ES2177193T3 - Metodo para la produccion de acido nitrico. - Google Patents

Metodo para la produccion de acido nitrico.

Info

Publication number
ES2177193T3
ES2177193T3 ES99125583T ES99125583T ES2177193T3 ES 2177193 T3 ES2177193 T3 ES 2177193T3 ES 99125583 T ES99125583 T ES 99125583T ES 99125583 T ES99125583 T ES 99125583T ES 2177193 T3 ES2177193 T3 ES 2177193T3
Authority
ES
Spain
Prior art keywords
nitric acid
gaseous
zone
nitric
production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES99125583T
Other languages
English (en)
Inventor
Diego Fernandez Echegaray
Velloso Antonio Augusto M
Matthew Loncoln Wagner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Praxair Technology Inc
Original Assignee
Praxair Technology Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Praxair Technology Inc filed Critical Praxair Technology Inc
Application granted granted Critical
Publication of ES2177193T3 publication Critical patent/ES2177193T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
    • C01B21/24—Nitric oxide (NO)
    • C01B21/26—Preparation by catalytic or non-catalytic oxidation of ammonia
    • C01B21/262—Preparation by catalytic or non-catalytic oxidation of ammonia obtaining nitrogen dioxide or tetroxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
    • C01B21/38—Nitric acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
    • C01B21/38—Nitric acid
    • C01B21/40—Preparation by absorption of oxides of nitrogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Treating Waste Gases (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

Un procedimiento mejorado para producir ácido nítrico por oxidación de amoníaco gaseoso para formar tetróxido de dinitrógeno gaseoso, haciendo reaccionar el tetróxido de dinitrógeno con agua en una zona de absorción para formar ácido nítrico acuoso y óxido nítrico gaseoso, separando la corriente ácido nítrico/óxido nítrico de la zona de absorción y alimentando la corriente a una zona de blanqueo del ácido nítrico, eliminando las impurezas del ácido nítrico en la zona de blanqueo para formar ácido nítrico producto y añadiendo oxígeno gaseoso suplementario a una o más de las corrientes de reacción para aumentar la producción de ácido nítrico y/o su concentración, consistiendo la mejora en inyectar el oxígeno suplementario en una corriente del procedimiento que contiene ácido nítrico para formar en ella una mezcla de burbujas de gas/líquido que consiste en una dispersión fina de burbujas de gas que tienen diámetros de menos de aproximadamente 0,1 mm y que de ese modo proporcionan una mayor superficie interfacial entre las burbujas de gas y la mezcla líquida.
ES99125583T 1998-12-24 1999-12-21 Metodo para la produccion de acido nitrico. Expired - Lifetime ES2177193T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US09/220,818 US6165435A (en) 1998-12-24 1998-12-24 Method and production of nitric acid

Publications (1)

Publication Number Publication Date
ES2177193T3 true ES2177193T3 (es) 2002-12-01

Family

ID=22825105

Family Applications (1)

Application Number Title Priority Date Filing Date
ES99125583T Expired - Lifetime ES2177193T3 (es) 1998-12-24 1999-12-21 Metodo para la produccion de acido nitrico.

Country Status (9)

Country Link
US (1) US6165435A (es)
EP (1) EP1013604B1 (es)
KR (1) KR100501462B1 (es)
CN (1) CN1157329C (es)
BR (1) BR9905929A (es)
CA (1) CA2293004C (es)
DE (1) DE69902139T2 (es)
ES (1) ES2177193T3 (es)
ID (1) ID24018A (es)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7410626B2 (en) * 2003-09-10 2008-08-12 Basf Catalysts Llc Layered ammonia oxidation catalyst
DE102005023161A1 (de) * 2005-05-19 2006-11-23 Siemens Ag Verfahren und Anlage zur Herstellung von Salpetersäure
CN100396360C (zh) * 2006-04-24 2008-06-25 南京大学 一种工业过程氮氧化物(nox)废气治理及资源化的方法
BRPI0801209B1 (pt) * 2008-04-14 2017-07-04 White Martins Gases Industriais Ltda. Ethanol fermentation system
EP2306814B1 (en) * 2008-07-24 2013-11-27 Geno LLC Methods for diagnosing and treating a heart condition in a patient
UA91614C2 (uk) * 2008-11-28 2010-08-10 Іван Іванович Барабаш Спосіб виробництва азотної кислоти (варіанти) і агрегат для виробництва азотної кислоти
CN101575089B (zh) * 2009-06-10 2010-12-29 上海化工研究院 一种18o-硝酸的制备方法
CN101837961B (zh) * 2010-05-25 2012-08-22 安徽淮化股份有限公司 一种符合节能减排及低成本配制稀硝酸的方法及装置
AU2011335885B2 (en) * 2010-12-01 2013-02-14 The University Of Sydney Process for producing nitric acid
CN102491292A (zh) * 2011-12-06 2012-06-13 中国成达工程有限公司 一种低消耗、低排放的硝酸生产方法及其生产设备
EP2822681A1 (en) 2012-03-05 2015-01-14 Basf Se Ammonia oxidation reactor with internal filter element
CN103112835B (zh) * 2012-11-11 2014-11-26 安徽金禾实业股份有限公司 一种浓硝酸生产过程中的间接漂白方法
DE102013002201A1 (de) * 2013-02-07 2014-08-07 Messer Austria Gmbh Verfahren und Produktionsanlage zum Herstellen von Salpetersäure
DE102013004341A1 (de) * 2013-03-14 2014-09-18 Thyssenkrupp Uhde Gmbh Verfahren zur Oxidation von Ammoniak und dafür geeignete Anlage
CN103395758B (zh) * 2013-08-02 2015-03-25 柳州化工股份有限公司 一种配制硝酸水溶液的装置
CN103395759B (zh) * 2013-08-02 2015-01-14 柳州化工股份有限公司 一种配制硝酸水溶液脱色方法
DE102014006017B4 (de) 2014-04-23 2022-04-21 Messer Group Gmbh Verfahren und Vorrichtung zum Herstellen von Salpetersäure
KR101669976B1 (ko) * 2014-11-27 2016-11-09 휴켐스주식회사 질산의 제조방법
CN105134560A (zh) * 2015-08-23 2015-12-09 安徽金禾实业股份有限公司 硝酸生产中对压缩机进口空气进行冷冻脱湿的方法
DE102015014185A1 (de) 2015-11-03 2017-05-18 Messer Group Gmbh Verfahren zur Herstellung von Peroxosalpetersäure
CN105883735A (zh) * 2016-05-13 2016-08-24 河南心连心化肥有限公司 一种富氧法制硝酸装置及其硝酸生产方法
DE102016015322A1 (de) 2016-12-22 2018-06-28 Messer Group Gmbh Vorrichtung und Verfahren zum Eintragen von Gas in eine Mehrzahl von Prozessfluiden
CN106744746B (zh) * 2017-02-17 2018-11-02 交城县金兰化工有限公司 一种环保高效的硝酸生产方法
EP3372556A1 (en) * 2017-03-07 2018-09-12 Casale Sa A plant for the production of nitric acid, a related process and method of revamping
DE102017004329A1 (de) * 2017-05-04 2018-11-08 Messer Group Gmbh Verfahren und Vorrichtung zum Eintragen eines Gases in eine Flüssigkeit
CN109879258B (zh) * 2019-02-20 2024-03-08 浙江瀚普智慧科技有限公司 一种氮氧化物高效氧化吸收制硝酸的装置及方法
EP3927658B1 (en) * 2019-02-22 2023-06-07 Yara International ASA Bleaching tower and method for nitric acid production
CN110540178B (zh) * 2019-09-10 2024-02-02 中国成达工程有限公司 一种中压法硝酸生产工艺及其生产设备
CN112473570A (zh) * 2019-09-11 2021-03-12 南京延长反应技术研究院有限公司 一种基于微界面强化的硝酸工业制备系统及工艺
DE102020002008A1 (de) 2020-03-27 2021-09-30 Messer Group Gmbh Verfahren und Produktionsanlage zum Herstellen von Salpetersäure
EP3904280A1 (en) * 2020-04-29 2021-11-03 Yara International ASA Absorption column comprising a feed box having a serrated weir and a structured packing and process for the production of nitric acid
DE102020003083A1 (de) 2020-05-22 2021-11-25 Messer Group Gmbh Verfahren und Produktionsanlage zum Herstellen von Salpetersäure
CN217614063U (zh) * 2021-07-26 2022-10-21 青岛威巴克生物技术有限公司 次氯酸消毒液灌装设备
CN116395715B (zh) * 2023-06-07 2023-08-18 河北正元化工工程设计有限公司 一种绿氢、灰氢耦合制氨联产硝酸与硝酸铵工艺
KR102729732B1 (ko) * 2023-08-04 2024-11-13 주식회사 한화 일산화질소의 제조방법 및 이 방법으로 제조된 일산화질소
DE102024111801A1 (de) 2024-04-26 2025-10-30 Messer Se & Co. Kgaa Verfahren und Produktionsanlage zum Herstellen von Salpetersäure

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE551022A (es) * 1955-09-14 1900-01-01
US3927182A (en) * 1971-02-25 1975-12-16 James Basil Powell Process for making nitric acid by the ammonia oxidation-nitric oxide oxidation-water absorption method
IT1027882B (it) * 1974-12-20 1978-12-20 Sir Soc Italiana Resine Spa Procedimento per la produzione di acito nitrico
GB1603630A (en) * 1977-06-16 1981-11-25 Boc Ltd Gas-liquid contact process
EP0004746A3 (en) * 1978-04-07 1979-10-31 BOC Limited Gas-liquid contact process
DE2939674A1 (de) * 1979-09-29 1981-04-09 Hoechst Ag, 6000 Frankfurt Verfahren zur absorption nitroser gase
DE3704720A1 (de) * 1987-02-14 1988-08-25 Huels Troisdorf Verfahren und vorrichtung zur herstellung von benzolcarbonsaeuren bzw. benzoldicarbonsaeureestern
US4867918A (en) * 1987-12-30 1989-09-19 Union Carbide Corporation Gas dispersion process and system
US4931225A (en) * 1987-12-30 1990-06-05 Union Carbide Industrial Gases Technology Corporation Method and apparatus for dispersing a gas into a liquid
DE3826955A1 (de) * 1988-08-09 1990-02-15 Krupp Gmbh Verfahren und vorrichtung zum eintragen von sauerstoff in fluessigkeiten
US5167935A (en) * 1989-01-26 1992-12-01 Beco Engineering Company Apparatus for treatment of nitrogen oxides
US5356600A (en) * 1990-09-24 1994-10-18 Praxair Technology, Inc. Oxygen enrichment method and system
US5061406A (en) * 1990-09-25 1991-10-29 Union Carbide Industrial Gases Technology Corporation In-line gas/liquid dispersion
US5302325A (en) * 1990-09-25 1994-04-12 Praxair Technology, Inc. In-line dispersion of gas in liquid
US5108662A (en) * 1991-05-01 1992-04-28 Union Carbide Industrial Gases Technology Corporation Gas-liquid mixing process and apparatus
CA2200996A1 (en) * 1996-04-01 1997-10-01 Sandeep Bhatia Oxygen injection in nitric acid production
ID16932A (id) * 1996-05-23 1997-11-20 Praxair Technology Inc Penyemprot oksigen langsung dalam produksi asam nitrat
US5985230A (en) * 1996-10-03 1999-11-16 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Nitric acid production

Also Published As

Publication number Publication date
CN1157329C (zh) 2004-07-14
CA2293004C (en) 2003-05-13
KR20000052536A (ko) 2000-08-25
CA2293004A1 (en) 2000-06-24
BR9905929A (pt) 2000-08-15
KR100501462B1 (ko) 2005-07-18
DE69902139T2 (de) 2003-01-16
EP1013604A1 (en) 2000-06-28
ID24018A (id) 2000-06-29
US6165435A (en) 2000-12-26
EP1013604B1 (en) 2002-07-17
CN1261594A (zh) 2000-08-02
DE69902139D1 (de) 2002-08-22

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