ES2182025T3 - Procedimiento de separacion. - Google Patents

Procedimiento de separacion.

Info

Publication number
ES2182025T3
ES2182025T3 ES97903537T ES97903537T ES2182025T3 ES 2182025 T3 ES2182025 T3 ES 2182025T3 ES 97903537 T ES97903537 T ES 97903537T ES 97903537 T ES97903537 T ES 97903537T ES 2182025 T3 ES2182025 T3 ES 2182025T3
Authority
ES
Spain
Prior art keywords
phase
desired substance
crystallized
separation procedure
procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97903537T
Other languages
English (en)
Inventor
Karl Reuter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Reuter Chemischer Apparatebau KG
Original Assignee
Reuter Chemischer Apparatebau KG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Reuter Chemischer Apparatebau KG filed Critical Reuter Chemischer Apparatebau KG
Application granted granted Critical
Publication of ES2182025T3 publication Critical patent/ES2182025T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B01D9/0009—Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Enzymes And Modification Thereof (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

SE DESCRIBE UN PROCEDIMIENTO PARA SEPARAR UNA SUSTANCIA DESEADA DE UNA MEZCLA TOTAL EN EL QUE SE FORMA UNA DISPERSION EN TRES FASES, COMPRENDIENDO LA PRIMERA FASE UNAS PEQUEÑAS GOTAS QUE CONTIENEN LA MEZCLA AGREGADA, LA SEGUNDA FASE UNA FASE DE TRANSPORTE LIQUIDO, Y LA TERCERA FASE UNA SUPERFICIE SOBRE LA QUE PUEDE CRISTALIZARSE LA SUSTANCIA DESEADA, CARACTERIZADO PORQUE EXISTE UN POTENCIAL QUIMICO PARA EL CRECIMIENTO DEL CRISTAL DE LA SUSTANCIA DESEADA EN LA TERCERA FASE, CREANDOSE DE ESE MODO UN FLUJO DE LA SUSTANCIA DESEADA DESDE LA PRIMERA A LA TERCERA FASE, PASANDO POR LA SEGUNDA, EN CUYA TERCERA FASE SE CRISTALIZA LA SUSTANCIA DESEADA, Y CARACTERIZADO PORQUE LA ENTALPIA LIBRE DE GIBB DE LA FORMACION ( DE G) DE LAS GOTITAS ES < 0.
ES97903537T 1996-03-10 1997-03-07 Procedimiento de separacion. Expired - Lifetime ES2182025T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP96200654 1996-03-10

Publications (1)

Publication Number Publication Date
ES2182025T3 true ES2182025T3 (es) 2003-03-01

Family

ID=8223765

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97903537T Expired - Lifetime ES2182025T3 (es) 1996-03-10 1997-03-07 Procedimiento de separacion.

Country Status (9)

Country Link
US (1) US6383233B1 (es)
EP (1) EP0956122B1 (es)
JP (1) JP4157602B2 (es)
AT (1) ATE220939T1 (es)
DE (1) DE69714297T2 (es)
DK (1) DK0956122T3 (es)
ES (1) ES2182025T3 (es)
PT (1) PT956122E (es)
WO (1) WO1997032644A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001515776A (ja) * 1997-09-06 2001-09-25 ロイター・ヒェーミシェ・アパラーテバウ・コマンディート・ゲゼルシャフト 分離法
EP1034826A1 (en) * 1999-03-05 2000-09-13 Reuter Chemische Apparatebau Co-crystallization process
EP1161290B1 (en) * 1999-03-17 2007-09-12 Reuter Chemische Apparatebau KG Emulsion crystallisation with recycle
US7038073B2 (en) * 2002-05-15 2006-05-02 Genzyme Corporation Synthesis of 2-alkyl amino acids
JP2007326083A (ja) * 2006-06-09 2007-12-20 Fujifilm Corp 固体微粒子及びその製造方法
CN102112425B (zh) 2008-07-29 2014-06-11 普克塞尔公司 通过控制粒径的结晶从对映体混合物中分离对映体组分的方法
WO2010112222A1 (en) 2009-03-31 2010-10-07 Krka, D.D., Novo Mesto Progressive emulsion crystallization
EP2473247A2 (en) * 2009-09-01 2012-07-11 University Of Durham Method of controlling crystallisation
US8207352B2 (en) * 2009-10-08 2012-06-26 Drug Process Licensing Associates LLC Process for the manufacture of enantiomerically pure antifungal azoles as ravuconazole and isavuconazole
EP2364977A1 (en) 2010-01-26 2011-09-14 Reuter Chemische Apparatebau KG Process for the enantiomeric enrichment of 3-methyl-1-(2-piperidinophenyl)-1-butylamine
EP2861316B1 (en) 2012-06-15 2020-06-03 Farma GRS, d.o.o. Selective crystallization processes using reverse micelle and w/o microemulsion systems - multitask emulsion crystallization (mec)
WO2014128139A1 (en) 2013-02-20 2014-08-28 Reuter Chemische Apparatebau Kg Process for the preparation of enantiomerically enriched 3-aminopiperidine
JP6143808B2 (ja) * 2015-05-28 2017-06-07 曽田香料株式会社 水溶液中の溶質成分の抽出法
WO2017117567A1 (en) 2015-12-30 2017-07-06 Berkeley Lights, Inc. Droplet generation in a microfluidic device having an optoelectrowetting configuration

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3303121A (en) 1964-07-01 1967-02-07 Exxon Research Engineering Co Additives for maintaining a dense dispersion of crystallizable material in countercurrent contact with an immiscible coolant
US3364690A (en) * 1965-05-13 1968-01-23 Exxon Research Engineering Co Process for crystallization
US3643453A (en) * 1968-12-26 1972-02-22 Shell Oil Co Selective crystallization of paraxylene in a water-alkanol mixture
GB1255346A (en) 1969-09-18 1971-12-01 Graesser Ltd R Paraxylene production
US4995900A (en) * 1988-11-30 1991-02-26 American Cyanamid Company Herbidical aqueous based microemulsion compositions
GB9126832D0 (en) 1991-12-18 1992-02-19 Sandoz Ltd Separation process
AU6175594A (en) * 1993-02-16 1994-09-14 Alliance Pharmaceutical Corporation Method of microemulsifying fluorinated oils

Also Published As

Publication number Publication date
DE69714297D1 (de) 2002-08-29
US6383233B1 (en) 2002-05-07
DK0956122T3 (da) 2002-11-18
PT956122E (pt) 2002-12-31
JP4157602B2 (ja) 2008-10-01
ATE220939T1 (de) 2002-08-15
EP0956122A1 (en) 1999-11-17
JP2000506066A (ja) 2000-05-23
DE69714297T2 (de) 2003-03-27
EP0956122B1 (en) 2002-07-24
WO1997032644A1 (en) 1997-09-12

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