエフ ソシエタス・ヨーロピア 触媒の存在でモノエチレングリコール及びアンモニアの水素化アミノ化によるエチレンアミン及びエタノールアミンの製造方法
ATE517078T1 (de) * 2006-03-10 2011-08-15 Basf Se Verfahren zur herstellung von benzophenoniminen
JP2010513396A (ja) 2006-12-22 2010-04-30 ビーエーエスエフ ソシエタス・ヨーロピア ３−シアノ−３，５，５−トリメチル−シクロヘキシルイミンの連続的な水素化法
DE102007011483A1 (de) 2007-03-07 2008-09-18 Evonik Degussa Gmbh Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
ATE551318T1 (de) 2008-05-13 2012-04-15 Basf Se Verfahren zur herstellung von n,n-substituierten- 1,3-propandiaminen
CN102105434A (zh) * 2008-07-25 2011-06-22 巴斯夫欧洲公司 3-氨基甲基-1-环己基胺及其生产方法
CN102105435B (zh) 2008-07-25 2014-07-23 巴斯夫欧洲公司 5-异丙基-3-氨基甲基-2-甲基-1-氨基环己烷(香芹酮二胺)及其制备方法
CN102203054B (zh) 2008-11-05 2014-07-30 巴斯夫欧洲公司 生产n，n-取代的3-氨基丙-1-醇的方法
JP5650121B2 (ja) 2008-11-11 2015-01-07 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 環状ジアミンの製造方法
DE102010038310A1 (de) 2010-07-23 2012-01-26 Evonik Degussa Gmbh Verfahren zur Herstellung von Diamino-dianhydro-dideoxy-hexitolen, besonders bevorzugt 2,5-Diamino-1,4:3,6-Dianhydro-2,5-Dideoxy-D-Hexitol
DE102010062603A1 (de) 2010-12-08 2012-06-14 Evonik Degussa Gmbh Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE102010062594B4 (de) 2010-12-08 2022-02-17 Evonik Operations Gmbh Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
US9139511B2 (en) 2011-03-22 2015-09-22 Basf Se Process for hydrogenating nitriles
HUE031021T2 (en) * 2011-03-22 2017-06-28 Basf Se Process for hydrogenation of nitriles
EP2688862A1 (de) 2011-03-22 2014-01-29 Basf Se Verfahren zur hydrierung von nitrilen
CN102924291B (zh) 2011-08-08 2014-08-06 万华化学集团股份有限公司 3-氨甲基-3,5,5-三甲基环己胺的制备方法
EP3186221B1 (de) * 2014-08-28 2022-02-23 Basf Se Verfahren zur herstellung von primären aminen unter verwendung eines kobalt-vollkontaktkatalysators
EP3050870B1 (de) 2015-01-30 2024-11-27 Evonik Operations GmbH Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
EP3075721A1 (de) 2015-03-30 2016-10-05 Evonik Degussa GmbH Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
EP3406589B1 (de) 2017-05-23 2020-04-08 Evonik Operations GmbH Verfahren zur herstellung von aminoverbindungen aus nitrilverbindungen
CN107857704B (zh) * 2017-11-21 2020-04-10 万华化学集团股份有限公司 一种制备3-氨甲基-3,5,5-三甲基环己胺的方法及用于该方法的催化剂
EP3660001A1 (de) * 2018-11-27 2020-06-03 Evonik Operations GmbH Verbessertes verfahren zur herstellung von triacetondiamin und dessen derivaten
EP4294787A1 (en) 2021-02-16 2023-12-27 Basf Se Method for manufacture of isophoronediamine
WO2024115263A1 (en) 2022-12-02 2024-06-06 Basf Se Method for manufacture of isophoronediamine
EP4549616A1 (en) 2023-10-31 2025-05-07 Basf Se Process for making amines from carbonyl compounds using hydrogen having low deuterium content produced with non-fossil energy

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US2583729A (en) * 1947-11-28 1952-01-29 Universal Oil Prod Co Separation of a schiff's base from the condensation product of a primary amine with a carbonyl compound
DE1229078B (de) * 1961-10-18 1966-11-24 Hibernia Chemie Ges Mit Beschr Verfahren zur Herstellung von 3-(Aminomethyl)-3, 5, 5-trimethylcyclohexylderivaten
JPS5371032A (en) * 1976-12-02 1978-06-24 Mitsubishi Gas Chem Co Inc Preparation of imino cpds.
DE3011656A1 (de) * 1980-03-26 1981-10-01 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von 3-aminomethyl-3-5-5-trimethyl-cyclohexylamin
DE3021955A1 (de) * 1980-06-12 1981-12-24 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung primaerer mono- und diamine aus oxoverbindungen
GB2100718B (en) * 1981-06-16 1985-04-03 Kodak Ltd Polyamine compounds and their use as curing agents for epoxy resins
US4806690A (en) * 1985-05-13 1989-02-21 The Dow Chemical Company Method of producing amines
BR9001892A (pt) * 1989-04-25 1991-07-30 Union Carbide Chem Plastic Processo para aminacao de uma alimentacao compreendendo composto organico e processo para ativar um catalisador de aminacao redutora

Also Published As

Publication number Publication date
CA2039328A1 (en) 1991-10-01
JPH04221350A (ja) 1992-08-11
JP2965727B2 (ja) 1999-10-18
DE59100830D1 (de) 1994-02-24
CA2039328C (en) 2001-11-20
EP0449089B1 (de) 1994-01-12
US5371292A (en) 1994-12-06
EP0449089A1 (de) 1991-10-02
ES2047961T3 (es) 1994-03-01
DE4010227A1 (de) 1991-10-02

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