ES2082271T3 - Procedimiento para la eliminacion de impurezas de bromuros de alquilo perfluorados o de dibromuros de alquileno perfluorados. - Google Patents
Procedimiento para la eliminacion de impurezas de bromuros de alquilo perfluorados o de dibromuros de alquileno perfluorados.Info
- Publication number
- ES2082271T3 ES2082271T3 ES92108147T ES92108147T ES2082271T3 ES 2082271 T3 ES2082271 T3 ES 2082271T3 ES 92108147 T ES92108147 T ES 92108147T ES 92108147 T ES92108147 T ES 92108147T ES 2082271 T3 ES2082271 T3 ES 2082271T3
- Authority
- ES
- Spain
- Prior art keywords
- alkyl bromide
- perfluored
- alcohols
- elimination
- impurities
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000001347 alkyl bromides Chemical class 0.000 title abstract 2
- 230000008030 elimination Effects 0.000 title 1
- 238000003379 elimination reaction Methods 0.000 title 1
- 239000012535 impurity Substances 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 150000001298 alcohols Chemical class 0.000 abstract 3
- 230000001476 alcoholic effect Effects 0.000 abstract 2
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical compound BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 230000005670 electromagnetic radiation Effects 0.000 abstract 1
- 229910052731 fluorine Inorganic materials 0.000 abstract 1
- 239000011737 fluorine Substances 0.000 abstract 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 abstract 1
- 229910052740 iodine Inorganic materials 0.000 abstract 1
- 239000011630 iodine Substances 0.000 abstract 1
- 150000002497 iodine compounds Chemical class 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P7/00—Drugs for disorders of the blood or the extracellular fluid
- A61P7/08—Plasma substitutes; Perfusion solutions; Dialytics or haemodialytics; Drugs for electrolytic or acid-base disorders, e.g. hypovolemic shock
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Diabetes (AREA)
- Hematology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Water Treatments (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
LAS MEZCLAS DE BROMUROS DE ALQUILO O BROMUROS DE ALQUILENO PREFLUORADAS, QUE CONTIENEN COMPUESTOS DE YODO PERFLUORADOS, SON IRRADIADOS CON UNA RADIACION ELECTROMAGNETICA, EN LA BANDA DE LONGITUD DE ONDA DE 230 A 500 NM, Y BIEN DURANTE LA RADIACION O BIEN INMEDIATAMENTE DESPUES SE PONEN EN CONTACTO CON AL MENOS UNO DE LOS AGENTES SIGUIENTES: CARBONO ACTIVO, DETERMINADOS METALES EN PARTICULAS PEQUEÑAS, ALCOHOLES BAJOS ALIFATICOS, CLORO, BROMO, OXIGENO, PEROXIDO DE HIDROGENO, SOLUCIONES ACUOSAS O ALCOHOLICAS DE COMPUESTOS DE METALES ALCALINOS CON ANIONES DETERMINADOS INORGANICOS O CON ALCOHOLES BAJOS ALIFATICOS. DESPUES DE LA SEPARACION DEL MEDIO Y, DADO EL CASO, LA DESTILACION PUEDEN OBTENERSE COMPUESTOS DE YODO QUE CONTIENEN POR DEBAJO DE 0,0005% EN PESO Y QUE SON UTILIZABLES P. EJ. EN EL SECTOR MEDICO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4116121A DE4116121A1 (de) | 1991-05-17 | 1991-05-17 | Verfahren zur reinigung von gemischen, die im wesentlichen aus perfluorierten alkylbromiden oder alkylendibromiden bestehen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2082271T3 true ES2082271T3 (es) | 1996-03-16 |
Family
ID=6431845
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES92108147T Expired - Lifetime ES2082271T3 (es) | 1991-05-17 | 1992-05-14 | Procedimiento para la eliminacion de impurezas de bromuros de alquilo perfluorados o de dibromuros de alquileno perfluorados. |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5175380A (es) |
| EP (1) | EP0513783B1 (es) |
| JP (1) | JPH07206730A (es) |
| DE (2) | DE4116121A1 (es) |
| ES (1) | ES2082271T3 (es) |
| IE (1) | IE70515B1 (es) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2698094B1 (fr) * | 1992-11-18 | 1995-01-20 | Atochem Elf Sa | Purification du 1,1-dichloro-1-fluoroéthane. |
| FR2699531B1 (fr) * | 1992-12-17 | 1995-02-24 | Atochem Elf Sa | Synthèse d'un bromure de perfluoroalkyle par bromation photochimique de l'iodure correspondant. |
| DE4413658A1 (de) * | 1994-04-20 | 1995-10-26 | Hoechst Ag | Verfahren zur Reinigung von Perfluoralkylbromiden oder Perfluoralkylendibromiden |
| DE19942305C2 (de) | 1999-09-04 | 2001-06-28 | Solvay Fluor & Derivate | Herstellung hochreiner Fluorverbindungen |
| AU9379201A (en) * | 2000-08-10 | 2002-02-18 | Solvay | Process for obtaining a purified hydrofluoroalkane |
| US20080110833A1 (en) * | 2006-11-14 | 2008-05-15 | Samuels George J | Iodine removal with activated carbon |
| JP2019172709A (ja) * | 2019-07-17 | 2019-10-10 | ダイキン工業株式会社 | C8F17Brを含む組成物及びC8F17Brの製造方法 |
| CN115515918B (zh) * | 2020-05-15 | 2024-07-09 | 株式会社德山 | 有机化合物的纯化方法及有机化合物的制造方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1219460B (de) * | 1963-11-07 | 1966-06-23 | Hoechst Ag | Verfahren zur Reinigung von 2, 2, 2-Trifluor-1-chlor-1-bromaethan, welches als Verunreinigung 1, 1, 1, 4, 4, 4-Hexafluor-2, 3-dichlorbuten-2 enthaelt |
| CA1262346A (en) * | 1983-10-31 | 1989-10-17 | Thomas W. Bierl | Purification of fluorocarbons |
| IT1200594B (it) * | 1985-02-26 | 1989-01-27 | Montefluos Spa | Procedimento per la preparazione di alfa-omega-aloperfluorocarburi |
| US4801763A (en) * | 1987-07-27 | 1989-01-31 | Occidental Chemical Corporation | Selective chlorination of chlorotrifluoroethylene telomers |
| US4948479A (en) * | 1989-06-07 | 1990-08-14 | Atochem North America, Inc. | Removal of unsaturated carbon compounds from 1,1-dichloro-1-fluoroethane |
| DE3937567A1 (de) * | 1989-11-11 | 1991-05-16 | Hoechst Ag | Verfahren zur herstellung von weitgehend fluorierten alkylbromiden |
| JPH0684316B2 (ja) * | 1989-12-20 | 1994-10-26 | 株式会社トクヤマ | パーフルオロ化合物の安定化方法 |
| DE4004783A1 (de) * | 1990-02-16 | 1991-08-22 | Hoechst Ag | Verfahren zur herstellung von weitgehend fluorierten aliphatischen kohlenwasserstoffen, die 1 oder 2 brom- oder chloratome im molekuel aufweisen |
| DE4018913A1 (de) * | 1990-06-13 | 1991-12-19 | Hoechst Ag | Verfahren zur herstellung von weitgehend fluorierten alkylbromiden |
| DE4116361A1 (de) * | 1990-06-23 | 1992-01-02 | Hoechst Ag | Verfahren zur herstellung von perfluoralkylmonobromiden |
-
1991
- 1991-05-17 DE DE4116121A patent/DE4116121A1/de not_active Withdrawn
-
1992
- 1992-05-14 US US07/882,843 patent/US5175380A/en not_active Expired - Fee Related
- 1992-05-14 DE DE59204542T patent/DE59204542D1/de not_active Expired - Fee Related
- 1992-05-14 ES ES92108147T patent/ES2082271T3/es not_active Expired - Lifetime
- 1992-05-14 EP EP92108147A patent/EP0513783B1/de not_active Expired - Lifetime
- 1992-05-15 JP JP4123916A patent/JPH07206730A/ja not_active Withdrawn
- 1992-07-01 IE IE921576A patent/IE70515B1/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| US5175380A (en) | 1992-12-29 |
| DE59204542D1 (de) | 1996-01-18 |
| JPH07206730A (ja) | 1995-08-08 |
| IE921576A1 (en) | 1992-11-18 |
| EP0513783A3 (en) | 1994-06-01 |
| EP0513783A2 (de) | 1992-11-19 |
| IE70515B1 (en) | 1996-12-11 |
| EP0513783B1 (de) | 1995-12-06 |
| DE4116121A1 (de) | 1992-11-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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