ES2069084T3 - Procedimiento para la fabricacion de pigmentos agregados estructurales. - Google Patents

Procedimiento para la fabricacion de pigmentos agregados estructurales.

Info

Publication number
ES2069084T3
ES2069084T3 ES90911929T ES90911929T ES2069084T3 ES 2069084 T3 ES2069084 T3 ES 2069084T3 ES 90911929 T ES90911929 T ES 90911929T ES 90911929 T ES90911929 T ES 90911929T ES 2069084 T3 ES2069084 T3 ES 2069084T3
Authority
ES
Spain
Prior art keywords
manufacture
structural
procedure
added pigments
added
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES90911929T
Other languages
English (en)
Inventor
Adam F Kaliski
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Industrial Progress Inc
Original Assignee
Industrial Progress Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Industrial Progress Inc filed Critical Industrial Progress Inc
Application granted granted Critical
Publication of ES2069084T3 publication Critical patent/ES2069084T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/40—Compounds of aluminium
    • C09C1/42—Clays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/06—Treatment with inorganic compounds
    • C09C3/063—Coating
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/10—Treatment with macromolecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/19—Oil-absorption capacity, e.g. DBP values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/21—Attrition-index or crushing strength of granulates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C01P2006/62—L* (lightness axis)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C01P2006/63—Optical properties, e.g. expressed in CIELAB-values a* (red-green axis)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C01P2006/64—Optical properties, e.g. expressed in CIELAB-values b* (yellow-blue axis)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C01P2006/66—Hue (H*)
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Paper (AREA)
  • Exposure Control For Cameras (AREA)
  • Indication In Cameras, And Counting Of Exposures (AREA)
  • Studio Devices (AREA)
  • Paints Or Removers (AREA)

Abstract

PROCESO PARA LA FABRICACION DE PRODUCTOS DE PIGMENTO AGREGADO ESTRUCTURAL CON PROPIEDADES FUNCIONALES INTRINSECAMENTE CONSTRUIDAS, DE DISPERSIONES ACUOSAS DE MATERIA EN PARTICULAS TRATADA CON MICROGELES FUNCIONALES COMPLEJOS FORMADOS IN SITU CON CINETICA DE FORMACION RAPIDA.
ES90911929T 1989-10-12 1990-03-28 Procedimiento para la fabricacion de pigmentos agregados estructurales. Expired - Lifetime ES2069084T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/420,388 US5116418A (en) 1984-12-03 1989-10-12 Process for making structural aggregate pigments

Publications (1)

Publication Number Publication Date
ES2069084T3 true ES2069084T3 (es) 1995-05-01

Family

ID=23666267

Family Applications (1)

Application Number Title Priority Date Filing Date
ES90911929T Expired - Lifetime ES2069084T3 (es) 1989-10-12 1990-03-28 Procedimiento para la fabricacion de pigmentos agregados estructurales.

Country Status (15)

Country Link
US (1) US5116418A (es)
EP (1) EP0495784B1 (es)
JP (1) JPH05504905A (es)
CN (1) CN1050889A (es)
AR (1) AR244287A1 (es)
AT (1) ATE119507T1 (es)
AU (1) AU649377B2 (es)
CA (1) CA2067376A1 (es)
DE (1) DE69017705T2 (es)
ES (1) ES2069084T3 (es)
IL (1) IL94921A (es)
IN (1) IN171537B (es)
WO (1) WO1991005745A1 (es)
YU (1) YU152590A (es)
ZA (1) ZA905093B (es)

Families Citing this family (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5279663A (en) * 1989-10-12 1994-01-18 Industrial Progesss, Inc. Low-refractive-index aggregate pigments products
US5312484A (en) * 1989-10-12 1994-05-17 Industrial Progress, Inc. TiO2 -containing composite pigment products
US5378399A (en) * 1990-01-31 1995-01-03 Industrial Progress, Inc. Functional complex microgels with rapid formation kinetics
AU655753B2 (en) * 1990-01-31 1995-01-12 Industrial Progress, Inc. Functional complex microgels with rapid formation kinetics
US5152835A (en) * 1991-05-08 1992-10-06 Engelhard Corporation Composite titania-calcined kaolin opacifying pigments and method for making and using same
US5346546A (en) * 1991-07-22 1994-09-13 Industrial Progress, Inc. Aggregate-TiO2 pigment products
GB2267503B (en) * 1992-06-04 1996-07-24 Tioxide Group Services Ltd Composite pigmentary material comprising particles of opposite surface charge
GB9211822D0 (en) * 1992-06-04 1992-07-15 Tioxide Group Services Ltd Composite pigmentary material
US5336311A (en) * 1992-07-07 1994-08-09 Nord Kaolin Company Cationic pigments
WO1994004752A1 (en) * 1992-08-20 1994-03-03 Industrial Progress, Inc. Acid-to-alkaline papermaking process
US5676747A (en) * 1995-12-29 1997-10-14 Columbia River Carbonates Calcium carbonate pigments for coating paper and paper board
US5650002A (en) * 1995-11-13 1997-07-22 E. I. Du Pont De Nemours And Company TiO2 light scattering efficiency when incorporated in coatings
US5886069A (en) * 1995-11-13 1999-03-23 E. I. Du Pont De Nemours And Company Titanium dioxide particles having substantially discrete inorganic particles dispersed on their surfaces
US5650003A (en) * 1995-12-18 1997-07-22 Nord Naolin Company Cationized pigments and their use in papermaking
US5690728A (en) * 1996-01-02 1997-11-25 Nord Kaolin Company Way to synthesize structured composite premium pigments
US5755870A (en) * 1996-12-11 1998-05-26 Dry Branch Kaolin Company Composite aggregate pigments for the coating industry
EP1019454B1 (en) * 1997-01-09 2001-11-07 Ciba SC Holding AG Composite pigment
RU2189351C2 (ru) 1997-06-09 2002-09-20 Акцо Нобель Н.В. Полисиликатные микрогели и материалы на основе диоксида кремния
DE69834035T2 (de) * 1997-06-09 2006-11-02 Akzo Nobel N.V. Polysilikat-mikrogele
US6387500B1 (en) 1997-11-06 2002-05-14 Cabot Corporation Multi-layered coatings and coated paper and paperboards
JP3986758B2 (ja) * 1999-05-04 2007-10-03 アクゾ ノーベル エヌ．ブイ． シリカをベースとするゾル
US7169261B2 (en) 1999-05-04 2007-01-30 Akzo Nobel N.V. Silica-based sols
RU2144009C1 (ru) * 1999-07-27 2000-01-10 Закрытое акционерное общество "Пластоун" Способ изготовления декоративного наполнителя
CA2380408C (en) 1999-07-30 2008-04-22 Ppg Industries Ohio, Inc. Coating compositions having improved scratch resistance, coated substrates and methods related thereto
CA2380403C (en) 1999-07-30 2009-12-08 Ppg Industries Ohio, Inc. Cured coatings having improved scratch resistance, coated substrates and methods related thereto
EP1204709B1 (en) 1999-07-30 2007-02-14 PPG Industries Ohio, Inc. Coating compositions having improved scratch resistance, coated substrates and methods related thereto
US6610777B1 (en) 1999-07-30 2003-08-26 Ppg Industries Ohio, Inc. Flexible coating compositions having improved scratch resistance, coated substrates and methods related thereto
US6623791B2 (en) 1999-07-30 2003-09-23 Ppg Industries Ohio, Inc. Coating compositions having improved adhesion, coated substrates and methods related thereto
US6379501B1 (en) 1999-12-14 2002-04-30 Hercules Incorporated Cellulose products and processes for preparing the same
US6635341B1 (en) 2000-07-31 2003-10-21 Ppg Industries Ohio, Inc. Coating compositions comprising silyl blocked components, coating, coated substrates and methods related thereto
US6702922B2 (en) * 2002-07-17 2004-03-09 Mw Custom Papers, Llc Papers for use in decorative laminates and methods of making the same
US6863825B2 (en) * 2003-01-29 2005-03-08 Union Oil Company Of California Process for removing arsenic from aqueous streams
EP1586704A1 (en) * 2004-04-16 2005-10-19 SOLVAY (Société Anonyme) Use of ultrafine calcium carbonate particles in papermaking
US20070181275A1 (en) * 2005-04-14 2007-08-09 Solvay (Socete Anonyme) Use of calcuim carbonate particles in papermaking
US20070093572A1 (en) * 2005-10-20 2007-04-26 Jayprakash Bhatt White ink
US10369828B2 (en) * 2006-04-06 2019-08-06 Hewlett-Packard Development Company, L.P. Glossy media sheet
WO2008068322A1 (en) * 2006-12-08 2008-06-12 Solvay (Société Anonyme) Coated alkaline-earth metal carbonate particles, use of such particles in the production of construction materials and construction materials compositions containing such particles
US8066874B2 (en) 2006-12-28 2011-11-29 Molycorp Minerals, Llc Apparatus for treating a flow of an aqueous solution containing arsenic
US8252087B2 (en) 2007-10-31 2012-08-28 Molycorp Minerals, Llc Process and apparatus for treating a gas containing a contaminant
US8349764B2 (en) 2007-10-31 2013-01-08 Molycorp Minerals, Llc Composition for treating a fluid
US20090107925A1 (en) * 2007-10-31 2009-04-30 Chevron U.S.A. Inc. Apparatus and process for treating an aqueous solution containing biological contaminants
EP2351803B1 (en) * 2008-11-25 2018-12-12 Toppan Printing Co., Ltd. Coating liquid and gas barrier laminate
MX2012005351A (es) * 2009-11-09 2012-11-23 Molycorp Minerals Llc Remocion de los colorantes con tierras raras.
US9233863B2 (en) 2011-04-13 2016-01-12 Molycorp Minerals, Llc Rare earth removal of hydrated and hydroxyl species
MX370462B (es) 2014-03-07 2019-12-13 Secure Natural Resources Llc Oxido de cerio (iv) con propiedades de remocion de arsenico excepcionales.

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US2913419A (en) * 1956-04-18 1959-11-17 Du Pont Chemical process and composition
US2974108A (en) * 1957-01-14 1961-03-07 Du Pont Aluminosilicate aquasols and their preparation
US3002932A (en) * 1958-10-27 1961-10-03 Minnesota Mining & Mfg Inorganic anion-exchangers and a process for their preparation
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US3726700A (en) * 1971-03-19 1973-04-10 Du Pont Composite pigments and their preparation
CA1045912A (en) * 1973-12-20 1979-01-09 Alvin Allen Tio2 pigment coated successively with silica and alumina
US4247420A (en) * 1979-03-23 1981-01-27 W. R. Grace & Co. Hydrocarbon conversion catalyst preparation
US4329328A (en) * 1979-10-19 1982-05-11 National Research Development Corporation Method of synthesizing zincosilicate or stannosilicate or titanosilicate material
JPS6033531A (ja) * 1983-08-04 1985-02-20 Canon Inc 光導波路レンズ
US4816074A (en) * 1985-07-12 1989-03-28 E.C.C. America Inc. Kaolinite aggregation using sodium silicate
US4927560A (en) * 1987-02-25 1990-05-22 Nippon Shokubai Kagaku Kogyo Co., Ltd. Method for production of inorganic minute globular particles
ATE67379T1 (de) * 1987-07-10 1991-10-15 Unilever Nv Verfahren zur zubereitung eines aromatisierten nahrungsmittel sowie durch solch ein verfahren erhaltenes nahrungsmittel.
US4927498A (en) * 1988-01-13 1990-05-22 E. I. Du Pont De Nemours And Company Retention and drainage aid for papermaking
JP2629013B2 (ja) * 1988-02-12 1997-07-09 雪印乳業株式会社 粉体等の造粒方法
JPH05506179A (ja) * 1989-10-12 1993-09-16 インダストリアル　プログレス、インク 構造アグリゲート顔料

Also Published As

Publication number Publication date
JPH05504905A (ja) 1993-07-29
IN171537B (es) 1992-11-14
DE69017705D1 (de) 1995-04-13
AU649377B2 (en) 1994-05-19
EP0495784B1 (en) 1995-03-08
AR244287A1 (es) 1993-10-29
CA2067376A1 (en) 1991-04-13
AU6154290A (en) 1991-05-16
ZA905093B (en) 1991-05-29
DE69017705T2 (de) 1995-08-31
CN1050889A (zh) 1991-04-24
EP0495784A1 (en) 1992-07-29
IL94921A0 (en) 1991-04-15
YU152590A (sh) 1993-05-28
EP0495784A4 (en) 1992-11-25
WO1991005745A1 (en) 1991-05-02
IL94921A (en) 1994-06-24
ATE119507T1 (de) 1995-03-15
US5116418A (en) 1992-05-26

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