ES212646A2 - Un procedimiento de preparar 2-benzotiazolil sulfeno morfolida - Google Patents
Un procedimiento de preparar 2-benzotiazolil sulfeno morfolidaInfo
- Publication number
- ES212646A2 ES212646A2 ES0212646A ES212646A ES212646A2 ES 212646 A2 ES212646 A2 ES 212646A2 ES 0212646 A ES0212646 A ES 0212646A ES 212646 A ES212646 A ES 212646A ES 212646 A2 ES212646 A2 ES 212646A2
- Authority
- ES
- Spain
- Prior art keywords
- morpholine
- chloromorpholine
- toluene
- acid acceptor
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 2-benzothiazolyl sulfene Chemical compound 0.000 title 1
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 abstract 14
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 9
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 4
- ILNGCUVXLQVDTC-UHFFFAOYSA-N 4-chloromorpholine Chemical compound ClN1CCOCC1 ILNGCUVXLQVDTC-UHFFFAOYSA-N 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 3
- 235000019270 ammonium chloride Nutrition 0.000 abstract 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 abstract 2
- AFZSMODLJJCVPP-UHFFFAOYSA-N dibenzothiazol-2-yl disulfide Chemical compound C1=CC=C2SC(SSC=3SC4=CC=CC=C4N=3)=NC2=C1 AFZSMODLJJCVPP-UHFFFAOYSA-N 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- RPAJWWXZIQJVJF-UHFFFAOYSA-N 2,4-dichloro-6-(3,5-dichloro-2-hydroxyphenyl)sulfinylphenol Chemical compound OC1=C(Cl)C=C(Cl)C=C1S(=O)C1=CC(Cl)=CC(Cl)=C1O RPAJWWXZIQJVJF-UHFFFAOYSA-N 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 150000001555 benzenes Chemical class 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 150000008282 halocarbons Chemical class 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 238000011065 in-situ storage Methods 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
- C07D277/60—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings condensed with carbocyclic rings or ring systems
- C07D277/62—Benzothiazoles
- C07D277/68—Benzothiazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached in position 2
- C07D277/70—Sulfur atoms
- C07D277/76—Sulfur atoms attached to a second hetero atom
- C07D277/80—Sulfur atoms attached to a second hetero atom to a nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0025—Crosslinking or vulcanising agents; including accelerators
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US325699A US2730527A (en) | 1952-12-12 | 1952-12-12 | Preparation of 2-benzothiazolyl sulfene morpholide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES212646A2 true ES212646A2 (es) | 1955-03-01 |
Family
ID=23269035
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES0212646A Expired ES212646A2 (es) | 1952-12-12 | 1953-12-11 | Un procedimiento de preparar 2-benzotiazolil sulfeno morfolida |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US2730527A (fr) |
| DE (1) | DE1013653B (fr) |
| ES (1) | ES212646A2 (fr) |
| FR (1) | FR64850E (fr) |
| GB (1) | GB737252A (fr) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3070599A (en) * | 1962-12-25 | Method fos preparing secondary amino- | ||
| US3126394A (en) * | 1964-03-24 | Crystallizing z | ||
| US3022300A (en) * | 1954-09-23 | 1962-02-20 | Goodyear Tire & Rubber | Method of preparing sulfenamides |
| US2816881A (en) * | 1955-07-08 | 1957-12-17 | American Cyanamid Co | Method of vulcanizing a rubber in the presence of an accelerator and the product obtained thereby |
| US2839531A (en) * | 1955-09-19 | 1958-06-17 | Ici Ltd | Process for preparing 2-benzthiazylsulfeno morpholide |
| DE1175239B (de) * | 1955-11-30 | 1964-08-06 | American Cyanamid Co | Verfahren zur Herstellung von Sulfenmorpholiden |
| US2871239A (en) * | 1955-12-27 | 1959-01-27 | Monsanto Chemicals | 2-(2,6-dimethyl-4-morpholinylmercapto)-benzothiazoles |
| US3086018A (en) * | 1957-12-24 | 1963-04-16 | Goodyear Tire & Rubber | Manufacture of amino thiazole disulfides |
| US3055909A (en) * | 1960-01-13 | 1962-09-25 | American Cyanamid Co | Preparation of n-cyclohexyl-2-benzothiazole sulfenamide |
| DE3517084A1 (de) * | 1985-05-11 | 1986-11-13 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von benzothiazolsulfenamiden |
| JP6968099B2 (ja) | 2016-05-10 | 2021-11-17 | ハンツマン・アドバンスド・マテリアルズ・アメリカズ・エルエルシー | ベンズオキサジン樹脂のための潜在性触媒としてのベンゾチアゾール |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2045888A (en) * | 1936-06-30 | Preparation of sulphene amides | ||
| US2271834A (en) * | 1939-03-03 | 1942-02-03 | Firestone Tire & Rubber Co | Method of treating mercaptothiazoles with ammonia derivatives |
| US2261024A (en) * | 1939-06-22 | 1941-10-28 | Us Rubber Co | Vulcanization accelerator |
-
1952
- 1952-12-12 US US325699A patent/US2730527A/en not_active Expired - Lifetime
-
1953
- 1953-11-27 GB GB32976/53A patent/GB737252A/en not_active Expired
- 1953-12-05 DE DEA19284D patent/DE1013653B/de active Pending
- 1953-12-08 FR FR64850D patent/FR64850E/fr not_active Expired
- 1953-12-11 ES ES0212646A patent/ES212646A2/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR64850E (fr) | 1955-12-02 |
| US2730527A (en) | 1956-01-10 |
| DE1013653B (de) | 1957-08-14 |
| GB737252A (en) | 1955-09-21 |
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