ES2110290T3 - Proceso para recuperar dipropilenglicol-terc-butil-eteres. - Google Patents
Proceso para recuperar dipropilenglicol-terc-butil-eteres.Info
- Publication number
- ES2110290T3 ES2110290T3 ES95300945T ES95300945T ES2110290T3 ES 2110290 T3 ES2110290 T3 ES 2110290T3 ES 95300945 T ES95300945 T ES 95300945T ES 95300945 T ES95300945 T ES 95300945T ES 2110290 T3 ES2110290 T3 ES 2110290T3
- Authority
- ES
- Spain
- Prior art keywords
- dptb
- dipropylene glycol
- glycol
- purify
- dipropilenglicol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 4
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 abstract 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- BLIDAHWLLQVLLU-UHFFFAOYSA-N 1-(1-hydroxypropan-2-yloxy)-4,4-dimethylpentan-2-ol Chemical compound OCC(C)OCC(O)CC(C)(C)C BLIDAHWLLQVLLU-UHFFFAOYSA-N 0.000 abstract 1
- -1 BUTYL Chemical class 0.000 abstract 1
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000037213 diet Effects 0.000 abstract 1
- 235000005911 diet Nutrition 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/34—Separation; Purification; Stabilisation; Use of additives
- C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
- C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/17—Saline water conversion
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
SE DESCRIBE UN PROCESO PARA PURIFICAR ETERES TERT-BUTILO DE DIPROPILENO GLICOL (DPTB). EL DPTB SE HACE REACCIONANDO DIPROPILENO GLICOL CON ISOBUTILENO EN LA PRESENCIA DE UN CATALIZADOR ACIDO Y LA MEZCLA DEL PRODUCTO INCLUYE IMPUREZAS DE ETER BUTILO DI-TERCIARIO DERIVADAS DE DIPROPILENO GLICOL. EL PROCESO DE PURIFICACION COMPRENDE DESTILACION EXTRACTORA DE LA MEZCLA DEL PRODUCTO USANDO UN AGENTE EXTRACTOR DE GLICOL, PREFERIBLEMENTE DIPROPILENO GLICOL, QUE PERMITE LA ELIMINACION DE IMPUREZAS DE ETER DITERT-BUTILO COMO UN PRODUCTO EVAPORADO, Y LA DESTILACION DEL PRODUCTO DPTB PARA SEPARARLO DEL AGENTE EXTRACTOR DE GLICOL. DPTB DE ALTA PUREZA, SUSTANCIALMENTE EXENTO DE DIETERES Y EXCEPCIONALMENTE USADO COMO UN DISOLVENTE, ES OBTENIDO DEL PROCESO. EL PROCESO PARA FORMAR EL DPTB Y ENTONCES PURIFICARLO TAMBIEN SE DESCRIBE.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/203,162 US5552024A (en) | 1994-02-28 | 1994-02-28 | Process for recovering dipropylene glycol tert-butyl ethers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2110290T3 true ES2110290T3 (es) | 1998-02-01 |
Family
ID=22752772
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES95300945T Expired - Lifetime ES2110290T3 (es) | 1994-02-28 | 1995-02-15 | Proceso para recuperar dipropilenglicol-terc-butil-eteres. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5552024A (es) |
| EP (1) | EP0669307B1 (es) |
| JP (1) | JPH07258135A (es) |
| AU (1) | AU680709B2 (es) |
| CA (1) | CA2143407A1 (es) |
| DE (1) | DE69501120T2 (es) |
| ES (1) | ES2110290T3 (es) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5723683A (en) * | 1996-03-12 | 1998-03-03 | Arco Chemical Technology, L.P. | Separation of monoethers from diethers |
| US6306263B1 (en) * | 1999-03-31 | 2001-10-23 | Arco Chemical Technology, L.P. | Impurities separation by distillation |
| US6264800B1 (en) * | 2000-07-19 | 2001-07-24 | Arco Chemical Technology, L.P. | Purification process |
| US8269049B2 (en) * | 2009-12-31 | 2012-09-18 | Chinese Petroleum Corp. | Method of producing diethylene-glycol tert-butyl ether using isobutylene and diethylene glycol |
| KR101187574B1 (ko) * | 2010-06-14 | 2012-10-05 | 대림산업 주식회사 | 글리콜 모노-터셔리-부틸에테르와 글리콜 디-터셔리-부틸에테르 혼합물의 분리 방법 |
| KR101331553B1 (ko) * | 2011-02-18 | 2013-11-20 | 대림산업 주식회사 | 글리콜에테르를 이용한 고순도 이소부텐의 제조 방법 |
| KR101331551B1 (ko) | 2011-02-22 | 2013-11-20 | 대림산업 주식회사 | 글리콜 모노-터셔리-부틸에테르 화합물의 제조 방법 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2927064A (en) * | 1958-03-11 | 1960-03-01 | Union Carbide Corp | Refining of alpha-methylbenzyl ether |
| GB981943A (en) * | 1962-07-27 | 1965-02-03 | Ici Ltd | Separation of ethers from distillation residues of synthetic alcohols |
| US3578568A (en) * | 1968-11-29 | 1971-05-11 | Atlantic Richfield Co | Purification of low molecular weight epoxides by extractive distillation with a glycol or glycol ether |
| JPS4880507A (es) * | 1972-02-05 | 1973-10-29 | ||
| JPS6034936B2 (ja) * | 1978-08-30 | 1985-08-12 | 丸善石油株式会社 | エチレングライコ−ルモノタ−シャリ−ブチルエ−テルの製造方法 |
| US4254246A (en) * | 1979-03-26 | 1981-03-03 | Davy International Ag | Column system process for polyester plants |
| US4551207A (en) * | 1983-01-06 | 1985-11-05 | Lloyd Berg | Separation of isopropyl ether from acetone by extractive distillation |
| US4510022A (en) * | 1983-08-08 | 1985-04-09 | Lloyd Berg | Separation of isopropyl ether from isopropanol and water by extractive distillation |
| US4585526A (en) * | 1984-04-11 | 1986-04-29 | Lloyd Berg | Separation of m-xylene from o-xylene by extractive distillation |
| US4709101A (en) * | 1985-09-30 | 1987-11-24 | Allied Corporation | Process for the production of methyl ethers from branched monoolefins |
| US4666563A (en) * | 1985-11-20 | 1987-05-19 | Lloyd Berg | Separation of isopropyl ether from isopropanol and water by extractive distillation |
| DE3629233A1 (de) * | 1986-08-28 | 1988-03-10 | Erdoelchemie Gmbh | Verfahren zur katalytischen umsetzung von isoolefinen |
| US4675082A (en) * | 1986-09-22 | 1987-06-23 | Atlantic Richfield Company | Recovery of propylene glycol mono t-butoxy ether |
| US4855531A (en) * | 1988-11-29 | 1989-08-08 | Lloyd Berg | Separation of M-diisopropylbenzene from p-diisoporopylbenzene by azeotropic distillation with ethers |
| US4897161A (en) * | 1989-03-20 | 1990-01-30 | Lloyd Berg | Separation of vinyl acetate from ethyl acetate by extractive distillation |
| DE3923291A1 (de) * | 1989-07-14 | 1991-01-24 | Erdoelchemie Gmbh | Verfahren zur herstellung von reinen c(pfeil abwaerts)4(pfeil abwaerts)-c(pfeil abwaerts)7(pfeil abwaerts)-tert.-alkenen |
| US5152876A (en) * | 1991-03-27 | 1992-10-06 | Lloyd Berg | Separation of methylene chloride from the lower alcohols by extractive distillation |
| US5160414A (en) * | 1991-07-19 | 1992-11-03 | Phillips Petroleum Company | Extractive distillation of alcohol/ether/hydrocarbon mixtures |
| US5160585A (en) * | 1991-07-23 | 1992-11-03 | Lloyd Berg | Separation of tetrachloroethylene from a butyl alcohol by extractive distillation |
-
1994
- 1994-02-28 US US08/203,162 patent/US5552024A/en not_active Expired - Fee Related
-
1995
- 1995-02-15 ES ES95300945T patent/ES2110290T3/es not_active Expired - Lifetime
- 1995-02-15 EP EP95300945A patent/EP0669307B1/en not_active Expired - Lifetime
- 1995-02-15 DE DE69501120T patent/DE69501120T2/de not_active Expired - Fee Related
- 1995-02-17 JP JP7052110A patent/JPH07258135A/ja active Pending
- 1995-02-23 AU AU13465/95A patent/AU680709B2/en not_active Ceased
- 1995-02-24 CA CA002143407A patent/CA2143407A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| US5552024A (en) | 1996-09-03 |
| DE69501120T2 (de) | 1998-03-26 |
| EP0669307B1 (en) | 1997-12-03 |
| AU1346595A (en) | 1995-09-07 |
| EP0669307A1 (en) | 1995-08-30 |
| DE69501120D1 (de) | 1998-01-15 |
| CA2143407A1 (en) | 1995-08-29 |
| JPH07258135A (ja) | 1995-10-09 |
| AU680709B2 (en) | 1997-08-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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