ES2160941T3 - Procedimiento para elaborar aluminoxanos. - Google Patents
Procedimiento para elaborar aluminoxanos.Info
- Publication number
- ES2160941T3 ES2160941T3 ES97917847T ES97917847T ES2160941T3 ES 2160941 T3 ES2160941 T3 ES 2160941T3 ES 97917847 T ES97917847 T ES 97917847T ES 97917847 T ES97917847 T ES 97917847T ES 2160941 T3 ES2160941 T3 ES 2160941T3
- Authority
- ES
- Spain
- Prior art keywords
- aluminum
- solution
- hydrocarbylaluminum
- weight
- range
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 6
- 229910052782 aluminium Inorganic materials 0.000 abstract 6
- 239000003960 organic solvent Substances 0.000 abstract 2
- 125000001183 hydrocarbyl group Chemical group 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/06—Aluminium compounds
- C07F5/061—Aluminium compounds with C-aluminium linkage
- C07F5/066—Aluminium compounds with C-aluminium linkage compounds with Al linked to an element other than Al, C, H or halogen (this includes Al-cyanide linkage)
- C07F5/068—Aluminium compounds with C-aluminium linkage compounds with Al linked to an element other than Al, C, H or halogen (this includes Al-cyanide linkage) preparation of alum(in)oxanes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
Abstract
Un procedimiento en el que se alimentan hidrocarbilaluminio, agua y disolvente orgánico a un reactor para formar hidrocarbilaluminoxano, comprendiendo dicho procedimiento (a) alimentar tales materiales al reactor bajo condiciones de temperatura y en proporciones que forman una solución que contiene en el intervalo de 0, 5 a 15% en peso de aluminio como hidrocarbilaluminio e hidrocarbilaluminoxano, y en donde para cada parte molar de aluminio en la solución hay en la solución en el intervalo de 0, 1 a 0, 9 partes molares de hidrocarbilaluminio; y (b) separar la solución en una primera porción que consiste esencialmente en de 0, 5 a 15% en peso de aluminio como hidrocarbilaluminio disuelto en disolvente orgánico y una segunda porción que consiste esencialmente en de 3 a 20% en peso de aluminio total como hidrocarbilaluminoxano e hidrocarbilaluminio, y en donde para cada parte molar de aluminio en solución en dicha segunda porción hay en el intervalo de no más de 0, 03 a 0, 3 partes molares dehidrocarbilaluminio.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US635358 | 1996-04-19 | ||
| US08/635,358 US5606087A (en) | 1996-04-19 | 1996-04-19 | Process for making aluminoxanes |
| US08/680,087 US5663394A (en) | 1996-07-15 | 1996-07-15 | High yield aluminoxane synthesis process |
| US680087 | 1996-07-15 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2160941T3 true ES2160941T3 (es) | 2001-11-16 |
| ES2160941T5 ES2160941T5 (es) | 2007-06-01 |
Family
ID=27092356
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES97917847T Expired - Lifetime ES2160941T5 (es) | 1996-04-19 | 1997-04-02 | Procedimiento para elaborar aluminoxanos. |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP0906319B2 (es) |
| JP (2) | JP4291880B2 (es) |
| CA (1) | CA2252365A1 (es) |
| DE (1) | DE69705722T3 (es) |
| ES (1) | ES2160941T5 (es) |
| WO (1) | WO1997040053A1 (es) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8668389B2 (en) | 2000-11-07 | 2014-03-11 | Davis-Standard, Llc | Combination thrust flange and thrust plate |
| JP5440788B2 (ja) * | 2010-03-11 | 2014-03-12 | 東ソー・ファインケム株式会社 | フロー型反応器を用いたアルミノキサン組成物の製造方法 |
| JP6054659B2 (ja) * | 2011-07-13 | 2016-12-27 | ダウ グローバル テクノロジーズ エルエルシー | 有機金属化合物精製および装置 |
| EP2545972A1 (en) | 2011-07-13 | 2013-01-16 | Dow Global Technologies LLC | Organometallic compound purification by two steps distillation |
| EP2559681B1 (en) | 2011-08-15 | 2016-06-22 | Dow Global Technologies LLC | Organometallic compound preparation |
| EP2559682B1 (en) | 2011-08-15 | 2016-08-03 | Rohm and Haas Electronic Materials LLC | Organometallic compound preparation |
| EP3312200B1 (en) | 2013-02-08 | 2019-06-19 | Mitsui Chemicals, Inc. | Solid polyaluminoxane composition, olefin polymerization catalyst, olefin polymer production method and solid polyaluminoxane composition production method |
| CN110139882A (zh) | 2016-11-09 | 2019-08-16 | 株式会社普利司通 | 聚丁二烯和聚异戊二烯的高顺式-1,4嵌段共聚物 |
| CN117085625B (zh) * | 2023-09-07 | 2024-08-09 | 安徽博泰电子材料有限公司 | 一种连续式甲基铝氧烷制备系统 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2363888A1 (de) † | 1973-12-21 | 1975-07-03 | Auer Hans Heinrich | Vorrichtung mit rotierenden werkzeugen zur kontinuierlichen behandlung von stoffen in fliessfaehiger form |
| US4730072A (en) * | 1986-08-15 | 1988-03-08 | Shell Oil Company | Process for preparing aluminoxanes |
| US4908463A (en) * | 1988-12-05 | 1990-03-13 | Ethyl Corporation | Aluminoxane process |
| US4924018A (en) * | 1989-06-26 | 1990-05-08 | Ethyl Corporation | Alkylaluminoxane process |
| DE4004477A1 (de) † | 1990-02-14 | 1991-08-22 | Schering Ag | Verfahren zur herstellung von loesungen oligomerer methylaluminoxane |
| US5041585A (en) † | 1990-06-08 | 1991-08-20 | Texas Alkyls, Inc. | Preparation of aluminoxanes |
| US5248801A (en) * | 1992-08-27 | 1993-09-28 | Ethyl Corporation | Preparation of methylaluminoxanes |
| DE4314986A1 (de) * | 1993-05-06 | 1994-11-10 | Witco Gmbh | Verfahren zur Herstellung von Aluminoxanen |
| US5599964A (en) * | 1996-04-19 | 1997-02-04 | Albemarle Corporation | Continuous process for preparing hydrocarbylaluminoxanes |
| DE10133728A1 (de) * | 2001-07-11 | 2003-01-23 | Bayer Ag | Verfahren zur Herstellung von (cyclo)aliphatischen Diisocyanaten |
-
1997
- 1997-04-02 WO PCT/US1997/005554 patent/WO1997040053A1/en not_active Ceased
- 1997-04-02 DE DE69705722T patent/DE69705722T3/de not_active Expired - Lifetime
- 1997-04-02 CA CA 2252365 patent/CA2252365A1/en not_active Abandoned
- 1997-04-02 EP EP97917847A patent/EP0906319B2/en not_active Expired - Lifetime
- 1997-04-02 ES ES97917847T patent/ES2160941T5/es not_active Expired - Lifetime
- 1997-04-02 JP JP53808997A patent/JP4291880B2/ja not_active Expired - Fee Related
-
2008
- 2008-11-05 JP JP2008284860A patent/JP5066058B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CA2252365A1 (en) | 1997-10-30 |
| EP0906319B1 (en) | 2001-07-18 |
| EP0906319B2 (en) | 2006-12-06 |
| DE69705722T3 (de) | 2007-04-26 |
| WO1997040053A1 (en) | 1997-10-30 |
| JP2000509040A (ja) | 2000-07-18 |
| ES2160941T5 (es) | 2007-06-01 |
| JP4291880B2 (ja) | 2009-07-08 |
| JP2009073849A (ja) | 2009-04-09 |
| DE69705722D1 (de) | 2001-08-23 |
| DE69705722T2 (de) | 2002-05-08 |
| EP0906319A1 (en) | 1999-04-07 |
| JP5066058B2 (ja) | 2012-11-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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