ES2178214T3 - Preparacion de zeolita l. - Google Patents
Preparacion de zeolita l.Info
- Publication number
- ES2178214T3 ES2178214T3 ES98923542T ES98923542T ES2178214T3 ES 2178214 T3 ES2178214 T3 ES 2178214T3 ES 98923542 T ES98923542 T ES 98923542T ES 98923542 T ES98923542 T ES 98923542T ES 2178214 T3 ES2178214 T3 ES 2178214T3
- Authority
- ES
- Spain
- Prior art keywords
- preparation
- zeolite
- reaction mixture
- source
- sufficient
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000002360 preparation method Methods 0.000 title abstract 3
- 229910021536 Zeolite Inorganic materials 0.000 abstract 4
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 4
- 239000010457 zeolite Substances 0.000 abstract 4
- 239000011541 reaction mixture Substances 0.000 abstract 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 229910052681 coesite Inorganic materials 0.000 abstract 1
- 229910052906 cristobalite Inorganic materials 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 235000012239 silicon dioxide Nutrition 0.000 abstract 1
- 229910052682 stishovite Inorganic materials 0.000 abstract 1
- 229910052905 tridymite Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/32—Type L
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/28—LTL, e.g. BA-G, L, AG-1, AG-2, AG-4, BA-6
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Catalysts (AREA)
Abstract
Un procedimiento para la preparación de zeolita L cristalina, comprendiendo dicho procedimiento: (A) la preparación de una mezcla de reacción auto-soportante que comprende al menos una fuente activa de silicio, al menos una fuente activa de alúmina y una fuente de hidróxido en cantidades suficientes para producir zeolita L, y suficiente agua para producir zeolita L, en el que la mezcla de reacción tiene una relación molar de OH-/ SiO2 de desde 0, 20 hasta 0, 40; y (B) el calentamiento de dicha mezcla de reacción a una temperatura desde aproximadamente 90°C hasta aproximadamente 200°C bajo condiciones de cristalización y en ausencia de una fase líquida externa agregada durante un tiempo suficiente para formar cristales de zeolita L.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/690,711 US5785945A (en) | 1996-07-31 | 1996-07-31 | Preparation of zeolite L |
| PCT/US1998/010268 WO1999059917A1 (en) | 1996-07-31 | 1998-05-20 | Preparation of zeolite l |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2178214T3 true ES2178214T3 (es) | 2002-12-16 |
Family
ID=26794127
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES98923542T Expired - Lifetime ES2178214T3 (es) | 1996-07-31 | 1998-05-20 | Preparacion de zeolita l. |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5785945A (es) |
| EP (1) | EP1080037B1 (es) |
| JP (1) | JP4361689B2 (es) |
| CN (1) | CN1148319C (es) |
| AU (1) | AU753445B2 (es) |
| BR (1) | BR9815862A (es) |
| CA (1) | CA2333210A1 (es) |
| DE (1) | DE69804513T2 (es) |
| ES (1) | ES2178214T3 (es) |
| WO (1) | WO1999059917A1 (es) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5919430A (en) * | 1996-06-19 | 1999-07-06 | Degussa Aktiengesellschaft | Preparation of crystalline microporous and mesoporous metal silicates, products produced thereby and use thereof |
| US5785945A (en) * | 1996-07-31 | 1998-07-28 | Chevron Chemical Company Llc | Preparation of zeolite L |
| US6444865B1 (en) | 1997-12-01 | 2002-09-03 | Shell Oil Company | Process wherein a hydrocarbon feedstock is contacted with a catalyst |
| US6261534B1 (en) * | 1999-11-24 | 2001-07-17 | Chevron U.S.A. Inc. | Method for making ZSM-5 zeolites |
| US6632415B2 (en) | 2001-04-09 | 2003-10-14 | Chevron U.S.A. Inc. | Methods for making molecular sieves |
| EP2029664A4 (en) * | 2006-05-31 | 2015-09-09 | Dow Global Technologies Llc | ADJUVANTS FOR THE USE OF MICROWAVE ENERGY IN THE SELECTIVE HEATING OF THERMOPLASTIC POLYMER SYSTEMS |
| US20080159950A1 (en) * | 2006-12-27 | 2008-07-03 | Miller Stephen J | Preparation of molecular sieve ssz-13 |
| FR2916435B1 (fr) * | 2007-05-25 | 2010-01-08 | Inst Francais Du Petrole | Nouveau procede de preparation de la zolithe eu-1. |
| US8992884B2 (en) * | 2009-11-30 | 2015-03-31 | Chevron U.S.A. Inc. | Preparation of X zeolite |
| DE102010034005A1 (de) | 2010-08-11 | 2012-02-16 | Süd-Chemie AG | Hydrothermale Synthese von Zeolithen oder zeolithähnlichen Materialien unter Verwendung von modifizierten Mischoxiden |
| CN102530985B (zh) * | 2010-12-17 | 2013-07-31 | 中国石油天然气股份有限公司 | 一种原位晶化制备l沸石的方法 |
| US9784688B2 (en) | 2012-10-10 | 2017-10-10 | Seagate Technology Llc | Apparatus for uniformly irradiating and imaging an article |
| WO2016078035A1 (zh) * | 2014-11-19 | 2016-05-26 | 中国石油大学(北京) | 一种活性硅铝酸盐材料及其制备方法 |
| CN106495182A (zh) * | 2016-10-27 | 2017-03-15 | 湖南理工学院 | 一种l型沸石分子筛的制备方法 |
| CN113415808B (zh) * | 2021-06-13 | 2023-02-28 | 浙江大学 | 一种无有机模板剂原位合成成型分子筛的方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3119659A (en) * | 1960-09-26 | 1964-01-28 | Union Carbide Corp | Process for producing molecular sieve bodies |
| US3094383A (en) * | 1960-12-16 | 1963-06-18 | Minerals & Chem Philipp Corp | Method for making synthetic zeolitic material |
| NL238183A (es) * | 1962-08-03 | |||
| FR1598506A (es) * | 1968-01-05 | 1970-07-06 | ||
| US4058586A (en) * | 1976-02-25 | 1977-11-15 | W. R. Grace & Co. | Forming and crystallization process for molecular sieve manufacture |
| US4544539A (en) * | 1982-05-14 | 1985-10-01 | Exxon Research & Engineering Co. | Zeolite L with cylindrical morphology |
| GB8329973D0 (en) * | 1983-11-10 | 1983-12-14 | Exxon Research Engineering Co | Recycled zeolite l preparation |
| FR2565847B1 (fr) * | 1984-06-18 | 1986-08-29 | Inst Francais Du Petrole | Synthese et utilisation de zeolithes preformees |
| GB8704365D0 (en) * | 1987-02-25 | 1987-04-01 | Exxon Chemical Patents Inc | Zeolite l preparation |
| GB8709506D0 (en) * | 1987-04-22 | 1987-05-28 | Exxon Chemical Patents Inc | Zeolite l synthesis |
| GB8800045D0 (en) * | 1988-01-04 | 1988-02-10 | Exxon Chemical Patents Inc | Zeolite l |
| US5318766A (en) * | 1992-09-25 | 1994-06-07 | Exxon Research And Engineering Company | Process for preparing LTL nano-crystalline zeolite compositions |
| WO1994013584A1 (en) * | 1992-12-16 | 1994-06-23 | Chevron Research And Technology Company, A Division Of Chevron U.S.A. Inc. | Preparation of aluminosilicate zeolites |
| US5785944A (en) * | 1996-07-31 | 1998-07-28 | Chevron U.S.A. Inc. | Preparation of Y zeolite |
| US5785945A (en) * | 1996-07-31 | 1998-07-28 | Chevron Chemical Company Llc | Preparation of zeolite L |
-
1996
- 1996-07-31 US US08/690,711 patent/US5785945A/en not_active Expired - Lifetime
-
1998
- 1998-05-20 JP JP2000549540A patent/JP4361689B2/ja not_active Expired - Fee Related
- 1998-05-20 ES ES98923542T patent/ES2178214T3/es not_active Expired - Lifetime
- 1998-05-20 CA CA002333210A patent/CA2333210A1/en not_active Abandoned
- 1998-05-20 EP EP98923542A patent/EP1080037B1/en not_active Expired - Lifetime
- 1998-05-20 AU AU75810/98A patent/AU753445B2/en not_active Ceased
- 1998-05-20 DE DE69804513T patent/DE69804513T2/de not_active Expired - Lifetime
- 1998-05-20 WO PCT/US1998/010268 patent/WO1999059917A1/en not_active Ceased
- 1998-05-20 CN CNB988141264A patent/CN1148319C/zh not_active Expired - Fee Related
- 1998-05-20 BR BR9815862-7A patent/BR9815862A/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JP4361689B2 (ja) | 2009-11-11 |
| BR9815862A (pt) | 2001-01-16 |
| CA2333210A1 (en) | 1999-11-25 |
| AU753445B2 (en) | 2002-10-17 |
| CN1299336A (zh) | 2001-06-13 |
| AU7581098A (en) | 1999-12-06 |
| WO1999059917A1 (en) | 1999-11-25 |
| US5785945A (en) | 1998-07-28 |
| EP1080037B1 (en) | 2002-03-27 |
| JP2002515394A (ja) | 2002-05-28 |
| CN1148319C (zh) | 2004-05-05 |
| DE69804513D1 (de) | 2002-05-02 |
| EP1080037A1 (en) | 2001-03-07 |
| DE69804513T2 (de) | 2002-10-17 |
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