ES2190474T3 - Proceso para la fabricacion de halocarburos y compuestos seleccionados, y formas azeotropicas con hf. - Google Patents

Proceso para la fabricacion de halocarburos y compuestos seleccionados, y formas azeotropicas con hf.

Info

Publication number
ES2190474T3
ES2190474T3 ES96926206T ES96926206T ES2190474T3 ES 2190474 T3 ES2190474 T3 ES 2190474T3 ES 96926206 T ES96926206 T ES 96926206T ES 96926206 T ES96926206 T ES 96926206T ES 2190474 T3 ES2190474 T3 ES 2190474T3
Authority
ES
Spain
Prior art keywords
ccl
azeotropes
production
compounds
halogened
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96926206T
Other languages
English (en)
Inventor
Ralph Thomas Baker
Ralph Newton Miller
Viacheslave Alexandrovi Petrov
Velliyur Nott Mallikarjuna Rao
Allen Capron Sievert
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of ES2190474T3 publication Critical patent/ES2190474T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
    • C07C19/10—Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO EN FASE LIQUIDA PARA LA PRODUCCION DE ADUCTOS DE ALCANO HALOGENADOS, DE FORMULA: CAR 1 R 2CBR 3 R 4 (DONDE A, B, R 1 , R 2 , R 3 Y R 4 SON TAL Y COMO SE LOS DEFINE EN LA DESCRIPCION). DICHO METODO IMPLICA LA PUESTA EN CONTACTO DEL ALCANO HALOGENADO CORRESPONDIENTE, AB, CON LA CORRESPONDIENTE OLEFINA, CR 1 R 2 = CR 3 R 4 EN UN DISOLVENTE DE DINITRILO O DE CARBONATO CICLICO, QUE DIVIDE LA MEZCLA DE REACCION EN DOS FASES LIQUIDAS, Y EN PRESENCIA DE UN SISTEMA CATALIZADOR QUE CONTIENE: (I) AL MENOS UN CATALIZADOR SELECCIONADO A PARTIR COBRE MONOVALENTE Y DIVALENTE Y, OPCIONALMENTE (II) UN PROMOTOR SELECCIONADO A PARTIR DE COMPUESTOS HETEROCICLICOS ALIFATICOS O AROMATICOS, QUE CONTIENEN AL MENOS UN ENLACE DOBLE CARBONO - NITROGENO EN EL CICLO HETEROCICLICO. CUANDO SE FORMAN HIDROCLOROFLUOROCARBUROS, EL CONTENIDO DE CLORO SE PUEDE REDUCIR HACIENDO REACCIONAR DICHOS HIDROCLOROFLUOROCARBUROS CON HF. LOS NUEVOS COMPUESTOS DESCRITOS INCLUYEN CF 3 CF SU B,2 CCL 2 CH 2 CCL 3 , CF 3 CCL 2 CH 2CH 2 CL Y CF 3 CCL 2 CH 2 CHCIF. DICHOS COMPU ESTOS SON UTILES COMO INTERMEDIARIOS PARA LA PRODUCCION DE HIDROFLUOROCARBUROS. SE DESCRIBEN ASIMISMO AZEOTROPOS DE CCLF SUB,2 CH 2 CF 3 CON HF Y AZEOTROPOS DE CF 3 CH 2 CHF 2 ; ASI COMO LOS PROCEDIMIENTOS DE PRODUCCION DE DICHOS AZEOTROPOS. SE DESCRIBE ASIMISMO UN PROCEDIMIENTO DE PURIFICACION DE CIERTOS HIDROCARBUROS FLUORADOS Y/O PRECURSORES CLORADOS DE LOS MISMOS A PARTIR DE MEZCLAS DE DICHOS COMPUESTOS CON HF.
ES96926206T 1995-08-01 1996-07-31 Proceso para la fabricacion de halocarburos y compuestos seleccionados, y formas azeotropicas con hf. Expired - Lifetime ES2190474T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US170295P 1995-08-01 1995-08-01
US1481096P 1996-04-04 1996-04-04
US1999496P 1996-06-18 1996-06-18

Publications (1)

Publication Number Publication Date
ES2190474T3 true ES2190474T3 (es) 2003-08-01

Family

ID=27356974

Family Applications (1)

Application Number Title Priority Date Filing Date
ES96926206T Expired - Lifetime ES2190474T3 (es) 1995-08-01 1996-07-31 Proceso para la fabricacion de halocarburos y compuestos seleccionados, y formas azeotropicas con hf.

Country Status (12)

Country Link
US (1) US6291730B1 (es)
EP (1) EP0876314B1 (es)
KR (2) KR100516407B1 (es)
CN (1) CN1082039C (es)
AU (1) AU6643696A (es)
BR (1) BR9609924A (es)
CA (1) CA2228287C (es)
DE (1) DE69626415T2 (es)
ES (1) ES2190474T3 (es)
MX (1) MX9800871A (es)
TW (1) TW421643B (es)
WO (1) WO1997005089A1 (es)

Families Citing this family (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2933014B2 (ja) * 1996-01-23 1999-08-09 ダイキン工業株式会社 ペンタフルオロプロパンとフッ化水素の共沸混合物およびペンタフルオロプロパンの分離精製方法
US5817893A (en) * 1996-06-18 1998-10-06 E. I. Du Pont De Nemours And Company Processes for the manufacture and purification of 1,1,2,2,3,3,4,4-octafluorobutane and by-products
US6001796A (en) * 1996-07-03 1999-12-14 Alliedsignal Inc. Azeotrope-like compositions of 1,1,1,3,3-pentafluoropropane and hydrogen fluoride
US6040487A (en) * 1996-07-31 2000-03-21 E. I. Du Pont De Nemours And Company Process for the manufacture of halocarbons
CA2277169C (en) 1997-01-16 2007-10-02 E.I. Du Pont De Nemours And Company Process for the manufacture of halocarbons
US6376727B1 (en) 1997-06-16 2002-04-23 E. I. Du Pont De Nemours And Company Processes for the manufacture of 1,1,1,3,3-pentafluoropropene, 2-chloro-pentafluoropropene and compositions comprising saturated derivatives thereof
ES2224359T3 (es) 1997-02-19 2005-03-01 E. I. Du Pont De Nemours And Company Procesos para producir 1,1,1,3,3,-pentafluoropropano, 2-cloro-pentafluoropropano.sp.
WO1998050330A1 (fr) * 1997-05-05 1998-11-12 Solvay (Societe Anonyme) Procede de preparation d'hydrocarbures halogenes
JP4111548B2 (ja) 1997-05-05 2008-07-02 ソルヴェイ （ソシエテ アノニム） １，１，１，３，３−ペンタクロロブタンの調製法
BE1011319A3 (fr) * 1997-05-05 1999-07-06 Solvay Procede de preparation d'hydrocarbures halogenes.
US5902912A (en) * 1997-06-26 1999-05-11 Alliedsignal Inc. Process for preparing hydrofluorocarbons
ES2189240T3 (es) 1997-08-08 2003-07-01 Solvay Procedimiento de preparacion de hidrocarburos halogenados.
FR2768717B1 (fr) 1997-09-24 1999-11-12 Solvay Procede de separation de fluorure d'hydrogene de ses melanges avec un hydrofluoroalcane contenant de 3 a 6 atomes de carbone
EP1027313A1 (en) * 1997-10-17 2000-08-16 E.I. Du Pont De Nemours And Company Separating 1,1,1,3,3-pentafluoropropane from hydrogen fluoride
US5918481A (en) * 1997-11-20 1999-07-06 Alliedsignal Inc. Process for separating hydrogen fluoride from fluorocarbons
US6100229A (en) * 1998-01-12 2000-08-08 Alliedsignal Inc. Compositions of 1,1,1,3,3,-pentafluoropropane and chlorinated ethylenes
BE1012268A3 (fr) 1998-11-05 2000-08-01 Solvay Procede de preparation d'hydrocarbures halogenes.
ATE430119T1 (de) 1998-12-18 2009-05-15 Solvay Verfahren zur trennung einer mischung, die mindestens ein hydrofluoralkan und fluorwasserstoff enthält, und verfahren zur herstellung eines hydrofluoralkans
ES2320850T5 (es) 1999-10-06 2012-07-03 Solvay (Société Anonyme) Procedimiento de preparación de hidrocarburos halogenados en presencia de un cocatalizador
US6500795B2 (en) * 2001-01-24 2002-12-31 Honeywell International Inc. Azeotrope-like composition of 1-chloro-1,3,3,3-tetrafluoropropane and hydrogen fluoride
JP4511827B2 (ja) 2001-06-01 2010-07-28 ハネウェル・インターナショナル・インコーポレーテッド １，１，１，３，３−ペンタフルオロブタンと弗化水素との共沸混合物様組成物
US6500995B1 (en) 2001-06-14 2002-12-31 Vulcan Chemicals Water-enhanced production of 1,1,1,3,3,-pentachloropropane
US20030028057A1 (en) * 2001-07-20 2003-02-06 Stephen Owens Methods and materials for the preparation and purification of halogenated hydrocarbons
US7094936B1 (en) 2001-07-20 2006-08-22 Great Lakes Chemical Corporation Process for preparing halogenated alkanes
US20050177012A1 (en) * 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
WO2005037742A1 (en) * 2003-10-14 2005-04-28 E.I. Dupont De Nemours And Company Process for the preparation of 1,1,1,3,3,3-hexafluoropropane and at least one of 1,1,1,2,3,3-hexafluoropropane and 1,1,1,2,3,3,3-heptafluoropropane
EP1673326A1 (en) 2003-10-14 2006-06-28 E.I. Dupont De Nemours And Company Process for the preparation of 1,1,1,3,3-pentafluoropropane and 1,1,1,3,3,3-hexafluoropropane
JP2007508376A (ja) 2003-10-14 2007-04-05 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー １，１，１，３，３−ペンタフルオロプロパンおよび１，１，１，２，３−ペンタフルオロプロパンの調製法
WO2005080303A1 (en) * 2004-01-21 2005-09-01 Great Lakes Chemical Corporation Product stream processing methods, product stream processing systems, and mixtures
US20060036117A1 (en) * 2004-08-10 2006-02-16 Mitchel Cohn Catalyst preparation processes, catalyst regeneration processes, halocarbon production processes, and halocarbon production systems
WO2006069105A1 (en) * 2004-12-22 2006-06-29 E.I. Dupont De Nemours And Company Process for the production of 1,1,1,3,3,3-hexafluoropropane
DE102005012632A1 (de) * 2005-03-18 2006-09-21 Infineon Technologies Ag Verfahren und Schaltungsanordnung zur geschützten Übertragung von Datenworten
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US7388117B2 (en) * 2005-11-01 2008-06-17 E.I. Du Pont De Nemours And Company Azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof
US7709438B2 (en) * 2005-11-01 2010-05-04 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising nonafluoropentene and hydrogen fluoride and uses thereof
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GB0806422D0 (en) 2008-04-09 2008-05-14 Ineos Fluor Holdings Ltd Process
CN101522597B (zh) 2006-10-03 2013-05-29 墨西哥化学阿玛科股份有限公司 通过脱卤化氢制备c3-c6(氢)氟烯烃的方法
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TW200844075A (en) * 2006-10-31 2008-11-16 Du Pont Processes for the production of fluoropropanes and halopropenes
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GB0806419D0 (en) 2008-04-09 2008-05-14 Ineos Fluor Holdings Ltd Process
GB0806389D0 (en) 2008-04-09 2008-05-14 Ineos Fluor Holdings Ltd Process
JP5365064B2 (ja) * 2008-05-12 2013-12-11 日本ゼオン株式会社 新規含ハロゲン化合物及びそれらの製造方法
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RU2010147002A (ru) * 2010-11-17 2012-05-27 Е.И.Дюпон де Немур энд Компани (US) Каталитический синтез галогенированных углеводородов
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CN107434759B (zh) * 2016-05-25 2019-12-13 浙江省化工研究院有限公司 一种制备1,1,3,3,3-五氟丙烯的方法
US11731925B2 (en) * 2016-07-27 2023-08-22 The Chemours Company Fc, Llc Process for producing halogenated olefins
GB201615209D0 (en) 2016-09-07 2016-10-19 Mexichem Fluor Sa De Cv Catalyst and process using the catalyst
GB201615197D0 (en) 2016-09-07 2016-10-19 Mexichem Fluor Sa De Cv Catalyst and process using the catalyst
CN109721465B (zh) * 2018-12-17 2022-03-15 西安近代化学研究所 一种制备反式-1,1,1,4,4,4-六氟-2-丁烯的方法
GB2580623A (en) 2019-01-17 2020-07-29 Mexichem Fluor Sa De Cv Method
CN115210202B (zh) * 2020-03-04 2025-01-21 科慕埃弗西有限公司 用于制备(z)-1,1,1,4,4,4-六氟-2-丁烯和中间体的方法
WO2022225830A1 (en) 2021-04-19 2022-10-27 The Chemours Company Fc, Llc Compositions containing 3,3,3-trifluoropropene (1243zf) and methods for making and using the compositions
KR102730416B1 (ko) 2022-01-25 2024-11-15 엘지전자 주식회사 압축기용 어큐뮬레이터 고정정치 및 이를 구비한 압축기
AU2025212227A1 (en) * 2024-01-22 2026-05-28 The Chemours Company Fc, Llc Compositions of and processes for 2,2,4-trichloro-1,1,1-trifluorobutane
WO2025264752A1 (en) 2024-06-21 2025-12-26 The Chemours Company Fc, Llc Process for producing hydrochloro(fluoro)carbon compounds

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Also Published As

Publication number Publication date
TW421643B (en) 2001-02-11
KR19990036037A (ko) 1999-05-25
CA2228287C (en) 2008-06-10
AU6643696A (en) 1997-02-26
US6291730B1 (en) 2001-09-18
EP0876314A1 (en) 1998-11-11
CA2228287A1 (en) 1997-02-13
DE69626415T2 (de) 2003-09-25
CN1082039C (zh) 2002-04-03
KR100517576B1 (ko) 2005-12-21
DE69626415D1 (de) 2003-04-03
KR100516407B1 (ko) 2005-09-27
EP0876314B1 (en) 2003-02-26
WO1997005089A1 (en) 1997-02-13
KR20050074649A (ko) 2005-07-18
MX9800871A (es) 1998-04-30
BR9609924A (pt) 1999-06-08
CN1196716A (zh) 1998-10-21

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