ES2197785A1 - Procedimiento para depositar recubrimientos de metales y oxidos metalicos. - Google Patents

Procedimiento para depositar recubrimientos de metales y oxidos metalicos.

Info

Publication number
ES2197785A1
ES2197785A1 ES200102825A ES200102825A ES2197785A1 ES 2197785 A1 ES2197785 A1 ES 2197785A1 ES 200102825 A ES200102825 A ES 200102825A ES 200102825 A ES200102825 A ES 200102825A ES 2197785 A1 ES2197785 A1 ES 2197785A1
Authority
ES
Spain
Prior art keywords
metal
coatings
precursor solutions
procedure
temperatures
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
ES200102825A
Other languages
English (en)
Other versions
ES2197785B1 (es
Inventor
Sabio Angel Morales
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT
Original Assignee
Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT filed Critical Centro de Investigaciones Energeticas Medioambientales y Tecnologicas CIEMAT
Priority to ES200102825A priority Critical patent/ES2197785B1/es
Priority to EP02380267A priority patent/EP1321539A3/en
Publication of ES2197785A1 publication Critical patent/ES2197785A1/es
Application granted granted Critical
Publication of ES2197785B1 publication Critical patent/ES2197785B1/es
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1216—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/06—Surface treatment of glass, not in the form of fibres or filaments, by coating with metals
    • C03C17/10—Surface treatment of glass, not in the form of fibres or filaments, by coating with metals by deposition from the liquid phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • C03C17/23—Oxides
    • C03C17/25—Oxides by deposition from the liquid phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/20—Materials for coating a single layer on glass
    • C03C2217/21—Oxides
    • C03C2217/229—Non-specific enumeration
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/10—Deposition methods
    • C03C2218/11—Deposition methods from solutions or suspensions

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Chemically Coating (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)

Abstract

Procedimiento para depositar recubrimientos de metales y óxidos metálicos. El procedimiento permite producir recubrimientos metálicos y de óxidos metálicos a partir de soluciones precursoras, como ocurre en la técnica denominada sol-gel, pero con la ventaja de que las soluciones precursoras no incorporan alcóxidos metálicos a hidrolizar, por lo que su estabilidad a lo largo del tiempo es excelente. Las soluciones precursoras de los recubrimientos se preparan disolviendo en etanol una sal del metal, con un agente complejante para favorecer su estabilidad y/o un aditivo para dotar a la solución de las propiedades necesarias para depositarlo homogéneamente sobre un sustrato. Las soluciones precursoras, se depositan por extracción del sustrato a velocidad constante, centrifugación o pulverización, se secan a temperaturas entre 50 y 150ºC y se densifican mediante un tratamiento térmico a temperaturas entre 300 y 600ºC, con un tiempo variable entre 10 a 60 minutos.
ES200102825A 2001-12-18 2001-12-18 Procedimiento para depositar recubrimientos de metales y oxidos metalicos. Expired - Fee Related ES2197785B1 (es)

Priority Applications (2)

Application Number Priority Date Filing Date Title
ES200102825A ES2197785B1 (es) 2001-12-18 2001-12-18 Procedimiento para depositar recubrimientos de metales y oxidos metalicos.
EP02380267A EP1321539A3 (en) 2001-12-18 2002-12-18 Process to deposit metal and metal oxide coatings

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES200102825A ES2197785B1 (es) 2001-12-18 2001-12-18 Procedimiento para depositar recubrimientos de metales y oxidos metalicos.

Publications (2)

Publication Number Publication Date
ES2197785A1 true ES2197785A1 (es) 2004-01-01
ES2197785B1 ES2197785B1 (es) 2005-03-01

Family

ID=8499783

Family Applications (1)

Application Number Title Priority Date Filing Date
ES200102825A Expired - Fee Related ES2197785B1 (es) 2001-12-18 2001-12-18 Procedimiento para depositar recubrimientos de metales y oxidos metalicos.

Country Status (2)

Country Link
EP (1) EP1321539A3 (es)
ES (1) ES2197785B1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10359884A1 (de) * 2003-12-19 2005-07-21 Ferro Gmbh Substrate mit einer transparenten, spiegelnden Metalloxid-Teilbeschichtung, deren Herstellung und Anwendung
WO2011027425A1 (ja) 2009-09-02 2011-03-10 東芝三菱電機産業システム株式会社 金属酸化膜の成膜方法、金属酸化膜および金属酸化膜の成膜装置
US11352292B2 (en) * 2019-01-30 2022-06-07 Ppg Industries Ohio, Inc. Method for preparing optical articles with multi-layer antireflective coatings

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3515600A (en) * 1966-10-19 1970-06-02 Hooker Chemical Corp Metal treating process and composition
US5273776A (en) * 1991-12-06 1993-12-28 Mitsubishi Materials Corporation Method for forming thermistor thin film
JPH1087345A (ja) * 1996-09-09 1998-04-07 Teikoku Chem Ind Corp Ltd 酸化チタン薄膜形成用塗布液組成物

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH026335A (ja) * 1988-01-12 1990-01-10 Toray Ind Inc チタン酸ジルコン酸鉛薄膜の形成方法
WO1991009151A1 (en) * 1989-12-08 1991-06-27 Akzo N.V. Method of metallizing substrates by chemical redox
CN1137285C (zh) * 1997-04-30 2004-02-04 高松研究所 金属糊和金属膜的制造方法
DE19736925A1 (de) * 1996-08-26 1998-03-05 Central Glass Co Ltd Hydrophiler Film und Verfahren zur Erzeugung desselben auf einem Substrat

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3515600A (en) * 1966-10-19 1970-06-02 Hooker Chemical Corp Metal treating process and composition
US5273776A (en) * 1991-12-06 1993-12-28 Mitsubishi Materials Corporation Method for forming thermistor thin film
JPH1087345A (ja) * 1996-09-09 1998-04-07 Teikoku Chem Ind Corp Ltd 酸化チタン薄膜形成用塗布液組成物

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
[en linea] [recuperado el 26.11.2003] Recuperado de: EPO, PAJ Database & JP 10087345 A (TEIKOKU CHEM. IND. CORP LTD) 07.04.1998 (resumen) *

Also Published As

Publication number Publication date
ES2197785B1 (es) 2005-03-01
EP1321539A2 (en) 2003-06-25
EP1321539A3 (en) 2004-06-09

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