ES2187857T3 - Procedimiento para preparar organosilicio-disulfanos de elevada pureza. - Google Patents
Procedimiento para preparar organosilicio-disulfanos de elevada pureza.Info
- Publication number
- ES2187857T3 ES2187857T3 ES98112029T ES98112029T ES2187857T3 ES 2187857 T3 ES2187857 T3 ES 2187857T3 ES 98112029 T ES98112029 T ES 98112029T ES 98112029 T ES98112029 T ES 98112029T ES 2187857 T3 ES2187857 T3 ES 2187857T3
- Authority
- ES
- Spain
- Prior art keywords
- alk
- formula
- hal
- phe
- iii
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000460 chlorine Substances 0.000 abstract 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- 239000011593 sulfur Substances 0.000 abstract 2
- 229910052717 sulfur Inorganic materials 0.000 abstract 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- QMMFVYPAHWMCMS-UHFFFAOYSA-N Dimethyl sulfide Chemical compound CSC QMMFVYPAHWMCMS-UHFFFAOYSA-N 0.000 abstract 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 abstract 1
- 125000000051 benzyloxy group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])O* 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 125000000000 cycloalkoxy group Chemical group 0.000 abstract 1
- 125000000753 cycloalkyl group Chemical group 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 125000001183 hydrocarbyl group Chemical group 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 150000003961 organosilicon compounds Chemical class 0.000 abstract 1
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
Abstract
LA INVENCION TRATA DE LA OBTENCION DE ORGANOSILICIODISULFANOS DE ELEVADA PUREZA, MEDIANTE LA CUAL Y EN UN PROCEDIMIENTO DE DOS ETAPAS PRIMERO SE HACE REACCIONAR AZUFRE ELEMENTAL Y UN SULFURO ALCALINO ANHIDRO EN GRAN CANTIDAD CON UN HALOALQUILALCOXISILANO Y A CONTINUACION LA CANTIDAD DE AZUFRE QUE PERMANECE SE HACE REACCIONAR A¥ADIENDO MAS SULFURO ALCALINO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19734295A DE19734295C1 (de) | 1997-08-08 | 1997-08-08 | Verfahren zur Herstellung von Organosiliciumdisulfanen hoher Reinheit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2187857T3 true ES2187857T3 (es) | 2003-06-16 |
Family
ID=7838330
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES98112029T Expired - Lifetime ES2187857T3 (es) | 1997-08-08 | 1998-06-30 | Procedimiento para preparar organosilicio-disulfanos de elevada pureza. |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US5892085A (es) |
| EP (1) | EP0895996B1 (es) |
| JP (1) | JP4391607B2 (es) |
| KR (1) | KR100647445B1 (es) |
| CN (1) | CN1116302C (es) |
| AT (1) | ATE228138T1 (es) |
| BR (1) | BR9802875A (es) |
| CA (1) | CA2244597A1 (es) |
| DE (2) | DE19734295C1 (es) |
| ES (1) | ES2187857T3 (es) |
| PT (1) | PT895996E (es) |
| RU (1) | RU2199544C2 (es) |
| TW (1) | TW513436B (es) |
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3498559B2 (ja) * | 1997-12-01 | 2004-02-16 | 信越化学工業株式会社 | 短鎖ポリスルフィドシラン混合物の製造方法 |
| DE19819373A1 (de) * | 1998-04-30 | 1999-11-04 | Degussa | Verfahren zur Herstellung von Gemischen von Organosiliciumoligosulfanen mit einem hohen Anteil an Organanosiliciumdisulfanen |
| US6518335B2 (en) * | 2000-01-05 | 2003-02-11 | Crompton Corporation | Sulfur-containing silane coupling agents |
| FR2804120A1 (fr) * | 2000-01-24 | 2001-07-27 | Michelin Soc Tech | Composition de caoutchouc pour pneumatique comportant une charge blanche renforcante et un systeme de couplage (charge blanche/elstomere) |
| FR2804121A1 (fr) | 2000-01-24 | 2001-07-27 | Michelin Soc Tech | Composition de caoutchouc pour pneumatique comportant une charge blanche renforcante et un systeme de couplage ( charge blanche/elastomere) |
| DE10009790C1 (de) * | 2000-03-01 | 2001-09-20 | Degussa | Verfahren zur Herstellung von Organosilylalkylpolysulfanen |
| JP5113970B2 (ja) | 2000-04-25 | 2013-01-09 | コンパニー ゼネラール デ エタブリッスマン ミシュラン | タイヤに使用できるゴム組成物用ブロックコポリマー |
| KR100806662B1 (ko) * | 2000-05-22 | 2008-02-28 | 소시에떼 드 테크놀로지 미쉐린 | 타이어 주행 트레드용 조성물 및 이의 제조방법 |
| WO2001092402A1 (fr) | 2000-05-26 | 2001-12-06 | Societe De Technologie Michelin | Composition de caoutchouc utilisable comme bande de roulement de pneumatique |
| CA2410156C (fr) * | 2001-03-12 | 2011-08-23 | Michelin Recherche Et Technique S.A. | Composition de caoutchouc pour bande de roulement de pneumatique |
| FR2823210B1 (fr) * | 2001-04-10 | 2005-04-01 | Rhodia Chimie Sa | Organoxysilanes polysulfures utilisables notamment en tant qu'agent de couplage, compositions d'elastomere(s) les contenant et articles en elastomere(s) prepares a partir de telles compositions |
| DE10122269A1 (de) | 2001-05-08 | 2002-11-21 | Degussa | Silanmodifizierter biopolymerer, biooligomerer, oxidischer oder silikatischer Füllstoff, Verfahren zu seiner Herstellung und seine Verwendung |
| EP1404755A1 (fr) * | 2001-06-28 | 2004-04-07 | Société de Technologie Michelin | Bande de roulement pour pneumatique renforcee d'une silice a tres basse surface specifique |
| EP1419195B1 (fr) * | 2001-06-28 | 2010-04-21 | Société de Technologie Michelin | Bande de roulement pour pneumatique renforcee d'une silice a basse surface specifique |
| US6448426B1 (en) | 2001-06-29 | 2002-09-10 | Dow Corning Corporation | Process for the preparation of sulfur-containing organosilicon compounds |
| US6384256B1 (en) | 2001-06-29 | 2002-05-07 | Dow Corning Corporation | Process for the preparation of sulfur-containing organosilicon compounds |
| US6384255B1 (en) | 2001-06-29 | 2002-05-07 | Dow Corning Corporation | Process for the preparation of sulfur-containing organosilicon compounds |
| US6534668B2 (en) | 2001-06-29 | 2003-03-18 | Dow Corning Corporation | Preparation of sulfur-containing organosilicon compounds using a buffered phase transfer catalysis process |
| FR2830014B1 (fr) | 2001-09-21 | 2005-02-18 | Rhodia Chimie Sa | Procede d'obtention de monoorganoxysilanes halogenes utilisables notamment en tant qu'intermediaires de synthese |
| US6433206B1 (en) | 2001-11-05 | 2002-08-13 | Crompton Corporation | Process for preparing silylorganomercaptans |
| WO2003046066A1 (fr) | 2001-11-26 | 2003-06-05 | Societe De Technologie Michelin | Composition de caoutchouc pour bande de roulement de pneu et son procede d'obtention |
| JP2003261580A (ja) * | 2002-03-08 | 2003-09-19 | Shin Etsu Chem Co Ltd | スルフィド鎖含有有機珪素化合物の製造方法 |
| DE10218350A1 (de) | 2002-04-25 | 2003-11-20 | Degussa | Silanmodifizierter oxidischer oder silikatischer Füllstoff, Verfahren zu seiner Herstellung und seine Verwendung |
| AU2003255474A1 (en) * | 2002-09-04 | 2004-03-29 | Michelin Recherche Et Technique S.A. | Rubber composition for tyre treads |
| JP4203718B2 (ja) * | 2002-10-31 | 2009-01-07 | 東レ・ダウコーニング株式会社 | 含ケイ素ポリサルファイド系重合体の製造方法 |
| DE10327624B3 (de) * | 2003-06-20 | 2004-12-30 | Degussa Ag | Organosiliciumverbindungen, Verfahren zu ihrer Herstellung, sowie ihre Verwendung |
| RU2391291C2 (ru) * | 2005-03-07 | 2010-06-10 | Эвоник Дегусса Гмбх | Способ получения органосиланов |
| FR2918065B1 (fr) | 2007-06-28 | 2011-04-15 | Michelin Soc Tech | Procede de preparation d'un copolymere dienique a bloc polyether, composition de caoutchouc renforcee et enveloppe de pneumatique. |
| EA012626B1 (ru) * | 2007-08-01 | 2009-10-30 | Ооо "Абидофарма" | Способ получения органосилилполисульфанов |
| CN101735262B (zh) * | 2010-01-07 | 2012-10-24 | 日照岚星化工工业有限公司 | 一种双-(γ-三甲氧基硅丙基)二硫化物的合成工艺 |
| DE102013226162A1 (de) | 2013-12-17 | 2015-06-18 | Evonik Degussa Gmbh | Silanmodifizierte Kieselsäure, Verfahren zu deren Herstellung und deren Verwendung |
| JP6378100B2 (ja) * | 2015-01-28 | 2018-08-22 | 住友ゴム工業株式会社 | タイヤ用ゴム組成物およびタイヤ |
| TWI605782B (zh) * | 2016-11-28 | 2017-11-21 | 立地企業有限公司 | 雙面均可使用之地板運動鋪巾 |
| FR3065960B1 (fr) | 2017-05-05 | 2019-06-28 | Compagnie Generale Des Etablissements Michelin | Composition de caoutchouc comprenant au moins une silice en tant que charge renforcante inorganique |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE787691A (fr) * | 1971-08-17 | 1973-02-19 | Degussa | Composes organosiliciques contenant du soufre |
| DE2141159C3 (de) * | 1971-08-17 | 1983-11-24 | Degussa Ag, 6000 Frankfurt | Schwefel enthaltende Organosiliciumverbindungen |
| DE2712866C3 (de) * | 1977-03-24 | 1980-04-30 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zum Herstellen von schwefelhaltigen Organosiliciumverbindungen |
| DE3311340A1 (de) * | 1983-03-29 | 1984-10-11 | Degussa Ag, 6000 Frankfurt | Verfahren zur herstellung von schwefelhaltigen organosiliciumverbindungen |
| JP3543352B2 (ja) * | 1994-02-16 | 2004-07-14 | 信越化学工業株式会社 | 含硫黄有機珪素化合物の製造方法 |
| US5399739A (en) * | 1994-04-18 | 1995-03-21 | Wright Chemical Corporation | Method of making sulfur-containing organosilanes |
| US5468893A (en) * | 1994-07-08 | 1995-11-21 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| US5489701A (en) * | 1994-09-28 | 1996-02-06 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| US5580919A (en) * | 1995-03-14 | 1996-12-03 | The Goodyear Tire & Rubber Company | Silica reinforced rubber composition and use in tires |
| US5596116A (en) * | 1995-09-11 | 1997-01-21 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
| DE19541404A1 (de) * | 1995-11-07 | 1997-05-15 | Degussa | Verfahren zur selektiven Synthese von Silylalkyldisulfiden |
| US5583245A (en) * | 1996-03-06 | 1996-12-10 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| DE19610281A1 (de) * | 1996-03-15 | 1997-09-18 | Bayer Ag | Verfahren zur Herstellung von polysulfidischen Silylethern |
| US5663396A (en) * | 1996-10-31 | 1997-09-02 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
| JP3465558B2 (ja) * | 1997-09-26 | 2003-11-10 | 信越化学工業株式会社 | ポリスルフィドシランの製造方法 |
-
1997
- 1997-08-08 DE DE19734295A patent/DE19734295C1/de not_active Expired - Fee Related
-
1998
- 1998-06-30 EP EP98112029A patent/EP0895996B1/de not_active Expired - Lifetime
- 1998-06-30 AT AT98112029T patent/ATE228138T1/de not_active IP Right Cessation
- 1998-06-30 ES ES98112029T patent/ES2187857T3/es not_active Expired - Lifetime
- 1998-06-30 PT PT98112029T patent/PT895996E/pt unknown
- 1998-06-30 DE DE59806324T patent/DE59806324D1/de not_active Expired - Lifetime
- 1998-08-05 TW TW087112905A patent/TW513436B/zh not_active IP Right Cessation
- 1998-08-06 JP JP22315598A patent/JP4391607B2/ja not_active Expired - Fee Related
- 1998-08-07 RU RU98115574/04A patent/RU2199544C2/ru not_active IP Right Cessation
- 1998-08-07 CA CA002244597A patent/CA2244597A1/en not_active Abandoned
- 1998-08-07 BR BR9802875-8A patent/BR9802875A/pt not_active IP Right Cessation
- 1998-08-07 KR KR1019980032113A patent/KR100647445B1/ko not_active Expired - Fee Related
- 1998-08-10 US US09/131,745 patent/US5892085A/en not_active Expired - Lifetime
- 1998-08-10 CN CN98117152A patent/CN1116302C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH11116585A (ja) | 1999-04-27 |
| KR100647445B1 (ko) | 2007-04-26 |
| CN1116302C (zh) | 2003-07-30 |
| DE59806324D1 (de) | 2003-01-02 |
| US5892085A (en) | 1999-04-06 |
| TW513436B (en) | 2002-12-11 |
| EP0895996B1 (de) | 2002-11-20 |
| ATE228138T1 (de) | 2002-12-15 |
| CN1208040A (zh) | 1999-02-17 |
| JP4391607B2 (ja) | 2009-12-24 |
| RU2199544C2 (ru) | 2003-02-27 |
| BR9802875A (pt) | 2000-05-02 |
| EP0895996A3 (de) | 2000-07-19 |
| DE19734295C1 (de) | 1999-02-25 |
| KR19990023436A (ko) | 1999-03-25 |
| PT895996E (pt) | 2003-03-31 |
| CA2244597A1 (en) | 1999-02-08 |
| EP0895996A2 (de) | 1999-02-10 |
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