ES2088114T3 - Procedimiento para la separacion de fluoruro de hidrogeno de sus mezclas con el 1,1,1-trifluor-2-cloroetano. - Google Patents
Procedimiento para la separacion de fluoruro de hidrogeno de sus mezclas con el 1,1,1-trifluor-2-cloroetano.Info
- Publication number
- ES2088114T3 ES2088114T3 ES92401005T ES92401005T ES2088114T3 ES 2088114 T3 ES2088114 T3 ES 2088114T3 ES 92401005 T ES92401005 T ES 92401005T ES 92401005 T ES92401005 T ES 92401005T ES 2088114 T3 ES2088114 T3 ES 2088114T3
- Authority
- ES
- Spain
- Prior art keywords
- chloroethane
- mixtures
- separation
- hydrogen fluoride
- trifluor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 title abstract 8
- 229910000040 hydrogen fluoride Inorganic materials 0.000 title abstract 7
- 239000000203 mixture Substances 0.000 title abstract 3
- CYXIKYKBLDZZNW-UHFFFAOYSA-N 2-Chloro-1,1,1-trifluoroethane Chemical compound FC(F)(F)CCl CYXIKYKBLDZZNW-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000926 separation method Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- 238000004821 distillation Methods 0.000 abstract 2
- 239000012071 phase Substances 0.000 abstract 2
- 238000003682 fluorination reaction Methods 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
- C01B7/195—Separation; Purification
- C01B7/196—Separation; Purification by distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
- C01B7/195—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
LA INVENCION SE REFIERE A LA SEPARACION DEL FLUORURO DE HIDROGENO (HF) DE SUS MEZCLAS CON EL 1,1,1-TRIFLUORO-2-CLOROETANO (F133A). POR DECANTACION DE LA MEZCLA DE HF Y DE F133A A UNA TEMPERATURA INFERIOR A 0 (GRADOS) C, SE OBTIENE UNA FASE INFERIOR ORGANICA POBRE EN HF Y UNA FASE SUPERIOR RICA EN HF. ESTA ULTIMA PUEDE SER DIRECTAMENTE RECICLADA EN EL REACTOR DE FLUORACION O SOMETIDA A UNA DESTILACION PARA SEPARAR EN CABEZA EL AZEOTROPO HF-F133A QUE SE REENVIA AL DECANTADOR Y RECUPERAR EN PIE EL HF PRACTICAMENTE PURO. POR DESTILACION DE LA FASE INFERIOR, SE SEPARA EN CABEZA EL AZEOTROPO HF-F133A QUE SE REENVIA AL DECANTADOR Y SE RECUPERA EN PIE EL F133A.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9104736A FR2675496B1 (fr) | 1991-04-17 | 1991-04-17 | Procede de separation du fluorure d'hydrogene de ses melanges avec le 1,1,1-trifluoro-2-chloroethane. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2088114T3 true ES2088114T3 (es) | 1996-08-01 |
Family
ID=9411958
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES92401005T Expired - Lifetime ES2088114T3 (es) | 1991-04-17 | 1992-04-09 | Procedimiento para la separacion de fluoruro de hidrogeno de sus mezclas con el 1,1,1-trifluor-2-cloroetano. |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0509885B1 (es) |
| JP (1) | JPH06135867A (es) |
| AT (1) | ATE139513T1 (es) |
| AU (1) | AU650333B2 (es) |
| CA (1) | CA2065952A1 (es) |
| ES (1) | ES2088114T3 (es) |
| FR (1) | FR2675496B1 (es) |
| GR (1) | GR3020642T3 (es) |
| MX (1) | MX9201720A (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5401430A (en) * | 1991-04-15 | 1995-03-28 | Daikin Industries, Ltd. | Azeotropic mixture of hydrogen fluoride and 1,1,1-trifluoro-2-chloroethane |
| JPH05255144A (ja) * | 1991-11-15 | 1993-10-05 | Hoechst Ag | 弗化水素および1−クロロ−2,2,2−トリフルオロエタンを含有する混合物の分離方法 |
| FR2695386B1 (fr) * | 1992-09-10 | 1994-10-14 | Atochem Elf Sa | Procédé de séparation de fluorure d'hydrogène de ses mélanges avec le 1,1,1-trifluoro-2-chloroéthane. |
| GB9305148D0 (en) * | 1993-03-12 | 1993-04-28 | Ici Plc | Hydrogen fluoride recovery process |
| US5800795A (en) * | 1993-03-12 | 1998-09-01 | Imperial Chemical Industries Plc | Hydrogen fluoride recovery process |
| JP2933014B2 (ja) | 1996-01-23 | 1999-08-09 | ダイキン工業株式会社 | ペンタフルオロプロパンとフッ化水素の共沸混合物およびペンタフルオロプロパンの分離精製方法 |
| GB9707176D0 (en) * | 1997-04-09 | 1997-05-28 | Ici Plc | Hydrogen fluoride recovery process |
| AU3377899A (en) * | 1998-04-03 | 1999-10-25 | E.I. Du Pont De Nemours And Company | Processes for the purification and use of 2,2-dichloro-1,1,1,3,3,3-hexafluoropropane and azeotropes thereof with hf |
| DE69911186T2 (de) * | 1998-04-03 | 2004-07-15 | E.I. Du Pont De Nemours And Co., Wilmington | Verfahren zur reinigung und verwendung von 2-chloro-1,1,1,2,3,3,3-heptafluorpropan und ihre azeotrope mit hf |
| AU769137B2 (en) * | 1999-05-18 | 2004-01-15 | Ineos Fluor Holdings Limited | Production of 1,1,1,2,3,3,3-heptafluoropropane |
| CN101541715B (zh) * | 2006-08-24 | 2013-09-11 | 纳幕尔杜邦公司 | 通过共沸蒸馏将氟代烯烃与氟化氢分离的方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2414475A1 (fr) * | 1978-01-13 | 1979-08-10 | Solvay | Procede pour la separation du fluorure d'hydrogene de ses melanges avec le 1-chloro-1, 1-difluorethane |
| DE3362972D1 (en) * | 1982-06-08 | 1986-05-22 | Pennwalt Corp | Anhydrous phase separation for recovering hydrogen fluoride from a fluorination reaction |
| US4911797A (en) * | 1983-06-24 | 1990-03-27 | American Cyanamid Company | Contact roller mounting assembly and tensioning mechanism for electroplating fiber |
| US4944846A (en) * | 1988-08-01 | 1990-07-31 | E. I. Dupont De Nemours And Company | Process for the separation of HF via Azeotropic distillation |
| US4911792A (en) * | 1988-08-01 | 1990-03-27 | E. I. Du Pont De Nemours And Company | Process for the separation of HF via phase separation and distillation |
| JP3175286B2 (ja) * | 1991-04-15 | 2001-06-11 | ダイキン工業株式会社 | フッ化水素と1,1,1−トリフルオロ−2−クロロエタンの共沸混合物および1,1,1−トリフルオロ−2−クロロエタンの精製方法 |
-
1991
- 1991-04-17 FR FR9104736A patent/FR2675496B1/fr not_active Expired - Lifetime
-
1992
- 1992-04-09 EP EP92401005A patent/EP0509885B1/fr not_active Expired - Lifetime
- 1992-04-09 ES ES92401005T patent/ES2088114T3/es not_active Expired - Lifetime
- 1992-04-09 AT AT92401005T patent/ATE139513T1/de not_active IP Right Cessation
- 1992-04-13 MX MX9201720A patent/MX9201720A/es unknown
- 1992-04-14 CA CA002065952A patent/CA2065952A1/fr not_active Abandoned
- 1992-04-16 AU AU14971/92A patent/AU650333B2/en not_active Ceased
- 1992-04-17 JP JP4098277A patent/JPH06135867A/ja active Pending
-
1996
- 1996-07-26 GR GR960401998T patent/GR3020642T3/el unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0509885B1 (fr) | 1996-06-19 |
| EP0509885A3 (fr) | 1992-12-09 |
| JPH06135867A (ja) | 1994-05-17 |
| EP0509885A2 (fr) | 1992-10-21 |
| AU1497192A (en) | 1992-10-22 |
| ATE139513T1 (de) | 1996-07-15 |
| MX9201720A (es) | 1992-10-01 |
| CA2065952A1 (fr) | 1992-10-18 |
| GR3020642T3 (en) | 1996-10-31 |
| FR2675496A1 (fr) | 1992-10-23 |
| AU650333B2 (en) | 1994-06-16 |
| FR2675496B1 (fr) | 1993-09-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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