ES2135486T3 - Un procedimiento para preparar dinitrotolueno. - Google Patents
Un procedimiento para preparar dinitrotolueno.Info
- Publication number
- ES2135486T3 ES2135486T3 ES93920409T ES93920409T ES2135486T3 ES 2135486 T3 ES2135486 T3 ES 2135486T3 ES 93920409 T ES93920409 T ES 93920409T ES 93920409 T ES93920409 T ES 93920409T ES 2135486 T3 ES2135486 T3 ES 2135486T3
- Authority
- ES
- Spain
- Prior art keywords
- procedure
- dinitrotoluene
- nitric acid
- preparing dinitrotoluene
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- DYSXLQBUUOPLBB-UHFFFAOYSA-N 2,3-dinitrotoluene Chemical compound CC1=CC=CC([N+]([O-])=O)=C1[N+]([O-])=O DYSXLQBUUOPLBB-UHFFFAOYSA-N 0.000 title abstract 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 2
- 229910017604 nitric acid Inorganic materials 0.000 abstract 2
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCESO PARA PREPARAR DINITROTOLUENO HACIENDO REACCIONAR TOLUENO CON ACIDO NITRICO CONCENTRADO. EL PROCESO REACCIONA TOLUENO CON UN AMPLIO EXCESO DE ACIDO NITRICO CONCENTRADO EN CONDICIONES SELECCIONADAS PARA PRODUCIR UN PRODUCTO QUE TIENE SUSTANCIALMENTE CONTENIDO DE SUBPRODUCTO REDUCIDO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/944,639 US5245092A (en) | 1991-03-15 | 1992-09-14 | Process for preparing dinitrotoluene with low by-product content |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2135486T3 true ES2135486T3 (es) | 1999-11-01 |
Family
ID=25481784
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93920409T Expired - Lifetime ES2135486T3 (es) | 1992-09-14 | 1993-08-30 | Un procedimiento para preparar dinitrotolueno. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US5245092A (es) |
| EP (1) | EP0660818B1 (es) |
| KR (2) | KR100289593B1 (es) |
| CN (1) | CN1053889C (es) |
| AU (1) | AU5096293A (es) |
| BR (1) | BR9307043A (es) |
| CA (1) | CA2144190A1 (es) |
| DE (1) | DE69324697T2 (es) |
| ES (1) | ES2135486T3 (es) |
| RU (1) | RU2100347C1 (es) |
| UA (1) | UA27939C2 (es) |
| WO (1) | WO1994006751A1 (es) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5245092A (en) * | 1991-03-15 | 1993-09-14 | Olin Corporation | Process for preparing dinitrotoluene with low by-product content |
| BR9306554A (pt) * | 1992-06-17 | 1998-09-15 | Olin Corp | Processo para nitração de tolueno para produzir dinitrotolueno e mistura de produto produzido pelo processo |
| DE4437047A1 (de) * | 1994-10-17 | 1996-04-18 | Bayer Ag | Verfahren zur Dinitrierung von aromatischen Verbindungen |
| US5948944A (en) * | 1998-11-18 | 1999-09-07 | Arco Chemical Technology, L.P. | Two-stage dinitrotoluene production process |
| CN101381311B (zh) * | 2007-09-07 | 2013-01-30 | 上海睿智化学研究有限公司 | 5-硝基-2,4-二卤代苯酚类化合物的制备方法 |
| CN101245010B (zh) * | 2008-03-08 | 2011-06-29 | 西北师范大学 | 民用二硝基甲苯的制备工艺 |
| CN101445458B (zh) * | 2009-01-06 | 2010-10-06 | 烟台巨力异氰酸酯有限公司 | 一种二硝基甲苯相分离方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2362743A (en) * | 1943-02-10 | 1944-11-14 | Hercules Powder Co Ltd | Manufacture of dinitrotoluene |
| US3928395A (en) * | 1972-10-05 | 1975-12-23 | Ciba Geigy Ag | Process for the nitration of aromatic compounds |
| US3957889A (en) * | 1975-05-02 | 1976-05-18 | Air Products And Chemicals, Inc. | Selective nitration of aromatic and substituted aromatic compositions |
| DE2521891B2 (de) * | 1975-05-16 | 1980-02-28 | Bayer Ag, 5090 Leverkusen | Verfahren zum Abstoppen von Nitrierungen durch Destillation |
| US4804792A (en) * | 1988-01-28 | 1989-02-14 | Olin Corporation | Nitration of benzene or toluene in a molten nitrate salt |
| US5001272A (en) * | 1988-06-22 | 1991-03-19 | Olin Corporation | Process for the production of dinitrotoluene |
| US4918250A (en) * | 1989-04-21 | 1990-04-17 | Olin Corporation | Process for the production of dinitrotoluene using an inorganic salt as a phase separation agent |
| US5099078A (en) * | 1990-12-21 | 1992-03-24 | Olin Corporation | Process for preparing dinitrotoluene |
| US5099080A (en) * | 1991-03-08 | 1992-03-24 | Olin Corporation | Process for preparing dinitrotoluene |
| US5245092A (en) * | 1991-03-15 | 1993-09-14 | Olin Corporation | Process for preparing dinitrotoluene with low by-product content |
| US5999078A (en) * | 1997-06-09 | 1999-12-07 | Herbert; Edward | Transformer and rectifier module with half-turn secondary windings |
-
1992
- 1992-09-14 US US07/944,639 patent/US5245092A/en not_active Expired - Lifetime
-
1993
- 1993-08-30 RU RU9595108602A patent/RU2100347C1/ru active
- 1993-08-30 KR KR1019950700968A patent/KR100289593B1/ko not_active Expired - Fee Related
- 1993-08-30 EP EP93920409A patent/EP0660818B1/en not_active Expired - Lifetime
- 1993-08-30 KR KR1019950700968A patent/KR950703512A/ko active Granted
- 1993-08-30 WO PCT/US1993/008135 patent/WO1994006751A1/en not_active Ceased
- 1993-08-30 DE DE69324697T patent/DE69324697T2/de not_active Expired - Fee Related
- 1993-08-30 CA CA002144190A patent/CA2144190A1/en not_active Abandoned
- 1993-08-30 ES ES93920409T patent/ES2135486T3/es not_active Expired - Lifetime
- 1993-08-30 UA UA95048337A patent/UA27939C2/uk unknown
- 1993-08-30 BR BR9307043A patent/BR9307043A/pt not_active IP Right Cessation
- 1993-08-30 AU AU50962/93A patent/AU5096293A/en not_active Abandoned
- 1993-09-13 CN CN93117282A patent/CN1053889C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CA2144190A1 (en) | 1994-03-31 |
| KR100289593B1 (ko) | 2001-05-02 |
| BR9307043A (pt) | 1999-06-29 |
| EP0660818A1 (en) | 1995-07-05 |
| CN1053889C (zh) | 2000-06-28 |
| KR950703512A (ko) | 1995-09-20 |
| EP0660818B1 (en) | 1999-04-28 |
| RU2100347C1 (ru) | 1997-12-27 |
| DE69324697T2 (de) | 1999-09-16 |
| WO1994006751A1 (en) | 1994-03-31 |
| UA27939C2 (uk) | 2000-10-16 |
| US5245092A (en) | 1993-09-14 |
| DE69324697D1 (de) | 1999-06-02 |
| EP0660818A4 (en) | 1995-05-23 |
| RU95108602A (ru) | 1996-12-27 |
| AU5096293A (en) | 1994-04-12 |
| CN1087897A (zh) | 1994-06-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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