ES2106441T3 - Procedimiento para la preparacion de dibencilamina. - Google Patents
Procedimiento para la preparacion de dibencilamina.Info
- Publication number
- ES2106441T3 ES2106441T3 ES94202692T ES94202692T ES2106441T3 ES 2106441 T3 ES2106441 T3 ES 2106441T3 ES 94202692 T ES94202692 T ES 94202692T ES 94202692 T ES94202692 T ES 94202692T ES 2106441 T3 ES2106441 T3 ES 2106441T3
- Authority
- ES
- Spain
- Prior art keywords
- dibencilamine
- preparation
- benzaldehyde
- catalyst
- procedure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title abstract 5
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 abstract 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 abstract 2
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000002612 dispersion medium Substances 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 230000035484 reaction time Effects 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
- C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
LA INVENCION SE REFIERE A UN PROCESO PARA LA PREPARACION DE DIBENCILAMINA POR HIDROGENACION DE BENZALDEHIDO EN PRESENCIA DE AMONIACO Y UN CATALIZADOR CON PALADIO USANDO UNA PEQUEÑA CANTIDAD DE SOLVENTE O MEDIO DE DISPERSION. CON ESTE PROCESO LA DIBENCILAMINA PUEDE PREPARARSE CON ALTA SELECTIVIDAD EN UN TIEMPO DE REACCION RELATIVAMENTE CORTO Y CON CONVERSION COMPLETA DEL BENZALDEHIDO EN UN PROCESO PARTICULARMENTE ATRACTIVO DESDE UN PUNTO DE VISTA COMERCIAL. EN ESTE PROCESO SE UTILIZA PREFERENTEMENTE UN CATALIZADOR DE PALADIOCARBON.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE9300975A BE1007529A3 (nl) | 1993-09-20 | 1993-09-20 | Werkwijze voor de bereiding van dibenzylamine. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2106441T3 true ES2106441T3 (es) | 1997-11-01 |
Family
ID=3887343
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES94202692T Expired - Fee Related ES2106441T3 (es) | 1993-09-20 | 1994-09-19 | Procedimiento para la preparacion de dibencilamina. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5616804A (es) |
| EP (1) | EP0644177B1 (es) |
| BE (1) | BE1007529A3 (es) |
| DE (1) | DE69404103T2 (es) |
| ES (1) | ES2106441T3 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10228594B4 (de) * | 2002-06-26 | 2006-06-08 | Lanxess Deutschland Gmbh | Herstellung von farblosem Dibenzylamin |
| CN102503836A (zh) * | 2011-10-11 | 2012-06-20 | 浙江新化化工股份有限公司 | 一种二苄胺的制备方法 |
| JP2014043415A (ja) * | 2012-08-27 | 2014-03-13 | Koei Chem Co Ltd | ジベンジルアミンの製造方法 |
| KR20200065723A (ko) | 2018-11-30 | 2020-06-09 | 롯데케미칼 주식회사 | 다이벤질아민의 제조방법 |
| CN111039794A (zh) * | 2019-12-30 | 2020-04-21 | 山东省越兴化工有限公司 | 一种高纯度二苄胺的制备方法 |
| CN120271452B (zh) * | 2025-03-18 | 2026-04-10 | 江苏济业医药化工有限公司 | 一种二苄胺的制备方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3597438A (en) * | 1968-05-06 | 1971-08-03 | Du Pont | Reductive amination of aldehydes with rhodium catalysts |
| US4163025A (en) * | 1975-01-16 | 1979-07-31 | Miles Laboratories, Inc. | Process for the production of benzylamine and dibenzylamine |
| US5266730A (en) * | 1987-10-16 | 1993-11-30 | Kao Corporation | Process for preparing N-substituted amine |
| US5430187A (en) * | 1991-12-21 | 1995-07-04 | Akzo N.V. | Method for manufacturing dibenzylamine |
-
1993
- 1993-09-20 BE BE9300975A patent/BE1007529A3/nl not_active IP Right Cessation
-
1994
- 1994-09-19 EP EP94202692A patent/EP0644177B1/en not_active Expired - Lifetime
- 1994-09-19 ES ES94202692T patent/ES2106441T3/es not_active Expired - Fee Related
- 1994-09-19 DE DE69404103T patent/DE69404103T2/de not_active Expired - Fee Related
-
1995
- 1995-11-17 US US08/560,510 patent/US5616804A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE69404103T2 (de) | 1998-02-05 |
| US5616804A (en) | 1997-04-01 |
| BE1007529A3 (nl) | 1995-07-25 |
| EP0644177B1 (en) | 1997-07-09 |
| EP0644177A1 (en) | 1995-03-22 |
| DE69404103D1 (de) | 1997-08-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EC2A | Search report published |
Date of ref document: 19950601 Kind code of ref document: R Effective date: 19950601 |
|
| FG2A | Definitive protection |
Ref document number: 644177 Country of ref document: ES |
|
| FD1A | Patent lapsed |
Effective date: 20000403 |