ES2078560T3 - Procedimiento para la preparacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina. - Google Patents
Procedimiento para la preparacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina.Info
- Publication number
- ES2078560T3 ES2078560T3 ES92101054T ES92101054T ES2078560T3 ES 2078560 T3 ES2078560 T3 ES 2078560T3 ES 92101054 T ES92101054 T ES 92101054T ES 92101054 T ES92101054 T ES 92101054T ES 2078560 T3 ES2078560 T3 ES 2078560T3
- Authority
- ES
- Spain
- Prior art keywords
- ciclohexilamina
- trimetil
- aminometil
- procedure
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 5
- JJDFVIDVSCYKDS-UHFFFAOYSA-N 1,3,3-trimethyl-5-oxocyclohexane-1-carbonitrile Chemical compound CC1(C)CC(=O)CC(C)(C#N)C1 JJDFVIDVSCYKDS-UHFFFAOYSA-N 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 239000007868 Raney catalyst Substances 0.000 abstract 2
- 229910017052 cobalt Inorganic materials 0.000 abstract 2
- 239000010941 cobalt Substances 0.000 abstract 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 2
- 229910052759 nickel Inorganic materials 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000003426 co-catalyst Substances 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052747 lanthanoid Inorganic materials 0.000 abstract 1
- 150000002602 lanthanoids Chemical class 0.000 abstract 1
- 238000006268 reductive amination reaction Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229910052727 yttrium Inorganic materials 0.000 abstract 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/45—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings
- C07C255/46—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of non-condensed rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
LA AMINACION POR REDUCCION DE 1,3,3 SENCIA DE CATALIZADORES RANEY DE NIQUEL O COBALTO EN 3 METIL TAPA CON BUEN RENDIMIENTO Y NO NECESITA DESTILACION POR PRESION, SI SE UTILIZA ADICIONALMENTE UN COCATALIZADOR DE LA SERIE DE UNA SAL DE NIQUEL, COBALTO, YTRIO O UN ELEMENTO LANTANIDO EN UNA CANTIDAD DE 0,01 HASTA 005 MOL POR MOL DE CATALIZADOR RANEY.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4106882A DE4106882C2 (de) | 1991-03-05 | 1991-03-05 | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethyl-cyclohexylamin durch reduktive Aminierung von 1,3,3-Trimethyl-5-oxocyclohexan-carbonitril |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2078560T3 true ES2078560T3 (es) | 1995-12-16 |
Family
ID=6426449
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES92101054T Expired - Lifetime ES2078560T3 (es) | 1991-03-05 | 1992-01-23 | Procedimiento para la preparacion de 3-aminometil-3,5,5-trimetil-ciclohexilamina. |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0503246B1 (es) |
| JP (1) | JP2525530B2 (es) |
| AT (1) | ATE128962T1 (es) |
| CA (1) | CA2062267A1 (es) |
| DE (2) | DE4106882C2 (es) |
| ES (1) | ES2078560T3 (es) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0534449A3 (en) * | 1991-09-25 | 1993-06-02 | Mitsubishi Kasei Corporation | Process for the preparation of 3-aminomethyl-3,5,5-trialkylcyclohexylamine |
| CA2115025A1 (en) * | 1993-02-08 | 1994-08-09 | Atsushi Furutani | Process for producing amines |
| CA2115024A1 (en) * | 1993-04-27 | 1994-10-28 | Atsushi Furutani | Process for producing amines |
| DE4343890A1 (de) * | 1993-12-22 | 1995-06-29 | Degussa | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| DE4343891A1 (de) * | 1993-12-22 | 1995-06-29 | Degussa | Verfahren zur Beeinflussung des cis-/trans-Isomerenverhältnisses von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin bei dessen Herstellung aus 3-Cyano-3,5,5-trimethylcyclohexanon |
| DE4407325B4 (de) * | 1994-03-04 | 2006-06-29 | Basf Ag | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| DE19507398C1 (de) * | 1995-03-03 | 1996-09-12 | Basf Ag | Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin |
| US5766006A (en) * | 1995-06-26 | 1998-06-16 | Murljacic; Maryann Lehmann | Tooth shade analyzer system and methods |
| JP5650121B2 (ja) * | 2008-11-11 | 2015-01-07 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 環状ジアミンの製造方法 |
| EP3162790A1 (de) | 2015-10-30 | 2017-05-03 | Evonik Degussa GmbH | Herstellungsverfahren für isophoronaminoalkohol (ipaa) |
| EP3162791A1 (de) | 2015-10-30 | 2017-05-03 | Evonik Degussa GmbH | Verbessertes herstellungsverfahren für isophoronaminoalkohol (ipaa) |
| DE102017202404A1 (de) | 2017-02-15 | 2018-08-16 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Isophoronaminoalkohol (IPAA) |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3011656A1 (de) * | 1980-03-26 | 1981-10-01 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 3-aminomethyl-3-5-5-trimethyl-cyclohexylamin |
| DE3021955A1 (de) * | 1980-06-12 | 1981-12-24 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung primaerer mono- und diamine aus oxoverbindungen |
| JPH0669991B2 (ja) * | 1985-11-25 | 1994-09-07 | ダイセル化学工業株式会社 | 3−アミノメチル−3,5,5−トリメチルシクロヘキシルアミンの製造法 |
| BR9001892A (pt) * | 1989-04-25 | 1991-07-30 | Union Carbide Chem Plastic | Processo para aminacao de uma alimentacao compreendendo composto organico e processo para ativar um catalisador de aminacao redutora |
| KR900016106A (ko) * | 1989-04-25 | 1990-11-12 | 마릴린 클로스티 | 카보닐니트릴 및 이와 유사한 화합물의 환원적 아민화 방법 |
-
1991
- 1991-03-05 DE DE4106882A patent/DE4106882C2/de not_active Expired - Fee Related
-
1992
- 1992-01-23 EP EP92101054A patent/EP0503246B1/de not_active Expired - Lifetime
- 1992-01-23 ES ES92101054T patent/ES2078560T3/es not_active Expired - Lifetime
- 1992-01-23 AT AT92101054T patent/ATE128962T1/de not_active IP Right Cessation
- 1992-01-23 DE DE59203933T patent/DE59203933D1/de not_active Expired - Fee Related
- 1992-03-04 CA CA002062267A patent/CA2062267A1/en not_active Abandoned
- 1992-03-04 JP JP4046917A patent/JP2525530B2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE4106882C2 (de) | 1994-02-03 |
| ATE128962T1 (de) | 1995-10-15 |
| JPH04338365A (ja) | 1992-11-25 |
| EP0503246B1 (de) | 1995-10-11 |
| JP2525530B2 (ja) | 1996-08-21 |
| CA2062267A1 (en) | 1992-09-06 |
| DE4106882A1 (de) | 1992-09-10 |
| EP0503246A1 (de) | 1992-09-16 |
| DE59203933D1 (de) | 1995-11-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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