ES2084929T3 - Eliminacion de impurezas de carbonilo de una corriente de un proceso de carbonilacion. - Google Patents
Eliminacion de impurezas de carbonilo de una corriente de un proceso de carbonilacion.Info
- Publication number
- ES2084929T3 ES2084929T3 ES92300647T ES92300647T ES2084929T3 ES 2084929 T3 ES2084929 T3 ES 2084929T3 ES 92300647 T ES92300647 T ES 92300647T ES 92300647 T ES92300647 T ES 92300647T ES 2084929 T3 ES2084929 T3 ES 2084929T3
- Authority
- ES
- Spain
- Prior art keywords
- waste
- elimination
- current
- carbonyl impurities
- recycling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical class [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 title abstract 2
- 239000012535 impurity Substances 0.000 title abstract 2
- 230000008030 elimination Effects 0.000 title 1
- 238000003379 elimination reaction Methods 0.000 title 1
- 239000002699 waste material Substances 0.000 abstract 3
- 238000004064 recycling Methods 0.000 abstract 2
- POQKXAGEBNZGTF-UHFFFAOYSA-N [C].CC(O)=O Chemical compound [C].CC(O)=O POQKXAGEBNZGTF-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 230000004048 modification Effects 0.000 abstract 1
- 238000012986 modification Methods 0.000 abstract 1
- 239000000376 reactant Substances 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
- C07C53/08—Acetic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
SE PRESENTA UN METODO PARA MEJORAR LA CALIDAD DEL RECICLADO DE CIERTOS RESIDUOS A BASE DE MODIFICAR LA SEPARACION DE MATERIALES ALCANOS Y TIPO ALCANO Y DE LAS IMPUREZAS QUE CONTIENEN CARBONILO DEL RECICLADO DURANTE LA PRODUCCION DE ACIDO ACETICO MEDIANTE LA CARBONILACION DE METANOL. LA MEJORA CONSISTE EN PONER EN FUNCIONAMIENTO UNA COLUMNA SEPARADORA DE LAS YA EXISTENTES A MODO DE REFLUJO Y SEPARAR EL RESIDUO DE LA MISMA A BASE DE AÑADIR AGUA. EL METODO REDUCE TAMBIEN EL VOLUMEN DE DESECHO DE REACTANTES RECICLABLES POTENCIALMENTE VALIOSOS.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US64691691A | 1991-01-28 | 1991-01-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2084929T3 true ES2084929T3 (es) | 1996-05-16 |
Family
ID=24594987
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES92300647T Expired - Lifetime ES2084929T3 (es) | 1991-01-28 | 1992-01-24 | Eliminacion de impurezas de carbonilo de una corriente de un proceso de carbonilacion. |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US5371286A (es) |
| EP (1) | EP0497521B1 (es) |
| JP (1) | JP3105326B2 (es) |
| KR (1) | KR100192733B1 (es) |
| CN (1) | CN1033386C (es) |
| AU (1) | AU639630B2 (es) |
| BR (1) | BR9200208A (es) |
| CA (1) | CA2060052C (es) |
| DE (1) | DE69209101T2 (es) |
| ES (1) | ES2084929T3 (es) |
| NO (1) | NO177745C (es) |
| RU (1) | RU2065850C1 (es) |
| SG (1) | SG49068A1 (es) |
| ZA (1) | ZA92575B (es) |
Families Citing this family (41)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR960007736B1 (ko) * | 1993-07-27 | 1996-06-11 | 한국과학기술연구원 | 원료 가스 중에 함유된 철 카르보닐 화합물의 제거 방법 |
| EP0665210B2 (en) * | 1993-08-18 | 2005-11-23 | Daicel Chemical Industries, Ltd. | Process for producing acetic anhydride alone or both of acetic anhydride and acetic acid |
| US5625095A (en) * | 1994-06-15 | 1997-04-29 | Daicel Chemical Industries, Ltd. | Process for producing high purity acetic acid |
| GB9503385D0 (en) * | 1995-02-21 | 1995-04-12 | Bp Chem Int Ltd | Process |
| US5599976A (en) * | 1995-04-07 | 1997-02-04 | Hoechst Celanese Corporation | Recovery of acetic acid from dilute aqueous streams formed during a carbonylation process |
| EP0768295B1 (en) * | 1995-04-27 | 2000-08-16 | Daicel Chemical Industries, Ltd. | Process for producing acetic acid |
| US5783731A (en) * | 1995-09-11 | 1998-07-21 | Hoechst Celanese Corporation | Removal of carbonyl impurities from a carbonylation process stream |
| DK136196A (da) * | 1996-11-29 | 1998-05-30 | Haldor Topsoe As | Fremgangsmåde til fremstilling af eddikesyre |
| GB9626324D0 (en) * | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9816385D0 (en) * | 1998-07-29 | 1998-09-23 | Bp Chem Int Ltd | Process |
| DE69915417T2 (de) * | 1998-08-06 | 2005-01-27 | Haldor Topsoe A/S | Reaktiv Distillierungsverfahren zur Herstellung von Essigsäure auf der Basis von DME/Methanol Carbonylierung |
| GB9819606D0 (en) * | 1998-09-08 | 1998-11-04 | Bp Chem Int Ltd | Carbonylation process |
| US6211405B1 (en) | 1998-10-23 | 2001-04-03 | Celanese International Corporation | Addition of iridium to the rhodium/inorganic iodide catalyst system |
| GB9825424D0 (en) * | 1998-11-19 | 1999-01-13 | Bp Chem Int Ltd | Process |
| US6552221B1 (en) | 1998-12-18 | 2003-04-22 | Millenium Petrochemicals, Inc. | Process control for acetic acid manufacture |
| US6251256B1 (en) | 1999-02-04 | 2001-06-26 | Celanese International Corporation | Process for electrochemical oxidation of an aldehyde to an ester |
| FR2795410B1 (fr) * | 1999-06-22 | 2002-12-27 | Acetex Chimie | Procede pour ameliorer la stabilite et/ou eviter la desactivation du catalyseur lors de la fabrication d'acide acetique et/ou d'acetate de methyle |
| US6346645B1 (en) | 2000-04-18 | 2002-02-12 | Uop Llc | Adsorptive removal of carbonyl impurities from oxygenated organic liquids |
| RU2238931C2 (ru) * | 2002-11-06 | 2004-10-27 | Государственный научно-исследовательский и проектный институт химических технологий "Химтехнология" | Способ очистки цикла синтеза уксусной кислоты от углеводородов |
| US7223883B2 (en) * | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
| US7208624B2 (en) * | 2004-03-02 | 2007-04-24 | Celanese International Corporation | Process for producing acetic acid |
| US7855306B2 (en) | 2005-04-28 | 2010-12-21 | Celanese International Corporation | Process for the production of acetic acid |
| US7524988B2 (en) * | 2006-08-01 | 2009-04-28 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
| US7208625B1 (en) | 2006-08-04 | 2007-04-24 | Lyondell Chemical Technology, L.P. | Removing permanganate-reducing impurities from acetic acid |
| US7485749B2 (en) * | 2006-08-22 | 2009-02-03 | Lyondell Chemical Technology, L.P. | Preparation of acetic acid |
| US7989659B2 (en) * | 2007-05-17 | 2011-08-02 | Celanese International Corporation | Method and apparatus for making acetic acid with improved light ends column productivity |
| US8076512B2 (en) * | 2009-08-27 | 2011-12-13 | Equistar Chemicals, L.P. | Preparation of acetic acid |
| US9090554B2 (en) | 2011-12-21 | 2015-07-28 | Lyondellbasell Acetyls, Llc | Process for the manufacture of acetic acid |
| US9051258B2 (en) | 2011-12-21 | 2015-06-09 | Lyondellbasell Acetyls, Llc | Process for the manufacture of acetic acid |
| RU2680101C2 (ru) * | 2014-06-20 | 2019-02-15 | Бп Кемикэлз Лимитед | Способ очистки смесей метилацетата |
| US9302975B1 (en) * | 2015-07-01 | 2016-04-05 | Celanese International Corporation | Process for flashing a reaction medium |
| KR102465649B1 (ko) | 2014-11-14 | 2022-11-11 | 셀라니즈 인터내셔날 코포레이션 | 낮은 요오드화에틸 함량을 갖는 반응 매질로부터 아세트산을 제조하기 위한 방법 |
| MX2018015918A (es) * | 2016-07-07 | 2019-05-02 | Daicel Corp | Procedimiento para producir acido acetico. |
| KR102281510B1 (ko) * | 2017-03-22 | 2021-07-26 | 주식회사 다이셀 | 아세트산의 제조 방법 |
| DE102017211435A1 (de) * | 2017-07-05 | 2019-01-10 | Evonik Röhm Gmbh | Verfahren zum kontinuierlichen Lösen eines Feststoffes in einem Reaktionsmedium |
| ES2867879T3 (es) | 2018-05-15 | 2021-10-21 | Daicel Corp | Método de producción de ácido acético |
| EP3792244B1 (en) | 2018-05-29 | 2022-07-27 | Daicel Corporation | Method for producing acetic acid |
| CN110325503B (zh) * | 2018-05-29 | 2023-05-02 | 株式会社大赛璐 | 乙酸的制备方法 |
| WO2019229857A1 (ja) * | 2018-05-29 | 2019-12-05 | 株式会社ダイセル | 酢酸の製造方法 |
| WO2019229856A1 (ja) | 2018-05-29 | 2019-12-05 | 株式会社ダイセル | 酢酸の製造方法 |
| US20230375478A1 (en) | 2022-05-19 | 2023-11-23 | Lyondellbasell Acetyls, Llc | Methods for improved control of glacial acetic acid processes |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB334189A (en) * | 1929-05-27 | 1930-08-27 | British Celanese | Manufacture of aliphatic compounds |
| US4102922A (en) * | 1974-12-30 | 1978-07-25 | Monsanto Company | Purification of carbonylation products |
-
1992
- 1992-01-21 AU AU10366/92A patent/AU639630B2/en not_active Ceased
- 1992-01-23 BR BR929200208A patent/BR9200208A/pt not_active IP Right Cessation
- 1992-01-24 EP EP92300647A patent/EP0497521B1/en not_active Expired - Lifetime
- 1992-01-24 SG SG1996005730A patent/SG49068A1/en unknown
- 1992-01-24 DE DE69209101T patent/DE69209101T2/de not_active Expired - Fee Related
- 1992-01-24 ES ES92300647T patent/ES2084929T3/es not_active Expired - Lifetime
- 1992-01-27 RU SU925010845A patent/RU2065850C1/ru active
- 1992-01-27 JP JP04011747A patent/JP3105326B2/ja not_active Expired - Fee Related
- 1992-01-27 NO NO920349A patent/NO177745C/no not_active IP Right Cessation
- 1992-01-27 KR KR1019920001132A patent/KR100192733B1/ko not_active Expired - Fee Related
- 1992-01-27 CA CA002060052A patent/CA2060052C/en not_active Expired - Fee Related
- 1992-01-28 CN CN92100678A patent/CN1033386C/zh not_active Expired - Fee Related
- 1992-01-28 ZA ZA92575A patent/ZA92575B/xx unknown
-
1993
- 1993-04-26 US US08/052,429 patent/US5371286A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE69209101D1 (de) | 1996-04-25 |
| AU1036692A (en) | 1992-07-30 |
| AU639630B2 (en) | 1993-07-29 |
| NO177745C (no) | 1995-11-15 |
| EP0497521B1 (en) | 1996-03-20 |
| CA2060052A1 (en) | 1992-07-29 |
| US5371286A (en) | 1994-12-06 |
| BR9200208A (pt) | 1992-10-06 |
| KR920014754A (ko) | 1992-08-25 |
| RU2065850C1 (ru) | 1996-08-27 |
| ZA92575B (en) | 1993-07-28 |
| CN1063865A (zh) | 1992-08-26 |
| CN1033386C (zh) | 1996-11-27 |
| JPH04295445A (ja) | 1992-10-20 |
| NO920349L (no) | 1992-07-29 |
| KR100192733B1 (ko) | 1999-06-15 |
| EP0497521A2 (en) | 1992-08-05 |
| NO920349D0 (no) | 1992-01-27 |
| EP0497521A3 (en) | 1993-01-13 |
| DE69209101T2 (de) | 1996-08-29 |
| JP3105326B2 (ja) | 2000-10-30 |
| CA2060052C (en) | 2003-01-07 |
| NO177745B (no) | 1995-08-07 |
| SG49068A1 (en) | 1998-05-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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