ES2077411T3 - Preparacion del glicol de politetrametileneter usando un catalizador acido de circonia. - Google Patents
Preparacion del glicol de politetrametileneter usando un catalizador acido de circonia.Info
- Publication number
- ES2077411T3 ES2077411T3 ES92908458T ES92908458T ES2077411T3 ES 2077411 T3 ES2077411 T3 ES 2077411T3 ES 92908458 T ES92908458 T ES 92908458T ES 92908458 T ES92908458 T ES 92908458T ES 2077411 T3 ES2077411 T3 ES 2077411T3
- Authority
- ES
- Spain
- Prior art keywords
- glycol
- politetrametileneter
- zirconia
- preparation
- acid catalyst
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title 2
- 239000003377 acid catalyst Substances 0.000 title 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 abstract 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 abstract 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/266—Metallic elements not covered by group C08G65/2648 - C08G65/2645, or compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/16—Cyclic ethers having four or more ring atoms
- C08G65/20—Tetrahydrofuran
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
UN PROCESO PARA POLIMERIZAR TETRAHIDROFURANO PARA PRODUCIR GLICOL ETHER POLITETRAMETILENO O GLICOL ETER POLITETRAMETILENO ESTER ENCAPSULADO. LA REACCION EN MASA SE LLEVA A CABO ENTRE 10 REFERIDO DEL INVENTO, UNA MEZCLA DE ANHIDRIDO ACETICO Y ACIDO ACETICO ESTA PRESENTE EN LA MEZCLA DE REACCION
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/661,010 US5149862A (en) | 1991-02-26 | 1991-02-26 | Preparation of polytetramethylene ether glycol using an acidic zirconia catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2077411T3 true ES2077411T3 (es) | 1995-11-16 |
Family
ID=24651828
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES92908458T Expired - Lifetime ES2077411T3 (es) | 1991-02-26 | 1992-02-06 | Preparacion del glicol de politetrametileneter usando un catalizador acido de circonia. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5149862A (es) |
| EP (1) | EP0573602B1 (es) |
| JP (1) | JP2976383B2 (es) |
| KR (1) | KR100193017B1 (es) |
| AU (1) | AU1581392A (es) |
| DE (1) | DE69203859T2 (es) |
| ES (1) | ES2077411T3 (es) |
| WO (1) | WO1992014773A1 (es) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5344964A (en) * | 1993-11-24 | 1994-09-06 | Industrial Technology Research Institute | Method for preparing ester end-capped polyalkylene ether |
| DE4433606A1 (de) * | 1994-09-21 | 1996-03-28 | Basf Ag | Verfahren zur Herstellung von Polyetrahydrofuran |
| DE19527532A1 (de) * | 1995-07-27 | 1997-01-30 | Basf Ag | Verfahren zur Herstellung von Polyoxytetramethylenglycol |
| US5684179A (en) * | 1995-12-14 | 1997-11-04 | E. I. Du Pont De Nemours And Company | Method for recovering diacetate esters of polytetramethylene ethers |
| TW343201B (en) * | 1995-12-14 | 1998-10-21 | Du Pont | Improved method for manufacturing diacetate esters of polytetramethylene ethers |
| DE19641481A1 (de) * | 1996-10-09 | 1998-04-16 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran |
| DE19719875A1 (de) * | 1997-05-12 | 1998-11-19 | Basf Ag | Verfahren zur Polymerisation cyclischer Ether |
| DE19726507A1 (de) * | 1997-06-23 | 1998-12-24 | Basf Ag | Verbessertes Verfahren zur Herstellung von Polytetrahydrofuran |
| TW442513B (en) | 1999-05-19 | 2001-06-23 | Dairen Chemical Corp | Method for preparing polyether diol |
| DE10032266A1 (de) | 2000-07-03 | 2002-01-17 | Basf Ag | Verbessertes Verfahren zur einstufigen Herstellung von Polytetrahydrofuran und Tetrahydrofuran-Copolymeren |
| DE10324998A1 (de) * | 2003-06-03 | 2004-12-23 | Basf Ag | Herstellung von Polyetheralkoholen unter Verwendung der DMC-Katalyse |
| CN102216255A (zh) * | 2008-11-18 | 2011-10-12 | 因温斯特技术公司 | 1,2-二氨基环己烷和化学方法 |
| US8609805B2 (en) | 2009-04-15 | 2013-12-17 | Invista North America S.A R.L. | Copolyether glycol manufacturing process |
| US8551192B2 (en) * | 2009-04-15 | 2013-10-08 | Invista North America S.A.R.L. | Miscibility of otherwise immiscible compounds |
| US8372946B2 (en) * | 2009-04-15 | 2013-02-12 | Invista North America S.A R.L. | Copolyether glycol manufacturing process |
| KR20120102072A (ko) | 2009-12-11 | 2012-09-17 | 인비스타 테크놀러지스 에스.에이.알.엘. | 올리고머 시클릭 에테르의 해중합 |
| JP6263877B2 (ja) * | 2013-07-03 | 2018-01-24 | 三菱ケミカル株式会社 | ポリアルキレンエーテルグリコールジエステルの製造方法 |
| TW201529636A (zh) * | 2013-12-19 | 2015-08-01 | Invista Tech Sarl | 經改良的聚四亞甲基醚二醇製造方法 |
| TWI646125B (zh) | 2014-01-06 | 2019-01-01 | 盧森堡商英威達技術有限公司 | 共聚醚酯聚醇製法 |
| CN110337428A (zh) | 2017-02-28 | 2019-10-15 | 拜耳作物科学股份公司 | 用于制备氟代烷基腈和相应的氟代烷基四唑的方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2445961C2 (de) * | 1974-09-26 | 1983-12-01 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Polymerisation von Tetrahydrofuran |
| US4163115A (en) * | 1976-03-31 | 1979-07-31 | E. I. Du Pont De Nemours And Company | Preparation of esters of poly-(tetramethylene ether) glycol |
| DE2951080A1 (de) * | 1979-12-19 | 1981-07-02 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von carbonsaeureestern von alkylenglykolethern |
| DE3008174A1 (de) * | 1980-03-04 | 1981-09-24 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von carbonsaeureestern von alkylenglykolethern |
| DE3211635A1 (de) * | 1982-03-30 | 1983-10-06 | Bayer Ag | Verfahren zur herstellung von polyetrahydrofuranen mit esterendgruppen |
| US4727199A (en) * | 1985-07-10 | 1988-02-23 | Union Carbide Corporation | Heterogeneous alkoxylation using anion-bound metal oxides |
-
1991
- 1991-02-26 US US07/661,010 patent/US5149862A/en not_active Expired - Lifetime
-
1992
- 1992-02-06 JP JP4508119A patent/JP2976383B2/ja not_active Expired - Lifetime
- 1992-02-06 AU AU15813/92A patent/AU1581392A/en not_active Abandoned
- 1992-02-06 KR KR1019930702533A patent/KR100193017B1/ko not_active Expired - Lifetime
- 1992-02-06 EP EP92908458A patent/EP0573602B1/en not_active Expired - Lifetime
- 1992-02-06 DE DE69203859T patent/DE69203859T2/de not_active Expired - Lifetime
- 1992-02-06 ES ES92908458T patent/ES2077411T3/es not_active Expired - Lifetime
- 1992-02-06 WO PCT/US1992/000693 patent/WO1992014773A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| JPH06505515A (ja) | 1994-06-23 |
| EP0573602B1 (en) | 1995-08-02 |
| AU1581392A (en) | 1992-09-15 |
| DE69203859T2 (de) | 1996-03-14 |
| EP0573602A1 (en) | 1993-12-15 |
| US5149862A (en) | 1992-09-22 |
| DE69203859D1 (de) | 1995-09-07 |
| WO1992014773A1 (en) | 1992-09-03 |
| KR100193017B1 (ko) | 1999-06-15 |
| JP2976383B2 (ja) | 1999-11-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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