ES2081712T3 - Un metodo para determinar urea en leche. - Google Patents
Un metodo para determinar urea en leche.Info
- Publication number
- ES2081712T3 ES2081712T3 ES93908832T ES93908832T ES2081712T3 ES 2081712 T3 ES2081712 T3 ES 2081712T3 ES 93908832 T ES93908832 T ES 93908832T ES 93908832 T ES93908832 T ES 93908832T ES 2081712 T3 ES2081712 T3 ES 2081712T3
- Authority
- ES
- Spain
- Prior art keywords
- frequency band
- determination
- urea
- fat
- absorbed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title abstract 5
- 239000004202 carbamide Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 3
- 239000008267 milk Substances 0.000 title abstract 3
- 210000004080 milk Anatomy 0.000 title abstract 3
- 235000013336 milk Nutrition 0.000 title abstract 3
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 abstract 4
- 239000008101 lactose Substances 0.000 abstract 4
- 102000004169 proteins and genes Human genes 0.000 abstract 4
- 108090000623 proteins and genes Proteins 0.000 abstract 4
- 238000010521 absorption reaction Methods 0.000 abstract 3
- 230000005855 radiation Effects 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
- G01N33/04—Dairy products
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3577—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2201/00—Features of devices classified in G01N21/00
- G01N2201/12—Circuits of general importance; Signal processing
- G01N2201/129—Using chemometrical methods
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S250/00—Radiant energy
- Y10S250/91—Food sample analysis using invisible radiant energy source
Landscapes
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Food Science & Technology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Medicinal Chemistry (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Dairy Products (AREA)
- Tea And Coffee (AREA)
- Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
- General Preparation And Processing Of Foods (AREA)
- Testing Or Measuring Of Semiconductors Or The Like (AREA)
- Amplifiers (AREA)
- Oscillators With Electromechanical Resonators (AREA)
- Peptides Or Proteins (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Abstract
UN METODO PARA DETERMINAR, CON UNA PRECISION MAYOR DE 0''007% EXPRESADO EN ERROR ESTANDAR DE PREDICCION, LA CONCENTRACION DE UREA EN UNA GAMA DE CONCENTRACION DE 0-0''1% EN MUESTRA DE LECHE, CONTENIENDO AL MENOS 1% DE GRASA, AL MENOS 1% DE LACTOSA DISUELTA, Y AL MENOS 1% DE PROTEINA, MEDIANTE UNA TECNICA DE MEDICION DE ABSORCION DE RAYOS INFRARROJOS, COMPRENDIENDO: (A) DETERMINACION DE LA ABSORCION EN UNA BANDA DE FRECUENCIAS DE RADIACION DE RAYOS INFRARROJOS DESDE 1000 CM-1 (10''0 UM) A 4000 CM-1 (2''50 UM) DE LA MUESTRA DE LECHE, DONDE AL MENOS SE HACE UNA DETERMINACION EN UNA BANDA DE FRECUENCIAS DESDE 1000 CM-1 (10''0 UM) A 1800-1 (5''56 UM), DONDE LA UREA SE ABSORBE, AL MENOS HACIENDO UNA DETERMINACION EN UNA BANDA DE FRECUENCIAS DONDE LA GRASA SE ABSORBE, AL MENOS HACIENDO UNA DETERMINACION EN UNA BANDA DE FRECUENCIAS DONDE LA LACTOSA SE ABSORBE, Y HACIENDO UNA DETERMINACION EN UNA BANDA DE FRECUENCIAS DONDE LA PROTEINA SE ABSORBE; (B) DETERMINANDO, SOBRE LA BASE DE DETERMINACIONES DE ABSORCION Y PARAMETROS PREDETERMINADOS ESTABLECIDOS POR CALIBRACION MULTIVARIANTE, UNA CONTRIBUCION DESDE GRASA, LACTOSA Y PROTEINA EN LA BANDA DE FRECUENCIAS DONDE LA UREA SE ABSORBE, (C) ESTABLECIENDO CUANTITATIVAMENTE LA CONCENTRACION DE UREA EN LA MUESTRA SOBRE LA BASE DE LA ABSORCION EN LA BANDA DE FRECUENCIAS DONDE LA UREA SE ABSORBE, Y SOBRE LA BASE DE LA CONTRIBUCION DETERMINADA DE GRASA, LACTOSA Y PROTEINA EN LA BANDA DE FRECUENCIAS.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DK92397A DK39792D0 (da) | 1992-03-25 | 1992-03-25 | Fremgangsmaade til bestemmelse af en komponent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2081712T3 true ES2081712T3 (es) | 1996-03-16 |
Family
ID=8093065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93908832T Expired - Lifetime ES2081712T3 (es) | 1992-03-25 | 1993-03-25 | Un metodo para determinar urea en leche. |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US5252829A (es) |
| EP (1) | EP0629290B1 (es) |
| JP (1) | JP2547311B2 (es) |
| KR (1) | KR0148750B1 (es) |
| AT (1) | ATE132972T1 (es) |
| AU (1) | AU655110B2 (es) |
| BR (1) | BR9306145A (es) |
| CA (1) | CA2132861C (es) |
| DE (2) | DE629290T1 (es) |
| DK (2) | DK39792D0 (es) |
| ES (1) | ES2081712T3 (es) |
| FI (1) | FI114573B (es) |
| NO (1) | NO316048B1 (es) |
| NZ (1) | NZ251676A (es) |
| WO (1) | WO1993019364A1 (es) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2677453B1 (fr) * | 1991-06-10 | 1993-10-08 | Aegys Technology Sa | Procede et appareil de dosage spectrophotometrique des liquides aqueux. |
| AU654933B3 (en) * | 1992-03-25 | 1994-11-24 | Foss Electric A/S | A method for determining urea in milk |
| DK138593D0 (da) * | 1993-12-10 | 1993-12-10 | Foss Electric As | Forbedret maalemetode |
| SG38866A1 (en) * | 1995-07-31 | 1997-04-17 | Instrumentation Metrics Inc | Liquid correlation spectrometry |
| US5747806A (en) * | 1996-02-02 | 1998-05-05 | Instrumentation Metrics, Inc | Method and apparatus for multi-spectral analysis in noninvasive nir spectroscopy |
| US6040578A (en) * | 1996-02-02 | 2000-03-21 | Instrumentation Metrics, Inc. | Method and apparatus for multi-spectral analysis of organic blood analytes in noninvasive infrared spectroscopy |
| EP0821232A1 (de) * | 1996-07-24 | 1998-01-28 | SY-LAB Vertriebsges.m.b.H. | Verfahren zur Bestimmung von Bestandteilen einer Probe und Vorrichtung zur Durchführung des Verfahrens |
| DK173073B1 (da) | 1996-11-01 | 1999-12-20 | Foss Electric As | Fremgangsmåde og flowsystem til spektrometri og en kuvette til flowsystemet |
| NL1004980C2 (nl) * | 1997-01-13 | 1998-07-15 | Maasland Nv | Werkwijze voor het vaststellen van de aanwezigheid van bepaalde stoffen in melk en inrichting voor het toepassen van deze werkwijze. |
| DK34297A (da) * | 1997-03-25 | 1998-09-26 | Foss Electric As | Måling af acetone i mælk ved brug af IR-spektroskopi |
| US6871169B1 (en) | 1997-08-14 | 2005-03-22 | Sensys Medical, Inc. | Combinative multivariate calibration that enhances prediction ability through removal of over-modeled regions |
| US7383069B2 (en) * | 1997-08-14 | 2008-06-03 | Sensys Medical, Inc. | Method of sample control and calibration adjustment for use with a noninvasive analyzer |
| WO2000017611A1 (en) * | 1998-09-18 | 2000-03-30 | Foss Electric A/S | Method and apparatus for process control |
| NL1010540C2 (nl) * | 1998-11-12 | 2000-05-15 | Maasland Nv | Werkwijze voor het vaststellen van de aanwezigheid van bepaalde stoffen in melk en inrichting voor het toepassen van deze werkwijze. |
| JP2000281638A (ja) | 1999-03-26 | 2000-10-10 | Snow Brand Milk Prod Co Ltd | 尿素の分離方法 |
| DE60010499T2 (de) | 1999-10-21 | 2005-05-19 | Foss Analytical A/S | Verfahren und vorrichtung zur bestimmung der eigenschaften von lebensmitteln oder tierfutter |
| DE19957493C2 (de) * | 1999-11-22 | 2001-09-20 | Ufz Leipzighalle Gmbh | Verfahren zur Identitätsprüfung von 13C-Harnstoff |
| EP1305600A2 (en) * | 2000-08-01 | 2003-05-02 | Instrumentation Metrics, Inc. | Combinative multivariate calibration that enhances prediction ability through removal of over-modeled regions |
| US6947848B2 (en) * | 2000-08-07 | 2005-09-20 | Cooper Union For The Advancement Of Science And Art | System and method for identifying unknown compounds using spectra pattern recognition |
| US6549861B1 (en) | 2000-08-10 | 2003-04-15 | Euro-Celtique, S.A. | Automated system and method for spectroscopic analysis |
| AU2001288292A1 (en) | 2000-08-21 | 2002-03-04 | Euroceltique S.A. | Near infrared blood glucose monitoring system |
| US7194369B2 (en) * | 2001-07-23 | 2007-03-20 | Cognis Corporation | On-site analysis system with central processor and method of analyzing |
| NZ533812A (en) * | 2002-01-10 | 2004-12-24 | Foss Analytical As | Method and means for correcting measuring instruments |
| US7302349B2 (en) * | 2002-08-16 | 2007-11-27 | Lattec I/S | System and a method for observing and predicting a physiological state of an animal |
| US7271912B2 (en) | 2003-04-15 | 2007-09-18 | Optiscan Biomedical Corporation | Method of determining analyte concentration in a sample using infrared transmission data |
| WO2007141416A1 (fr) | 2006-06-07 | 2007-12-13 | Valorex | Methode de determination de la qualite nutritionnelle des lipides du lait |
| EP1990617A1 (en) * | 2007-05-09 | 2008-11-12 | FOSS Analytical A/S | Determination of tannins in vinefication products |
| CA2760817C (en) * | 2009-05-14 | 2016-02-09 | Pioneer Hi-Bred International, Inc. | Inverse modeling for characteristic prediction from multi-spectral and hyper-spectral remote sensed datasets |
| US10475529B2 (en) | 2011-07-19 | 2019-11-12 | Optiscan Biomedical Corporation | Method and apparatus for analyte measurements using calibration sets |
| CN102564965B (zh) * | 2011-12-31 | 2014-10-08 | 聚光科技(杭州)股份有限公司 | 基于光谱检测技术的检测方法 |
| CN103245632B (zh) * | 2013-05-15 | 2015-06-03 | 河北科技大学 | 一种中红外光谱检测液态乳中含氮化合物的方法 |
| CN103884675B (zh) * | 2014-03-25 | 2016-08-17 | 史永刚 | 一种基于红外光谱的发动机润滑油识别算法 |
| CN105466906A (zh) * | 2015-12-16 | 2016-04-06 | 新希望双喜乳业(苏州)有限公司 | 一种快速检测牛奶中掺伪尿素含量的方法 |
| WO2017137805A1 (en) | 2016-02-11 | 2017-08-17 | Foss Analytical A/S | Systems for and method of quantitative measure of components of a liquid |
| EP4010688B1 (en) * | 2019-08-06 | 2025-10-01 | Amgen Inc. | System and method for determining protein concentrations of unknown protein samples based on automated multi-wavelength calibration |
| CN114184573B (zh) * | 2021-11-01 | 2022-12-13 | 华中农业大学 | 牛奶中κ-酪蛋白的中红外快速批量检测方法 |
| CN117990616B (zh) * | 2024-02-04 | 2024-10-08 | 北京建筑大学 | 基于分数阶微分的壁画地仗磷酸盐含量高光谱预测方法 |
| CN120721669B (zh) * | 2025-08-14 | 2025-11-07 | 河北省畜牧良种工作总站(河北省种畜禽质量监测站) | 一种生鲜牛奶中红外光谱数据采集与存储的设备与方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU420914A1 (es) * | 1972-06-16 | 1974-03-25 | В. Г. Гизатулин, В. П. Муругов И. И. Свентицкий | |
| DE2606991A1 (de) * | 1976-02-20 | 1977-08-25 | Nils Dr Med Kaiser | Geraet zur bestimmung des gehaltes von stoffwechselprodukten im blut |
| US4447725A (en) * | 1981-06-15 | 1984-05-08 | Biggs Delmar A | Quantitative measurement of fat, protein and lactose in dairy products |
| DE3470607D1 (en) * | 1983-04-05 | 1988-05-26 | Shields Instr Ltd | Measurement of fat |
| FR2606149B1 (fr) * | 1986-10-30 | 1989-01-27 | Jls Ste Civile Brevets | Procede et dispositif d'analyse spectrometrique automatique d'un liquide, notamment du lait |
| FI90592C (fi) * | 1989-02-16 | 1994-02-25 | Anadis Instr Sa | IR-spektrometrinen analysointimenetelmä sekä IR-spektrometri |
| US4975581A (en) * | 1989-06-21 | 1990-12-04 | University Of New Mexico | Method of and apparatus for determining the similarity of a biological analyte from a model constructed from known biological fluids |
| FI86480B (fi) * | 1990-10-03 | 1992-05-15 | Lauri Jalkanen | Foerfarande foer kvantitativ bestaemning av urea fraon mjoelk eller en mjoelkprodukt. |
-
1992
- 1992-03-25 DK DK92397A patent/DK39792D0/da not_active Application Discontinuation
- 1992-05-19 US US07/885,642 patent/US5252829A/en not_active Expired - Lifetime
-
1993
- 1993-03-25 BR BR9306145A patent/BR9306145A/pt not_active IP Right Cessation
- 1993-03-25 NZ NZ251676A patent/NZ251676A/en not_active IP Right Cessation
- 1993-03-25 AU AU39485/93A patent/AU655110B2/en not_active Ceased
- 1993-03-25 AT AT93908832T patent/ATE132972T1/de not_active IP Right Cessation
- 1993-03-25 CA CA002132861A patent/CA2132861C/en not_active Expired - Fee Related
- 1993-03-25 DE DE0629290T patent/DE629290T1/de active Pending
- 1993-03-25 DK DK93908832.4T patent/DK0629290T3/da active
- 1993-03-25 WO PCT/DK1993/000111 patent/WO1993019364A1/en not_active Ceased
- 1993-03-25 DE DE69301310T patent/DE69301310T2/de not_active Expired - Lifetime
- 1993-03-25 ES ES93908832T patent/ES2081712T3/es not_active Expired - Lifetime
- 1993-03-25 JP JP5516189A patent/JP2547311B2/ja not_active Expired - Lifetime
- 1993-03-25 EP EP93908832A patent/EP0629290B1/en not_active Expired - Lifetime
-
1994
- 1994-09-22 NO NO19943519A patent/NO316048B1/no not_active IP Right Cessation
- 1994-09-23 FI FI944410A patent/FI114573B/fi active IP Right Grant
- 1994-09-24 KR KR94703318A patent/KR0148750B1/ko not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR0148750B1 (en) | 1998-08-17 |
| FI114573B (fi) | 2004-11-15 |
| DK0629290T3 (da) | 1996-02-12 |
| JPH07504982A (ja) | 1995-06-01 |
| CA2132861A1 (en) | 1993-09-30 |
| EP0629290A1 (en) | 1994-12-21 |
| CA2132861C (en) | 2000-08-29 |
| ATE132972T1 (de) | 1996-01-15 |
| NZ251676A (en) | 1995-08-28 |
| DK39792D0 (da) | 1992-03-25 |
| AU3948593A (en) | 1993-10-21 |
| JP2547311B2 (ja) | 1996-10-23 |
| NO943519D0 (no) | 1994-09-22 |
| FI944410A0 (fi) | 1994-09-23 |
| US5252829A (en) | 1993-10-12 |
| DE69301310T2 (de) | 1996-05-23 |
| NO316048B1 (no) | 2003-12-01 |
| DE69301310D1 (de) | 1996-02-22 |
| FI944410L (fi) | 1994-09-23 |
| WO1993019364A1 (en) | 1993-09-30 |
| AU655110B2 (en) | 1994-12-01 |
| EP0629290B1 (en) | 1996-01-10 |
| NO943519L (no) | 1994-09-22 |
| BR9306145A (pt) | 1998-01-13 |
| DE629290T1 (de) | 1995-08-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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