ES206185A1 - UN PROCEDIMIENTO PARA LA FABRICACIoN DE COMPUESTOS ORGáNICOS NITROGENADOS. - Google Patents

UN PROCEDIMIENTO PARA LA FABRICACIoN DE COMPUESTOS ORGáNICOS NITROGENADOS.

Info

Publication number: ES206185A1
Authority: ES; Spain
Prior art keywords: distillation; hydroxides; alkali; nitrile; product
Prior art date: 1951-11-08
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

ES0206185A

Other languages

English (en)

Spanish (es)

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Distillers Co Yeast Ltd

Distillers Co Ltd

Original Assignee

Distillers Co Yeast Ltd

Distillers Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1951-11-08

Filing date

1952-11-07

Publication date

1952-12-16

1952-11-07 Application filed by Distillers Co Yeast Ltd, Distillers Co Ltd filed Critical Distillers Co Yeast Ltd

1952-12-16 Publication of ES206185A1 publication Critical patent/ES206185A1/es

Status Expired legal-status Critical Current

Links

150000002825 nitriles Chemical class 0.000 title abstract 8
238000004519 manufacturing process Methods 0.000 title 1
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 9
LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 abstract 8
239000003513 alkali Substances 0.000 abstract 6
238000004821 distillation Methods 0.000 abstract 6
239000000243 solution Substances 0.000 abstract 6
150000001299 aldehydes Chemical class 0.000 abstract 5
239000007795 chemical reaction product Substances 0.000 abstract 5
150000004679 hydroxides Chemical class 0.000 abstract 5
RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical class [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 abstract 4
239000012071 phase Substances 0.000 abstract 4
235000011121 sodium hydroxide Nutrition 0.000 abstract 4
239000007787 solid Substances 0.000 abstract 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
239000002253 acid Substances 0.000 abstract 3
229910001863 barium hydroxide Inorganic materials 0.000 abstract 3
239000003054 catalyst Substances 0.000 abstract 3
238000006243 chemical reaction Methods 0.000 abstract 3
150000001875 compounds Chemical class 0.000 abstract 3
239000007859 condensation product Substances 0.000 abstract 3
239000000203 mixture Substances 0.000 abstract 3
239000000047 product Substances 0.000 abstract 3
238000005201 scrubbing Methods 0.000 abstract 3
-1 -unsaturated aliphatic aldehydes Chemical class 0.000 abstract 2
HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 abstract 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract 2
XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 2
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 abstract 2
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 2
239000011575 calcium Substances 0.000 abstract 2
238000009833 condensation Methods 0.000 abstract 2
230000005494 condensation Effects 0.000 abstract 2
238000007701 flash-distillation Methods 0.000 abstract 2
239000007789 gas Substances 0.000 abstract 2
239000008246 gaseous mixture Substances 0.000 abstract 2
239000012535 impurity Substances 0.000 abstract 2
UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 2
239000000126 substance Substances 0.000 abstract 2
125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 abstract 1
MCIPQLOKVXSHTD-UHFFFAOYSA-N 3,3-diethoxyprop-1-ene Chemical compound CCOC(C=C)OCC MCIPQLOKVXSHTD-UHFFFAOYSA-N 0.000 abstract 1
WSGYTJNNHPZFKR-UHFFFAOYSA-N 3-hydroxypropanenitrile Chemical group OCCC#N WSGYTJNNHPZFKR-UHFFFAOYSA-N 0.000 abstract 1
ATVJXMYDOSMEPO-UHFFFAOYSA-N 3-prop-2-enoxyprop-1-ene Chemical compound C=CCOCC=C ATVJXMYDOSMEPO-UHFFFAOYSA-N 0.000 abstract 1
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 1
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical class [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
229910052783 alkali metal Inorganic materials 0.000 abstract 1
229910000272 alkali metal oxide Inorganic materials 0.000 abstract 1
150000001340 alkali metals Chemical class 0.000 abstract 1
229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 abstract 1
229910000287 alkaline earth metal oxide Inorganic materials 0.000 abstract 1
150000001342 alkaline earth metals Chemical class 0.000 abstract 1
229910021529 ammonia Inorganic materials 0.000 abstract 1
239000008346 aqueous phase Substances 0.000 abstract 1
239000007864 aqueous solution Substances 0.000 abstract 1
ZTQSAGDEMFDKMZ-UHFFFAOYSA-N butyric aldehyde Natural products CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 abstract 1
229910052791 calcium Inorganic materials 0.000 abstract 1
229910001861 calcium hydroxide Inorganic materials 0.000 abstract 1
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 abstract 1
239000000292 calcium oxide Substances 0.000 abstract 1
ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 abstract 1
150000004649 carbonic acid derivatives Chemical class 0.000 abstract 1
230000009194 climbing Effects 0.000 abstract 1
238000000354 decomposition reaction Methods 0.000 abstract 1
239000003085 diluting agent Substances 0.000 abstract 1
229910001882 dioxygen Inorganic materials 0.000 abstract 1
239000011790 ferrous sulphate Substances 0.000 abstract 1
235000003891 ferrous sulphate Nutrition 0.000 abstract 1
239000012467 final product Substances 0.000 abstract 1
AMIMRNSIRUDHCM-UHFFFAOYSA-N isobutyric aldehyde Natural products CC(C)C=O AMIMRNSIRUDHCM-UHFFFAOYSA-N 0.000 abstract 1
239000007788 liquid Substances 0.000 abstract 1
238000000034 method Methods 0.000 abstract 1
230000003647 oxidation Effects 0.000 abstract 1
238000007254 oxidation reaction Methods 0.000 abstract 1
235000011118 potassium hydroxide Nutrition 0.000 abstract 1
239000001294 propane Substances 0.000 abstract 1
NBBJYMSMWIIQGU-UHFFFAOYSA-N propionic aldehyde Natural products CCC=O NBBJYMSMWIIQGU-UHFFFAOYSA-N 0.000 abstract 1
239000000376 reactant Substances 0.000 abstract 1
239000011541 reaction mixture Substances 0.000 abstract 1
239000012047 saturated solution Substances 0.000 abstract 1
229910052708 sodium Inorganic materials 0.000 abstract 1
239000011734 sodium Substances 0.000 abstract 1
229910000029 sodium carbonate Inorganic materials 0.000 abstract 1
238000000638 solvent extraction Methods 0.000 abstract 1
238000001179 sorption measurement Methods 0.000 abstract 1
239000001117 sulphuric acid Substances 0.000 abstract 1
235000011149 sulphuric acid Nutrition 0.000 abstract 1
239000008096 xylene Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
- C07C253/26—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons containing carbon-to-carbon multiple bonds, e.g. unsaturated aldehydes

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

ES0206185A 1951-11-08 1952-11-07 UN PROCEDIMIENTO PARA LA FABRICACIoN DE COMPUESTOS ORGáNICOS NITROGENADOS. Expired ES206185A1 (es)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GB2620251A GB719635A (en)	1951-11-08	1951-11-08	Manufacture of substantially pure unsaturated nitriles

Publications (1)

Publication Number	Publication Date
ES206185A1 true ES206185A1 (es)	1952-12-16

Family

ID=10239950

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
ES0206185A Expired ES206185A1 (es)	1951-11-08	1952-11-07	UN PROCEDIMIENTO PARA LA FABRICACIoN DE COMPUESTOS ORGáNICOS NITROGENADOS.

Country Status (4)

Country	Link
AT (1)	AT180257B (de)
DE (1)	DE949053C (de)
ES (1)	ES206185A1 (de)
GB (1)	GB719635A (de)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1125911B (de) *	1957-10-10	1962-03-22	Distillers Co Yeast Ltd	Verfahren zur Gewinnung von reinem Acrylsaeurenitril aus einer verduennten waessrigen Acrylsaeurenitrilloesung
NL238154A (de) *	1958-04-16
IT625988A (de) *	1959-02-12
NL126011C (de) *	1959-02-14
BE587609A (de) *	1959-02-16
MX64564A (de) *	1959-02-24
US3043860A (en) *	1959-04-16	1962-07-10	Union Carbide Corp	Preparation of unsaturated nitriles
CA677475A (en) *	1962-12-08	1964-01-07	The Distillers Company Limited	Production of unsaturated aliphatic nitriles
NL253844A (de) *	1959-07-18
DE1212962B (de) *	1960-08-12	1966-03-24	Knapsack Ag	Verfahren zur Abtrennung und Gewinnung von Acrylsaeurenitril und Ammoniak aus gasfoermigen Gemischen durch Auswaschen
DE1229073B (de) *	1960-09-08	1966-11-24	Asahi Chemical Ind	Verfahren zur Wiedergewinnung von Selen als Selendioxyd aus jenes enthaltenden Reaktions-gasen
NL276444A (de) *	1961-03-29
US5866379A (en) *	1997-01-28	1999-02-02	Novus International	Enzymatic conversion of α-hydroxynitriles to the corresponding .alpha.

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2444589A (en) *	1945-08-10	1948-07-06	American Cyanamid Co	Purification of organic nitriles
US2570794A (en) *	1950-07-20	1951-10-09	Du Pont	Purification of organic nitriles

1951
- 1951-11-08 GB GB2620251A patent/GB719635A/en not_active Expired
1952
- 1952-11-04 DE DED13482A patent/DE949053C/de not_active Expired
- 1952-11-07 ES ES0206185A patent/ES206185A1/es not_active Expired
- 1952-11-07 AT AT180257D patent/AT180257B/de active

Also Published As

Publication number	Publication date
AT180257B (de)	1954-11-25
GB719635A (en)	1954-12-08
DE949053C (de)	1956-09-13

Publication	Publication Date	Title
ES206185A1 (es)	1952-12-16	UN PROCEDIMIENTO PARA LA FABRICACIoN DE COMPUESTOS ORGáNICOS NITROGENADOS.
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US3799940A (en)	1974-03-26	Process for producing aromatic aldehydes
US20080203355A1 (en)	2008-08-28	Method for Producing Salts of Hydrocyanic Acid
EP0079432B1 (de)	1984-10-24	Verfahren zur Herstellung von Methacrylsäure aus Isobutyraldehyd
US1996638A (en)	1935-04-02	Manufacture of olefine oxides
US1595299A (en)	1926-08-10	Manufacture of phenols
US2844630A (en)	1958-07-22	Nitrosation process
US3230260A (en)	1966-01-18	Process for the isolation of n,o-dimeth-ylhydroxylamine
US3296314A (en)	1967-01-03	Process for purifying methyl ether
SU138612A1 (ru)	1960-11-30	Способ получени 6-метил-гентадиен-3,5-она-2
US3979432A (en)	1976-09-07	Preparation of nitriles
KR890005062B1 (ko)	1989-12-09	헤미아세탈로부터 플루오랄 및 헥사플루오로아세톤의 순수한 히드레이트를 제조하는 방법
LYNN et al.	1961	Synthesis and Some Derivatives of 3-Butenenitrile
US2242485A (en)	1941-05-20	Production of alkylene oxides difficultly soluble in water
US3038941A (en)	1962-06-12	Process for preparing polyfluoroaldehydes
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US2405963A (en)	1946-08-20	Co-oxidation reaction
US2417685A (en)	1947-03-18	Separation of ethylene chlorohydrin from higher chlorohydrins