ES2067954T3 - Procedimiento para la obtencion de esferas de oxido de aluminio. - Google Patents

Procedimiento para la obtencion de esferas de oxido de aluminio.

Info

Publication number
ES2067954T3
ES2067954T3 ES91918749T ES91918749T ES2067954T3 ES 2067954 T3 ES2067954 T3 ES 2067954T3 ES 91918749 T ES91918749 T ES 91918749T ES 91918749 T ES91918749 T ES 91918749T ES 2067954 T3 ES2067954 T3 ES 2067954T3
Authority
ES
Spain
Prior art keywords
aluminum oxide
procedure
formation
performance
spheres
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES91918749T
Other languages
English (en)
Inventor
Martin Kadner
Egbert Brandau
Hans Huschka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nukem GmbH
Original Assignee
Nukem GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE4035089A external-priority patent/DE4035089C1/de
Application filed by Nukem GmbH filed Critical Nukem GmbH
Application granted granted Critical
Publication of ES2067954T3 publication Critical patent/ES2067954T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/06—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a liquid medium
    • B01J2/08—Gelation of a colloidal solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/51—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/34—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of sprayed or atomised solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/10—Solid density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Catalysts (AREA)

Abstract

PARA LA FABRICACION DE BOLITAS DE OXIDO DE ALUMINIO, UN ACIDO DE ALUMINIO OXIDOSOL O UNA SUSPENSION DE ACIDO DE ALUMINIO OXIDO ES CONVERTIDO EN GOTITAS MEDIANTE UNA PLACA DE TOBERAS DE VIBRACION Y SOLIDIFICADAS PREVIAMENTE DESPUES DE LA FORMACION DE UN PERFIL DE BOLA MEDIANTE EL SOPLADO LATERAL DE AMONIACO GASEOSO Y A CONTINUACION COAGULADAS EN UNA SOLUCION DE AMONIACO.
ES91918749T 1990-11-05 1991-10-30 Procedimiento para la obtencion de esferas de oxido de aluminio. Expired - Lifetime ES2067954T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE4042594A DE4042594A1 (de) 1990-11-05 1990-11-05 Verfahren zur herstellung von aluminiumoxidkugeln
DE4035089A DE4035089C1 (en) 1990-11-05 1990-11-05 Aluminium oxide spheres for adsorbent, chromatography, catalyst etc. - with defined surface area, density, pore vol, breaking strength and narrow particles size distribution etc.

Publications (1)

Publication Number Publication Date
ES2067954T3 true ES2067954T3 (es) 1995-04-01

Family

ID=25898252

Family Applications (1)

Application Number Title Priority Date Filing Date
ES91918749T Expired - Lifetime ES2067954T3 (es) 1990-11-05 1991-10-30 Procedimiento para la obtencion de esferas de oxido de aluminio.

Country Status (8)

Country Link
US (1) US6197073B1 (es)
EP (1) EP0556222B1 (es)
AT (1) ATE116156T1 (es)
AU (1) AU8762791A (es)
CA (1) CA2095349A1 (es)
DE (2) DE4042594A1 (es)
ES (1) ES2067954T3 (es)
WO (1) WO1992007653A1 (es)

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DE4237272A1 (de) * 1992-11-04 1994-05-05 Nukem Gmbh Verfahren zur Herstellung von stabilisiertem Hafniumoxidpulver oder Hafniumoxid enthaltendem Pulver
DE4491189D2 (de) * 1993-03-05 1995-04-27 Solvay Deutschland Verfahren zur katalytischen Behandlung von organische und anorganische Verbindungen enthaltenden Abwässern, vorzugsweise aus der Epichlorhydrinproduktion
DE19845126A1 (de) * 1998-09-30 2000-04-06 Marco Systemanalyse Entw Verfahren zur Tropfenbildung
US7068825B2 (en) * 1999-03-08 2006-06-27 Orametrix, Inc. Scanning system and calibration method for capturing precise three-dimensional information of objects
JP2001187773A (ja) * 2000-01-06 2001-07-10 Mitsubishi Chemicals Corp アクリロニトリル組成物
DE10135452A1 (de) * 2001-07-20 2003-02-06 Degussa Pyrogen hergestellte Aluminium-Silicium-Mischoxide
DE10138574A1 (de) * 2001-08-06 2003-02-27 Degussa Granulate auf Basis von pyrogen hergestelltem Aluminiumoxid, Verfahren zu ihrer Herstellung und ihre Verwendung
DE10152745A1 (de) * 2001-10-25 2003-05-15 Degussa Dispersion von Aluminiumoxid
US6797203B2 (en) * 2002-07-12 2004-09-28 Cerco Llc Method of forming ceramic beads
CA2447928C (en) * 2003-11-04 2007-09-04 Global Synfrac Inc. Proppants and their manufacture
US8012533B2 (en) * 2005-02-04 2011-09-06 Oxane Materials, Inc. Composition and method for making a proppant
US7491444B2 (en) * 2005-02-04 2009-02-17 Oxane Materials, Inc. Composition and method for making a proppant
ATE531895T1 (de) 2005-02-04 2011-11-15 Oxane Materials Inc Zusammensetzung und verfahren zur herstellung eines stützmittels
US7867613B2 (en) * 2005-02-04 2011-01-11 Oxane Materials, Inc. Composition and method for making a proppant
US8047288B2 (en) 2007-07-18 2011-11-01 Oxane Materials, Inc. Proppants with carbide and/or nitride phases
MX2012007248A (es) * 2009-12-22 2012-07-30 Oxane Materials Inc Un consolidante que tiene un material de vidrio-ceramica.
EP2519473A4 (en) 2009-12-31 2016-12-07 Halliburton Energy Services Inc CERAMIC PARTICLES WITH CONTROLLED PORENE AND / OR MICROBALL PLACEMENT AND / OR SIZE AND METHOD OF PRODUCTION THEREOF
WO2011094106A1 (en) 2010-01-29 2011-08-04 Oxane Materials, Inc. Self-toughened high-strengh proppant and methods of making same
DE102010045479A1 (de) 2010-09-16 2014-10-30 Brace Capital Gmbh Verfahren zur Mikroverkapselung, Herstellung von festen Formen mehrphasiger mischbarer und nichtmischbarer Materialien und Methode zur Herstellung vorgenannter Systeme
US9670400B2 (en) 2011-03-11 2017-06-06 Carbo Ceramics Inc. Proppant particles formed from slurry droplets and methods of use
US8865631B2 (en) 2011-03-11 2014-10-21 Carbo Ceramics, Inc. Proppant particles formed from slurry droplets and method of use
US9175210B2 (en) 2011-03-11 2015-11-03 Carbo Ceramics Inc. Proppant particles formed from slurry droplets and method of use
US8883693B2 (en) 2011-03-11 2014-11-11 Carbo Ceramics, Inc. Proppant particles formed from slurry droplets and method of use
US9315719B2 (en) 2011-07-13 2016-04-19 Halliburton Energy Services, Inc. Low surface friction proppants
SG11201403130VA (en) 2012-02-16 2014-07-30 Univ Nanyang Tech A metal oxide composite and a method of forming thereof
US10369724B2 (en) 2015-11-19 2019-08-06 Schlumberger Technology Corporation Method of making spheroidal particles
US9896618B2 (en) 2015-11-19 2018-02-20 Schlumberger Technology Corporation Method of making rod-shaped particles for use as proppant and anti-flowback additive
US9932519B2 (en) 2015-11-19 2018-04-03 Schlumberger Technology Corporation Method of making particles having a ridge portion for use as proppant
US10391679B2 (en) 2016-07-22 2019-08-27 Schlumberger Technology Corporation Perforated membranes and methods of making the same
US10557079B2 (en) 2016-07-22 2020-02-11 Schlumberger Technology Corporation Method of making rod-shaped particles for use as proppant and anti-flowback additive
DE102017128734A1 (de) 2017-12-04 2019-06-06 Schott Ag Verbundmaterial, umfassend wenigstens ein erstes Material und Partikel, wobei die Partikel einen negativen thermischen Ausdehnungskoeffizienten α aufweisen, und Klebematerial umfassend das Verbundmaterial
DE102017128719A1 (de) 2017-12-04 2019-06-06 Schott Ag Lithiumionenleitendes Verbundmaterial, umfassend wenigstens ein Polymer und lithiumionenleitende Partikel, und Verfahren zur Herstellung eines Lithiumionenleiters aus dem Verbundmaterial
CN108863435B (zh) * 2018-05-22 2021-02-19 清华大学 一种由铝溶胶自凝胶成型制备氧化铝泡沫陶瓷的方法
CN110871112B (zh) * 2018-08-31 2023-01-13 中国石油化工股份有限公司 一种制备球形载体的成球装置和方法
EP3882226A1 (de) 2020-03-19 2021-09-22 Sigmund Lindner GmbH Sphärische aluminiumoxidkörper
CN112429755A (zh) * 2020-11-18 2021-03-02 山东物华新材料科技有限公司 一种水处理活性氧化铝球的制备方法
CN115703066B (zh) * 2021-08-17 2024-03-26 中国石油天然气股份有限公司 一种连续重整催化剂的制备方法
CN115920977B (zh) * 2021-08-17 2024-04-30 中国石油天然气股份有限公司 一种球形氧化铝载体的成型方法
JP2025513598A (ja) 2022-04-25 2025-04-24 ビーエーエスエフ コーポレーション 粒状アルミナの調製方法

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US2968833A (en) * 1957-05-17 1961-01-24 Phillips Petroleum Co Method and apparatus for prilling ammonium nitrate
CH486273A (fr) * 1967-10-19 1970-02-28 Max Kaltenbach Roger Procédé de formation de gouttelettes uniformes d'un diamètre déterminé, appareil pour la mise en oeuvre de ce procédé et application de ce procédé à la fabrication d'un produit granulé
GB1395486A (en) * 1971-05-05 1975-05-29 Atomic Energy Authority Uk Formation of liquid droplets
US4043507A (en) * 1971-05-05 1977-08-23 United Kingdom Atomic Energy Authority Apparatus for the formation of liquid droplets
US4179408A (en) * 1977-03-25 1979-12-18 W. R. Grace & Co. Process for preparing spheroidal alumina particles
IT1075699B (it) * 1977-04-15 1985-04-22 Agip Nucleare Spa Apparecchiatura e procedimento per produrre microsfere mediante vibrazioni
US4190622A (en) * 1978-05-04 1980-02-26 Standard Oil Company (Ohio) Process for prilling urea
JPS5560022A (en) * 1978-10-26 1980-05-06 Nikki Universal Co Ltd Production of spherical alumina
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DE4214272A1 (de) * 1992-05-04 1993-11-11 Nukem Gmbh Verfahren und Vorrichtung zur Herstellung von Mikrokugeln

Also Published As

Publication number Publication date
AU8762791A (en) 1992-05-26
ATE116156T1 (de) 1995-01-15
DE4042594C2 (es) 1993-04-15
DE4042594A1 (de) 1992-07-02
US6197073B1 (en) 2001-03-06
DE59104098D1 (de) 1995-02-09
EP0556222B1 (de) 1994-12-28
WO1992007653A1 (de) 1992-05-14
CA2095349A1 (en) 1992-05-06
EP0556222A1 (de) 1993-08-25

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