ES2061961T3 - Procedimiento integrado para la produccion de aminoacetonitrilos. - Google Patents
Procedimiento integrado para la produccion de aminoacetonitrilos.Info
- Publication number
- ES2061961T3 ES2061961T3 ES89250068T ES89250068T ES2061961T3 ES 2061961 T3 ES2061961 T3 ES 2061961T3 ES 89250068 T ES89250068 T ES 89250068T ES 89250068 T ES89250068 T ES 89250068T ES 2061961 T3 ES2061961 T3 ES 2061961T3
- Authority
- ES
- Spain
- Prior art keywords
- production
- formaldehyde
- reactor
- acetonitrils
- amino
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- -1 AMINO Chemical class 0.000 title 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 9
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 abstract 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- 239000006096 absorbing agent Substances 0.000 abstract 2
- 150000008361 aminoacetonitriles Chemical class 0.000 abstract 2
- 238000011084 recovery Methods 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
- C07C255/24—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the same saturated acyclic carbon skeleton
- C07C255/25—Aminoacetonitriles
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
Abstract
EL INVENTO SE REFIERE A LA PRODUCCION DE AMINOACETONITRILOS, Y MAS ESPECIFICAMENTE A UN PROCESO INTEGRADO EN EL CUAL UNA CORRIENTE DE UN PRODUCTO REACTOR NO PURIFICADO, EN CRUDO DE UN REACTOR DE CIANURO DE HIDROGENO JUNTO CON UNA CORRIENTE DE FORMALDEHIDO, OPCIONALMENTE, UNA CORRIENTE DE PRUDUCTO REACTOR IMPURIFICADO, CRUDO DE UN REACTOR DE PROCESO DE FORMALDEHIDO SE ALIMENTA DIRECTAMENTE A UN ABSORVEADOR REACTIVO Y SE LAVA CON UNA SOLUCION ACUOSA DE PH CONTROLADA PARA PRODUCIR AMINOACETONITRILOS EN ALTAS CANTIDADES. ESTE PROCESO ELIMINA LA RECUPERACION INTERMEDIA Y EL PROCESO DE PURIFICACION ASOCIADO CON EL PROCESO DE PRUDUCCION DE CIANURO DE HIDROGENO Y FORMALDEHIDO MEDIANTE LA INTEGRACION DE LA RECUPERACION Y EL PROCESO DE REACCION EN UN ABSORVENTE REACTIVO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/264,413 US4895971A (en) | 1988-10-31 | 1988-10-31 | Process for the production of iminodiacetonitrile |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2061961T3 true ES2061961T3 (es) | 1994-12-16 |
Family
ID=23005972
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES89250068T Expired - Lifetime ES2061961T3 (es) | 1988-10-31 | 1989-10-31 | Procedimiento integrado para la produccion de aminoacetonitrilos. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4895971A (es) |
| EP (1) | EP0367364B1 (es) |
| AT (1) | ATE101123T1 (es) |
| CA (1) | CA1340024C (es) |
| DE (1) | DE68912878T2 (es) |
| ES (1) | ES2061961T3 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5008428A (en) * | 1989-10-26 | 1991-04-16 | W. R. Grace & Co.-Conn. | Integrated process for the production of aminoacetonitriles |
| US5187301A (en) * | 1989-10-26 | 1993-02-16 | W. R. Grace & Co.-Conn. | Preparation of iminodiacetonitrile from glycolonitrile |
| US5616772A (en) * | 1995-06-06 | 1997-04-01 | Hampshire Chemical Corp. | Method of stabilizing nitriles |
| US5844111A (en) * | 1995-06-07 | 1998-12-01 | The Procter & Gamble Company | Method for purifying an inert gas while preparing lower alkyl esters |
| US5648483A (en) * | 1995-06-07 | 1997-07-15 | The Procter & Gamble Company | Continuous transesterification method for preparing polyol polyesters |
| AU2001264605C1 (en) * | 2000-05-15 | 2005-10-06 | Monsanto Technology Llc | Preparation of iminodiacetic acid compounds from monoethanolamine substrates |
| CN101627005A (zh) * | 2007-03-01 | 2010-01-13 | 巴斯夫欧洲公司 | 制备氨基腈的方法 |
| CN101622222A (zh) * | 2007-03-01 | 2010-01-06 | 巴斯夫欧洲公司 | 由未处理的aan制备亚乙基胺的方法 |
| US20110207873A1 (en) * | 2008-11-07 | 2011-08-25 | Huntsman Petrochemical Llc | Preparation of di(aminoacetonitrile)s |
| CN105017074B (zh) * | 2015-06-16 | 2017-10-03 | 重庆紫光化工股份有限公司 | 亚氨基二乙腈生产母液的处理回收方法及装置 |
| CN105001121B (zh) * | 2015-06-16 | 2017-09-22 | 重庆紫光化工股份有限公司 | 亚氨基二乙腈生产母液的资源化利用方法及装置 |
| CN113402407A (zh) * | 2021-06-16 | 2021-09-17 | 上海蓝科石化环保科技股份有限公司 | 一种羟基乙腈氨化反应装置及工艺 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE669808C (de) * | 1935-12-05 | 1939-01-04 | Bergwerksverband Zur Verwertun | Verfahren zur Herstellung von Aminonitrilen |
| US2608380A (en) * | 1947-12-03 | 1952-08-26 | Union Carbide & Carbon Corp | Shaft seal for low-temperature expansion engines |
| US2794044A (en) * | 1955-08-30 | 1957-05-28 | Du Pont | Synthesis of iminodiacetonitrile |
| NL243269A (es) * | 1958-09-12 | |||
| US3167580A (en) * | 1962-04-12 | 1965-01-26 | American Cyanamid Co | Process for the preparation of iminodiacetonitrile |
| US3337607A (en) * | 1965-01-25 | 1967-08-22 | Process for preparation of an amine nitrile | |
| US3984453A (en) * | 1966-04-26 | 1976-10-05 | Stauffer Chemical Company | Process for preparing nitrilotriacetonitrile |
| US3907858A (en) * | 1967-10-30 | 1975-09-23 | Stauffer Chemical Co | Process of manufacturing nitrilotriacetonitrile |
| US3862203A (en) * | 1967-12-18 | 1975-01-21 | Stauffer Chemical Co | Process of manufacturing nitrilotriacetonitrile |
| US3840581A (en) * | 1970-05-26 | 1974-10-08 | Knapsack Ag | Process for the manufacture of nitrilotriacetonitrile |
| US3950384A (en) * | 1970-05-26 | 1976-04-13 | Hoechst Aktiengesellschaft | Process for the manufacture of nitrilotriacetonitrile |
| US3959342A (en) * | 1970-08-24 | 1976-05-25 | Bethlehem Steel Corporation | Process for the preparation of nitrilotriacetonitrile (NTN) |
| US3925448A (en) * | 1970-09-30 | 1975-12-09 | Ethyl Corp | Process for producing nitrilotriacetonitrile |
| US3856844A (en) * | 1970-12-11 | 1974-12-24 | Ethyl Corp | Chemical process |
| US3714335A (en) * | 1971-01-29 | 1973-01-30 | Ethyl Corp | Process for producing hf and nitrilotriacetonitrile |
| US3864378A (en) * | 1973-02-05 | 1975-02-04 | Bethlehem Steel Corp | Process for preparing 2-hydroxyethyliminodiacetonitrile |
| US3988360A (en) * | 1973-11-15 | 1976-10-26 | W. R. Grace & Co. | Process for preparing iminodiacetonitrile |
| US3993681A (en) * | 1975-04-04 | 1976-11-23 | W. R. Grace & Co. | Process for preparing iminodiacetonitrile |
| DE2942437A1 (de) * | 1979-10-20 | 1981-04-23 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung von iminodiacetonitril |
| DE3029205A1 (de) * | 1980-08-01 | 1982-03-11 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aminonitrilen |
| EP0102935B1 (en) * | 1982-08-30 | 1986-02-26 | Monsanto Company | Process for producing nitrilotriacetonitrile |
| US4731465A (en) * | 1982-08-30 | 1988-03-15 | Monsanto Company | Process for producing nitrilotriacetonitrile |
| DE3362308D1 (en) * | 1982-08-30 | 1986-04-03 | Monsanto Co | Process for producing nitrilotriacetonitrile |
| DE3242193A1 (de) * | 1982-11-15 | 1984-05-17 | Basf Ag, 6700 Ludwigshafen | Neue (alpha)-iminodiacetonitrile und verfahren zu ihrer herstellung |
| US4485049A (en) * | 1983-01-03 | 1984-11-27 | Monsanto Company | Two-stage crystallization of nitrilotriacetonitrile from a hot solution |
| DE3443462A1 (de) * | 1984-11-29 | 1986-05-28 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von umsetzungsprodukten des cyanwasserstoffs |
| US4661614A (en) * | 1986-03-06 | 1987-04-28 | Monsanto Company | Process for the preparation of iminodiacetonitrile |
-
1988
- 1988-10-31 US US07/264,413 patent/US4895971A/en not_active Expired - Lifetime
-
1989
- 1989-03-02 CA CA000592580A patent/CA1340024C/en not_active Expired - Fee Related
- 1989-10-31 AT AT89250068T patent/ATE101123T1/de not_active IP Right Cessation
- 1989-10-31 EP EP89250068A patent/EP0367364B1/en not_active Expired - Lifetime
- 1989-10-31 ES ES89250068T patent/ES2061961T3/es not_active Expired - Lifetime
- 1989-10-31 DE DE68912878T patent/DE68912878T2/de not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US4895971A (en) | 1990-01-23 |
| EP0367364B1 (en) | 1994-02-02 |
| DE68912878D1 (de) | 1994-03-17 |
| CA1340024C (en) | 1998-09-01 |
| DE68912878T2 (de) | 1994-05-19 |
| ATE101123T1 (de) | 1994-02-15 |
| EP0367364A1 (en) | 1990-05-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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