ES2156599T3 - Procedimiento de purificacion de 1,1,1,3,3-pentafluoro-2,3-dicloropropano. - Google Patents

Procedimiento de purificacion de 1,1,1,3,3-pentafluoro-2,3-dicloropropano.

Info

Publication number
ES2156599T3
ES2156599T3 ES95903913T ES95903913T ES2156599T3 ES 2156599 T3 ES2156599 T3 ES 2156599T3 ES 95903913 T ES95903913 T ES 95903913T ES 95903913 T ES95903913 T ES 95903913T ES 2156599 T3 ES2156599 T3 ES 2156599T3
Authority
ES
Spain
Prior art keywords
dicloropropane
aceotropic
composition
pentafluoro
hydrogen fluoride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95903913T
Other languages
English (en)
Inventor
Tatsuo Nakada
Hirokazu Aoyama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daikin Industries Ltd
Original Assignee
Daikin Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daikin Industries Ltd filed Critical Daikin Industries Ltd
Application granted granted Critical
Publication of ES2156599T3 publication Critical patent/ES2156599T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/195—Separation; Purification
    • C01B7/196—Separation; Purification by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
    • C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

UNA MEZCLA QUE CONTIENE FLUORURO DE HIDROGENO Y 1,1,1,3,3PENTAFLUOR-2,3-DICLOROPROPANO SE SOMETE A DESTILACION PARA FORMAR UNA COMPOSICION ACEOTROPICA DE 85% A 95% MOLES DE FLUORURO DE HIDROGENO Y DE 15 A 5% MOLES DE 1,1,1,3,3-PENTAFLUOR-2,3DICLOROPROPANO, Y LA COMPOSICION ACEOTROPICA ES SEPARADA DEL LIQUIDO PARA FORMAR UNA FASE LIQUIDA REBAJADA. A CONTINUACION, UNA COMPOSICION ACEOTROPICA ES EXTRAIDA DE LA FASE LIQUIDA REBAJADA MEDIANTE DESTILACION, OBTENIENDOSE 1,1,1,3,3-PENTAFLUOR2,3-DICLOROPROPANO. SE OBTIENE 1,1,1,3,3-PENTAFLUOR-2,3-DICLOROPROPANO, SIN LA FORMACION DE UNA SOLUCION ACUOSA DE ACIDO HIDROFLUORICO DILUIDO, SUSTANCIALMENTE LIBRE DE FLUORURO DE HIDROGENO.
ES95903913T 1993-12-22 1994-12-21 Procedimiento de purificacion de 1,1,1,3,3-pentafluoro-2,3-dicloropropano. Expired - Lifetime ES2156599T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP32471093 1993-12-22

Publications (1)

Publication Number Publication Date
ES2156599T3 true ES2156599T3 (es) 2001-07-01

Family

ID=18168849

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95903913T Expired - Lifetime ES2156599T3 (es) 1993-12-22 1994-12-21 Procedimiento de purificacion de 1,1,1,3,3-pentafluoro-2,3-dicloropropano.

Country Status (6)

Country Link
US (1) US5789632A (es)
EP (1) EP0736508B1 (es)
JP (1) JP3278848B2 (es)
DE (1) DE69426837T2 (es)
ES (1) ES2156599T3 (es)
WO (1) WO1995017366A1 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6001796A (en) * 1996-07-03 1999-12-14 Alliedsignal Inc. Azeotrope-like compositions of 1,1,1,3,3-pentafluoropropane and hydrogen fluoride
JP2002510664A (ja) * 1998-04-03 2002-04-09 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ２−クロロ−１，１，１，２，３，３，３−ヘプタフルオロプロパンと、そのｈｆとの共沸混合物を精製および使用する方法
EP1068170A2 (en) * 1998-04-03 2001-01-17 E.I. Du Pont De Nemours And Company Processes for the purification and use of 2,2-dichloro-1,1,1,3,3,3-hexafluoropropane and azeotropes thereof with hf
US6900998B2 (en) * 2002-05-31 2005-05-31 Midwest Research Institute Variable-speed wind power system with improved energy capture via multilevel conversion
US8410040B2 (en) * 2008-10-31 2013-04-02 Honeywell International Inc. Azeotrope-like compositions of 1,1,1,2,3-pentachloropropane and hydrogen fluoride
US8519200B1 (en) * 2012-02-23 2013-08-27 Honeywell International Inc. Azeotropic compositions of 1,1,3,3-tetrachloro-1-fluoropropane and hydrogen fluoride
CN111807925B (zh) * 2020-07-23 2021-11-02 山东海益化工科技有限公司 D-d混剂精馏分离工艺

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0692327B2 (ja) * 1989-01-26 1994-11-16 ダイキン工業株式会社 フッ化水素と１，１―ジクロロ―１―フルオロエタンとの混合物から１，１―ジクロロ―１―フルオロエタンを分離する方法
US4970013A (en) * 1989-12-11 1990-11-13 E. I. Dupont De Nemours And Company Binary azeotropic composition of 2,3-dichloro-1,1,1,3-3-pentafluoropropane and methanol
JP3175286B2 (ja) * 1991-04-15 2001-06-11 ダイキン工業株式会社 フッ化水素と１，１，１−トリフルオロ−２−クロロエタンの共沸混合物および１，１，１−トリフルオロ−２−クロロエタンの精製方法
JPH0532568A (ja) * 1991-07-31 1993-02-09 Daikin Ind Ltd フツ化水素とジクロロフルオロメタンの混合物からフツ化水素を除去する方法

Also Published As

Publication number Publication date
EP0736508A4 (en) 1997-04-02
EP0736508B1 (en) 2001-03-07
DE69426837D1 (de) 2001-04-12
EP0736508A1 (en) 1996-10-09
WO1995017366A1 (fr) 1995-06-29
DE69426837T2 (de) 2001-07-19
US5789632A (en) 1998-08-04
JP3278848B2 (ja) 2002-04-30

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