ES2193386T3 - PROCEDURE TO PRODUCE A DETERGENT COMPOSITION WITHOUT USING A TOWER. - Google Patents

PROCEDURE TO PRODUCE A DETERGENT COMPOSITION WITHOUT USING A TOWER.

Info

Publication number
ES2193386T3
ES2193386T3 ES97931058T ES97931058T ES2193386T3 ES 2193386 T3 ES2193386 T3 ES 2193386T3 ES 97931058 T ES97931058 T ES 97931058T ES 97931058 T ES97931058 T ES 97931058T ES 2193386 T3 ES2193386 T3 ES 2193386T3
Authority
ES
Spain
Prior art keywords
procedure
tower
produce
detergent composition
granular
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97931058T
Other languages
Spanish (es)
Inventor
Wayne Edward Beimesch
Jose Francisco Correa Romo
Steven Barrett Rogers
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Application granted granted Critical
Publication of ES2193386T3 publication Critical patent/ES2193386T3/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065—High-density particulate detergent compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146—Sulfuric acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29—Sulfates of polyoxyalkylene ethers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO QUE NO UTILIZA UNA TORRE, PARA PREPARAR DE FORMA CONTINUA UNA COMPOSICION DETERGENTE GRANULAR DE DENSIDAD APROX. DE 600 G/L. DICHO PROCEDIMIENTO COMPRENDE LAS SIGUIENTES FASES: (A) (I) DISPERSAR UN TENSIOACTIVO Y REVESTIR DICHO TENSIOACTIVO CON POLVO FINO, DE DIAMETRO COMPRENDIDO ENTRE 0,1 Y 500 MICRONES, EN UN MEZCLADOR, CON LO QUE SE FORMAN UNOS PRIMEROS AGLOMERADOS, (B) GRANULAR DICHOS PRIMEROS AGLOMERADOS EN UNO O MAS APARATOS DE FLUIDIFICACION.THE INVENTION REFERS TO A PROCEDURE THAT DOES NOT USE A TOWER, TO PREPARE A DETERGENT GRANULAR COMPOSITION OF APPROX DENSITY CONTINUOUSLY. OF 600 G / L. SUCH PROCEDURE INCLUDES THE FOLLOWING PHASES: (A) (I) DISPERSE A TENSIOACTIVE AND COVER THE SENSITIVE VOLTAGE WITH FINE POWDER, DIAMETER INCLUDED BETWEEN 0.1 AND 500 MICRONS, IN A MIXER, WITH WHICH ONE FIRST BATTERIES ARE FORMED ) GRANULAR SUCH FIRST AGLOMERATED IN ONE OR MORE FLUIDIFICATION DEVICES.

ES97931058T 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION WITHOUT USING A TOWER. Expired - Lifetime ES2193386T3 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US1996/015881 WO1998014549A1 (en) 1996-10-04 1996-10-04 Process for making a low density detergent composition by non-tower process

Publications (1)

Publication Number Publication Date
ES2193386T3 true ES2193386T3 (en) 2003-11-01

Family

ID=22255901

Family Applications (5)

Application Number Title Priority Date Filing Date
ES97931058T Expired - Lifetime ES2193386T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION WITHOUT USING A TOWER.
ES97929815T Expired - Lifetime ES2201305T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR MANUFACTURING A DETERGENT COMPOSITION WITHOUT USING TOWERS.
ES97928872T Expired - Lifetime ES2212109T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO MANUFACTURE A DETERGENT COMPOSITION BY A TOWER-FREE PROCEDURE.
ES97931056T Expired - Lifetime ES2210544T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION THROUGH A PROCEDURE WITHOUT TOWERS.
ES97928871T Expired - Lifetime ES2178778T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR OBTAINING A DETERGENT COMPOSITION BY A TOWER-FREE PROCESS.

Family Applications After (4)

Application Number Title Priority Date Filing Date
ES97929815T Expired - Lifetime ES2201305T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR MANUFACTURING A DETERGENT COMPOSITION WITHOUT USING TOWERS.
ES97928872T Expired - Lifetime ES2212109T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO MANUFACTURE A DETERGENT COMPOSITION BY A TOWER-FREE PROCEDURE.
ES97931056T Expired - Lifetime ES2210544T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION THROUGH A PROCEDURE WITHOUT TOWERS.
ES97928871T Expired - Lifetime ES2178778T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR OBTAINING A DETERGENT COMPOSITION BY A TOWER-FREE PROCESS.

Country Status (12)

Country Link
EP (9) EP0929645A1 (en)
JP (9) JP3305327B2 (en)
CN (8) CN1133738C (en)
AR (6) AR010729A1 (en)
AT (5) ATE246726T1 (en)
AU (9) AU7388196A (en)
BR (7) BR9612732A (en)
CA (9) CA2267291C (en)
DE (5) DE69721287T2 (en)
ES (5) ES2193386T3 (en)
MX (2) MX219076B (en)
WO (9) WO1998014549A1 (en)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2150113T3 (en) * 1995-04-03 2000-11-16 Novartis Ag DERIVATIVES OF PIRAZOLE AND PROCEDURES FOR THE PREPARATION OF THE SAME.
GB9526097D0 (en) * 1995-12-20 1996-02-21 Unilever Plc Process
GB9712583D0 (en) 1997-06-16 1997-08-20 Unilever Plc Production of detergent granulates
GB9712580D0 (en) * 1997-06-16 1997-08-20 Unilever Plc Production of detergent granulates
GB9713748D0 (en) * 1997-06-27 1997-09-03 Unilever Plc Production of detergent granulates
CA2296320C (en) 1997-07-14 2003-05-27 The Procter & Gamble Company Process for making a low density detergent composition by controlled agglomeration in a fluid bed dryer
US6258773B1 (en) 1997-07-14 2001-07-10 The Procter & Gamble Company Process for making a low density detergent composition by controlling agglomeration via particle size
DE69823668T2 (en) 1997-07-15 2005-04-07 The Procter & Gamble Company, Cincinnati METHOD FOR PRODUCING HIGHLY CONCENTRATED DETERGENT AGGLOMERATES BY MULTIPLE INJECTION OF TENSID PASTE
US6440342B1 (en) 1998-07-08 2002-08-27 The Procter & Gamble Company Process for making a low density detergent composition by controlling nozzle height in a fluid bed dryer
EP1105455B1 (en) 1998-08-20 2006-08-16 The Procter & Gamble Company High density detergent-making process involving a moderate speed mixer/densifier
US6794354B1 (en) * 1998-09-18 2004-09-21 The Procter & Gamble Company Continuous process for making detergent composition
CA2346926A1 (en) 1998-10-26 2000-05-04 Christopher Andrew Morrison Processes for making granular detergent composition having improved appearance and solubility
GB9825558D0 (en) * 1998-11-20 1999-01-13 Unilever Plc Granular detergent components and particulate detergent compositions containing them
GB9913546D0 (en) 1999-06-10 1999-08-11 Unilever Plc Granular detergent component containing zeolite map and laundry detergent compositions containing it
DE60012928T2 (en) * 1999-06-21 2005-08-18 The Procter & Gamble Company, Cincinnati PROCESS FOR PRODUCING GRANULAR DETERGENT COMPOSITIONS
US6894018B1 (en) 1999-06-21 2005-05-17 The Procter & Gamble Company Process for making granular detergent in a fluidized bed granulator having recycling of improperly sized particles
GB0009877D0 (en) † 2000-04-20 2000-06-07 Unilever Plc Granular detergent component and process for its preparation
EP2123742A1 (en) 2008-05-14 2009-11-25 The Procter and Gamble Company A solid laundry detergent composition comprising light density silicate salt
WO2011061045A1 (en) 2009-11-20 2011-05-26 Unilever Nv Detergent granule and its manufacture
EP3140386B1 (en) 2014-04-10 2024-02-28 The Procter & Gamble Company Composite detergent granules and laundry compositions comprising the same
CN111655829A (en) * 2018-01-26 2020-09-11 埃科莱布美国股份有限公司 Curing Liquid Amine Oxide, Betaine and/or Sultaine Surfactants with Binder and Optional Carrier
EP4600335A3 (en) 2018-01-26 2025-08-20 Ecolab USA Inc. Solidifying liquid betaine and/or sultaine surfactants with a sodium chloride carrier
CN121896042A (en) * 2018-01-26 2026-04-21 埃科莱布美国股份有限公司 Solidifying liquid anionic surfactant

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3625902A (en) * 1968-10-11 1971-12-07 Stauffer Chemical Co Method of preparing agglomerated detergent composition
US4169806A (en) * 1978-08-09 1979-10-02 The Procter & Gamble Company Agglomeration process for making granular detergents
US4992079A (en) * 1986-11-07 1991-02-12 Fmc Corporation Process for preparing a nonphosphate laundry detergent
GB2209172A (en) * 1987-08-28 1989-05-04 Unilever Plc Preparation of solid particulate components for detergents
KR0170424B1 (en) * 1990-07-05 1999-01-15 호르스트 헤를레,요한 글라슬 Method for preparing surface active agent granules for detergents and cleaning agents
FI932171A7 (en) * 1990-11-14 1993-05-13 Procter & Gamble Phosphate-free automatic laundry detergent compositions containing oxygen bleach systems and method for their preparation
EP0555622B1 (en) * 1992-02-14 1997-07-09 The Procter & Gamble Company Process for making detergent granules by neutralisation of sulphonic acids
ES2179054T5 (en) 1992-06-15 2006-06-16 THE PROCTER & GAMBLE COMPANY PROCEDURE TO PREPARE COMPACT DETERGENT COMPOSITIONS.
EP0578872B1 (en) * 1992-07-15 1998-10-14 The Procter & Gamble Company Detergent compositions
EP0723581A1 (en) 1993-10-15 1996-07-31 The Procter & Gamble Company Continuous process for making high density detergent granules
GB9322530D0 (en) 1993-11-02 1993-12-22 Unilever Plc Process for the production of a detergent composition
DE69425550T2 (en) 1994-01-17 2001-04-26 The Procter & Gamble Company, Cincinnati Process for the production of detergent granules
US5489392A (en) * 1994-09-20 1996-02-06 The Procter & Gamble Company Process for making a high density detergent composition in a single mixer/densifier with selected recycle streams for improved agglomerate properties
US5516448A (en) * 1994-09-20 1996-05-14 The Procter & Gamble Company Process for making a high density detergent composition which includes selected recycle streams for improved agglomerate
US5554587A (en) 1995-08-15 1996-09-10 The Procter & Gamble Company Process for making high density detergent composition using conditioned air

Also Published As

Publication number Publication date
ATE246726T1 (en) 2003-08-15
AU3303197A (en) 1998-04-24
ES2210544T3 (en) 2004-07-01
CA2268067C (en) 2004-01-06
CN1239995A (en) 1999-12-29
CN1239992A (en) 1999-12-29
JP2000503716A (en) 2000-03-28
CA2268063A1 (en) 1998-04-09
CN1239991A (en) 1999-12-29
ATE223476T1 (en) 2002-09-15
AU3478397A (en) 1998-04-24
CA2268067A1 (en) 1998-04-09
AU3478497A (en) 1998-04-24
CN1156561C (en) 2004-07-07
DE69726439D1 (en) 2004-01-08
EP0929650A1 (en) 1999-07-21
CN1239507A (en) 1999-12-22
CN1156560C (en) 2004-07-07
CA2268052C (en) 2003-12-30
BR9712490A (en) 1999-10-19
ATE255160T1 (en) 2003-12-15
EP0929648B1 (en) 2002-09-04
ES2212109T3 (en) 2004-07-16
EP0929645A1 (en) 1999-07-21
JP3299984B2 (en) 2002-07-08
CN1133738C (en) 2004-01-07
BR9711861A (en) 1999-08-24
CA2268062A1 (en) 1998-04-09
WO1998014554A1 (en) 1998-04-09
BR9612732A (en) 1999-08-24
CA2268068A1 (en) 1998-04-09
ATE238409T1 (en) 2003-05-15
CA2267291C (en) 2002-12-10
CA2268068C (en) 2003-06-03
AR010509A1 (en) 2000-06-28
EP0929649B1 (en) 2003-11-26
DE69715224D1 (en) 2002-10-10
JP3299981B2 (en) 2002-07-08
AU3378597A (en) 1998-04-24
EP0929655A1 (en) 1999-07-21
JP2000503720A (en) 2000-03-28
CN1239994A (en) 1999-12-29
CA2268055C (en) 2004-02-03
AU7388196A (en) 1998-04-24
CA2268062C (en) 2002-11-12
DE69726440D1 (en) 2004-01-08
DE69715224T2 (en) 2003-08-07
JP2000503718A (en) 2000-03-28
CN1239508A (en) 1999-12-22
CN1156562C (en) 2004-07-07
MX9903193A (en) 2000-01-31
ES2201305T3 (en) 2004-03-16
JP3299986B2 (en) 2002-07-08
WO1998014549A1 (en) 1998-04-09
CA2268060A1 (en) 1998-04-09
JP3345022B2 (en) 2002-11-18
JP2000503715A (en) 2000-03-28
CA2268063C (en) 2002-10-29
AU3478597A (en) 1998-04-24
EP0929648A1 (en) 1999-07-21
BR9713246A (en) 1999-11-03
BR9712492A (en) 1999-10-19
AU3303097A (en) 1998-04-24
BR9713249A (en) 1999-11-03
DE69723986T2 (en) 2004-06-03
WO1998014556A1 (en) 1998-04-09
CA2267424C (en) 2004-01-06
EP0929653B1 (en) 2003-04-23
MX9903195A (en) 1999-09-30
EP0929651B1 (en) 2003-11-26
JP3299982B2 (en) 2002-07-08
WO1998014557A1 (en) 1998-04-09
EP0929651A1 (en) 1999-07-21
AR010729A1 (en) 2000-07-12
CA2267291A1 (en) 1998-04-09
AR010507A1 (en) 2000-06-28
WO1998014558A1 (en) 1998-04-09
AR010508A1 (en) 2000-06-28
EP0929650B1 (en) 2003-08-06
JP3299983B2 (en) 2002-07-08
MX219077B (en) 2004-02-10
DE69723986D1 (en) 2003-09-11
DE69721287D1 (en) 2003-05-28
JP2000503719A (en) 2000-03-28
EP0929654A1 (en) 1999-07-21
ES2178778T3 (en) 2003-01-01
WO1998014552A1 (en) 1998-04-09
CN1239993A (en) 1999-12-29
JP3299987B2 (en) 2002-07-08
AU3568397A (en) 1998-04-24
ATE255159T1 (en) 2003-12-15
JP2000503721A (en) 2000-03-28
CA2268052A1 (en) 1998-04-09
AR010511A1 (en) 2000-06-28
JP2000503717A (en) 2000-03-28
WO1998014551A1 (en) 1998-04-09
JP3299985B2 (en) 2002-07-08
CN1239506A (en) 1999-12-22
AU3478297A (en) 1998-04-24
EP0929649A1 (en) 1999-07-21
EP0929653A1 (en) 1999-07-21
MX219076B (en) 2004-02-10
CA2268060C (en) 2003-04-22
CA2267424A1 (en) 1998-04-09
JP2000504062A (en) 2000-04-04
DE69721287T2 (en) 2004-03-11
DE69726440T2 (en) 2004-09-09
CA2268055A1 (en) 1998-04-09
WO1998014553A1 (en) 1998-04-09
EP0929652A1 (en) 1999-07-21
CN1133739C (en) 2004-01-07
DE69726439T2 (en) 2004-09-09
AR010510A1 (en) 2000-06-28
WO1998014555A1 (en) 1998-04-09
JP3305327B2 (en) 2002-07-22
JP2000507632A (en) 2000-06-20
BR9711865A (en) 1999-08-24
CN1156563C (en) 2004-07-07

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