ES2098596T3 - Procedimiento para la obtencion del acido 1,4-diaminoantraquinona-2,3-disulfonico y del 1,4-diaminoantraquinona-2,3-dinitrilo. - Google Patents

Procedimiento para la obtencion del acido 1,4-diaminoantraquinona-2,3-disulfonico y del 1,4-diaminoantraquinona-2,3-dinitrilo.

Info

Publication number
ES2098596T3
ES2098596T3 ES93110227T ES93110227T ES2098596T3 ES 2098596 T3 ES2098596 T3 ES 2098596T3 ES 93110227 T ES93110227 T ES 93110227T ES 93110227 T ES93110227 T ES 93110227T ES 2098596 T3 ES2098596 T3 ES 2098596T3
Authority
ES
Spain
Prior art keywords
diaminoantraquinone
obtaining
disulphonic acid
dinitrile
procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES93110227T
Other languages
English (en)
Inventor
Matthias Dr Dust
Udo Dr Bergmann
Gerd Dr Schwantje
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2098596T3 publication Critical patent/ES2098596T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/01—Sulfonic acids
    • C07C309/28—Sulfonic acids having sulfo groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
    • C07C309/33—Sulfonic acids having sulfo groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton of six-membered aromatic rings being part of condensed ring systems
    • C07C309/38—Sulfonic acids having sulfo groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton of six-membered aromatic rings being part of condensed ring systems formed by at least three rings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
    • C09B1/16—Amino-anthraquinones
    • C09B1/20—Preparation from starting materials already containing the anthracene nucleus
    • C09B1/22—Dyes with unsubstituted amino groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/16—Preparation of carboxylic acid nitriles by reaction of cyanides with lactones or compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
    • C09B1/16—Amino-anthraquinones
    • C09B1/20—Preparation from starting materials already containing the anthracene nucleus
    • C09B1/22—Dyes with unsubstituted amino groups
    • C09B1/24—Dyes with unsubstituted amino groups sulfonated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
    • C07C2603/22—Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
    • C07C2603/24—Anthracenes; Hydrogenated anthracenes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

OBTENCION DE ACIDO 1,4-DIAMINOANTRAQUINONA -2,3-DISULFONICO A TRAVES DE HACER REACCIONAR UNAS 1,4-DIAMINO-2,3-DIHALOGENOANTRAQUINONAS DE FORMULA (II) CON ACIDO BORICO EN UN DISOLVENTE Y POSTERIORMENTE TRANSFORMACION DEL PRODUCTO DE REACCION (IIA) OBTENIDO CON UNA SOLUCION ACUOSA DE SULFITO , EN EL CUAL COMO DISOLVENTE ORGANICO INERTE SE EMPLEA UN DISOLVENTE NO POLAR CON UN PUNTO DE EBULLICION MAS/MENOS 130 C Y UNA DENSIDAD MAS/MENOS DE 0,95 G/CM(3).ASI COMO LA OBTENCION DEL 1,4-DIAMINO-ANTRAQUINONA -2,3DINITRILO A TRAVES DE LA TRANSFORMACION DEL ACIDO 1,4DIAMINOANTRAQUINONA -2,3-DISULFONICO DE FORMULA (I) CON CIANURO
ES93110227T 1992-07-08 1993-06-26 Procedimiento para la obtencion del acido 1,4-diaminoantraquinona-2,3-disulfonico y del 1,4-diaminoantraquinona-2,3-dinitrilo. Expired - Lifetime ES2098596T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4222302A DE4222302A1 (de) 1992-07-08 1992-07-08 Verfahren zur Herstellung von 1,4-Diaminoanthrachinon-2,3-disulfonsäure und 1,4-Diaminoanthrachinon-2,3-dinitril

Publications (1)

Publication Number Publication Date
ES2098596T3 true ES2098596T3 (es) 1997-05-01

Family

ID=6462681

Family Applications (1)

Application Number Title Priority Date Filing Date
ES93110227T Expired - Lifetime ES2098596T3 (es) 1992-07-08 1993-06-26 Procedimiento para la obtencion del acido 1,4-diaminoantraquinona-2,3-disulfonico y del 1,4-diaminoantraquinona-2,3-dinitrilo.

Country Status (7)

Country Link
US (1) US5386042A (es)
EP (1) EP0582079B1 (es)
JP (1) JPH06179647A (es)
KR (1) KR100268980B1 (es)
CN (2) CN1052719C (es)
DE (2) DE4222302A1 (es)
ES (1) ES2098596T3 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1069896C (zh) * 1997-01-28 2001-08-22 常州市合成材料厂 1,4-二氨基-2,3-二氰基蒽醌的制备工艺
CN103242208B (zh) * 2013-05-03 2015-01-07 盐城市瓯华化学工业有限公司 烟酸法制备1,4-二氨基蒽醌-2,3-二磺酸的工艺
CN115521636B (zh) * 2022-10-24 2023-06-30 浙江博澳新材料股份有限公司 一种含双氰基耐晒型蒽醌分散染料及其制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1975386A (en) * 1932-03-26 1934-10-02 Gen Aniline Works Inc Process of preparing 1.4-diamino-anthraquinone-2.3-disulphonic acid
US2795593A (en) * 1953-07-22 1957-06-11 Du Pont Process for preparing alkali metal salts of 1, 4-diamino-2, 3-anthraquinone-disulfonic acid
DE2524748C3 (de) * 1975-06-04 1980-06-04 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von 1 ^-Diaminoanthrachinon^-dinitril
DE2846622A1 (de) * 1978-10-26 1980-05-08 Bayer Ag Verfahren zur herstellung von 1,4-diaminoanthrachinon-2,3-disulfonsaeure
JPS57158261A (en) * 1981-03-26 1982-09-30 Sumitomo Chem Co Ltd Preparation of 1,4-diamino anthraquinone-2,3-disulfonic acid
JPS58172364A (ja) * 1982-04-02 1983-10-11 Sumitomo Chem Co Ltd １，４−ジアミノアントラキノン−２，３−ジスルホン酸の製造方法
GB2185035B (en) * 1986-01-07 1989-11-08 Sumitomo Chemical Co Process for preparing 1,4-diaminoanthraquinone-2,3-disubstituted compound

Also Published As

Publication number Publication date
KR100268980B1 (en) 2000-10-16
DE4222302A1 (de) 1994-01-13
CN1085210A (zh) 1994-04-13
US5386042A (en) 1995-01-31
CN1052719C (zh) 2000-05-24
EP0582079B1 (de) 1997-03-12
DE59305709D1 (de) 1997-04-17
KR940005563A (ko) 1994-03-21
JPH06179647A (ja) 1994-06-28
CN1079392C (zh) 2002-02-20
EP0582079A1 (de) 1994-02-09
CN1218798A (zh) 1999-06-09

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