ES2175498T3 - Un procedimiento para la preparacion de un reactivo organico de zinc. - Google Patents

Un procedimiento para la preparacion de un reactivo organico de zinc.

Info

Publication number
ES2175498T3
ES2175498T3 ES97950253T ES97950253T ES2175498T3 ES 2175498 T3 ES2175498 T3 ES 2175498T3 ES 97950253 T ES97950253 T ES 97950253T ES 97950253 T ES97950253 T ES 97950253T ES 2175498 T3 ES2175498 T3 ES 2175498T3
Authority
ES
Spain
Prior art keywords
metal
preparation
organozinc
halide salt
hydrocarbon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97950253T
Other languages
English (en)
Inventor
Andrew John Blacker
Jan Michael Fielden
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Avecia Ltd
Original Assignee
Avecia Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Avecia Ltd filed Critical Avecia Ltd
Application granted granted Critical
Publication of ES2175498T3 publication Critical patent/ES2175498T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/28—Radicals substituted by singly-bound oxygen or sulphur atoms
    • C07D213/30—Oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B53/00—Asymmetric syntheses
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
    • C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
    • C07C29/40—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones with compounds containing carbon-to-metal bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F3/00—Compounds containing elements of Groups 2 or 12 of the Periodic Table
    • C07F3/06—Zinc compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Pyridine Compounds (AREA)
  • Pyrrole Compounds (AREA)
  • Steroid Compounds (AREA)
  • Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
  • Catalysts (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO DE PREPARACION DE UN COMPUESTO AROMATICO DE ORGANOZINC. DICHO PROCEDIMIENTO CONSISTE EN HACER REACCIONAR UN CLORURO, BROMURO O IODURO DE ZINC Y UN COMPUESTO ORGANOMETALICO DE OTRO METAL QUE COMPRENDE UNA FRACCION AROMATICA, Y PRODUCIR UN PRODUCTO DE REACCION QUE COMPRENDE UN COMPUESTO DE ORGANOZINC Y UNA SAL DE HALURO DEL OTRO METAL. DICHO PRODUCTO DE REACCION SE HACE REACCIONAR A CONTINUACION CON UN HIDROCARBURO LIQUIDO, EN EL CUAL ES SOLUBLE EL COMPUESTO DE ORGANOZINC Y LA SAL DE HALURO DEL OTRO METAL ES DEBILMENTE SOLUBLE. LA SAL DE HALURO DEL OTRO METAL SE SEPARA DEL HIDROCARBURO, Y EL COMPUESTO DE ORGANOZINC SE PUEDE RECUPERAR A PARTIR DE DICHO HIDROCARBURO. LOS COMPUESTOS DE ORGANOZINC OBTENIDOS MEDIANTE DICHO PROCEDIMIENTO SE PUEDEN EMPLEAR PARA GENERAR CENTROS QUIRALES EN SUSTRATOS ADECUADOS.
ES97950253T 1996-12-21 1997-12-15 Un procedimiento para la preparacion de un reactivo organico de zinc. Expired - Lifetime ES2175498T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB9626635.8A GB9626635D0 (en) 1996-12-21 1996-12-21 Zinc reagent and synthesis

Publications (1)

Publication Number Publication Date
ES2175498T3 true ES2175498T3 (es) 2002-11-16

Family

ID=10804854

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97950253T Expired - Lifetime ES2175498T3 (es) 1996-12-21 1997-12-15 Un procedimiento para la preparacion de un reactivo organico de zinc.

Country Status (12)

Country Link
US (1) US6258967B1 (es)
EP (1) EP0946570B1 (es)
JP (1) JP2001507348A (es)
AT (1) ATE219086T1 (es)
AU (1) AU5327998A (es)
CA (1) CA2273942C (es)
DE (1) DE69713385T2 (es)
DK (1) DK0946570T3 (es)
ES (1) ES2175498T3 (es)
GB (1) GB9626635D0 (es)
PT (1) PT946570E (es)
WO (1) WO1998028306A1 (es)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2826963B1 (fr) * 2001-07-04 2006-01-27 Rhodia Chimie Sa Preparation d'organozinciques aromatiques et composition pour ce faire
US8089904B2 (en) 2006-08-01 2012-01-03 Opnet Technologies, Inc. Link inference in large networks based on incomplete data
EP2155759A4 (en) 2007-05-07 2012-10-17 Valorisation Rech Soc En Commandite METHOD FOR PRODUCING DIORGANOZINK COMPOUNDS
JP5488786B2 (ja) * 2009-03-31 2014-05-14 宇部興産株式会社 アザボラシクロペンテン化合物の製造方法及びその合成中間体
JP5423212B2 (ja) * 2009-07-30 2014-02-19 宇部興産株式会社 アミノアザボラシクロペンテン化合物の製造方法
WO2011115963A1 (en) * 2010-03-16 2011-09-22 Rieke Metals Inc. Stabilized organometallic reagents
WO2012085168A1 (en) * 2010-12-22 2012-06-28 Ludwig-Maximilians-Universität München Organozinc complexes and processes for making and using the same
WO2012147897A1 (ja) * 2011-04-25 2012-11-01 住友化学株式会社 アミン化合物の製造方法
CN103272645B (zh) * 2013-06-19 2014-11-05 罗梅 一种手性锌配合物的用途
CN106414315B (zh) * 2014-01-03 2019-07-30 罗克伍德锂有限责任公司 制备含有溴化锌和溴化锂的非质子溶液的方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9012974D0 (en) 1990-06-11 1990-08-01 Ici Plc Chemical process

Also Published As

Publication number Publication date
CA2273942C (en) 2007-04-17
EP0946570A1 (en) 1999-10-06
US6258967B1 (en) 2001-07-10
ATE219086T1 (de) 2002-06-15
DK0946570T3 (da) 2002-10-07
AU5327998A (en) 1998-07-17
DE69713385T2 (de) 2003-02-06
WO1998028306A1 (en) 1998-07-02
PT946570E (pt) 2002-10-31
DE69713385D1 (de) 2002-07-18
JP2001507348A (ja) 2001-06-05
GB9626635D0 (en) 1997-02-12
CA2273942A1 (en) 1998-07-02
EP0946570B1 (en) 2002-06-12

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