ES2197796A1 - CIRCUIT FOR THE CHARACTERIZATION OF RESISTANT QUARTZ CRYSTAL SENSORS IN FLUID MEDIA. - Google Patents
CIRCUIT FOR THE CHARACTERIZATION OF RESISTANT QUARTZ CRYSTAL SENSORS IN FLUID MEDIA.Info
- Publication number
- ES2197796A1 ES2197796A1 ES200200306A ES200200306A ES2197796A1 ES 2197796 A1 ES2197796 A1 ES 2197796A1 ES 200200306 A ES200200306 A ES 200200306A ES 200200306 A ES200200306 A ES 200200306A ES 2197796 A1 ES2197796 A1 ES 2197796A1
- Authority
- ES
- Spain
- Prior art keywords
- circuit
- sensor
- quartz crystal
- quartz
- fluid media
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000010453 quartz Substances 0.000 title abstract 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title abstract 5
- 239000013078 crystal Substances 0.000 title abstract 4
- 239000012530 fluid Substances 0.000 title abstract 3
- 238000012512 characterization method Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000013626 chemical specie Substances 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 238000001514 detection method Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 230000003068 static effect Effects 0.000 abstract 1
Landscapes
- Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
Abstract
Sistema de caracterización de sensores de cristal de cuarzo resonante en medios fluidos, y procedimiento de calibración y compensación de la capacidad del cristal de cuarzo. El sistema de la invención suministra continua y automáticamente la frecuencia de resonancia serie y la resistencia de la rama dinámica y de un resonador de cuarzo. La frecuencia suministrada es independiente de la resistencia dinámica y de la capacidad estática del cristal. El sistema está diseñado para compensar los efectos capacitivos en paralelo con el sensor, incorporando un bucle de enganche de fase y un circuito que proporciona la resistencia dinámica del resonador, además, incluye procedimientos para la calibración del circuito externo al sensor y para la compensación capacitiva. La invención tiene utilidad en aplicaciones en que se utilizan resonadores de cuarzo como sensores, tales como: para la determinación de las propiedades visco-elásticas de fluidos, para la detección de especies químicas específicas en entorno gaseoso o en disolución mediante el recubrimiento adecuado del sensor, entre otras.Characterization system of resonant quartz crystal sensors in fluid media, and procedure for calibration and compensation of the quartz crystal capacity. The system of the invention continuously and automatically supplies the series resonance frequency and the resistance of the dynamic branch and of a quartz resonator. The supplied frequency is independent of the dynamic resistance and the static capacity of the crystal. The system is designed to compensate the capacitive effects in parallel with the sensor, incorporating a phase-locked loop and a circuit that provides the dynamic resistance of the resonator, in addition, it includes procedures for the calibration of the external circuit to the sensor and for capacitive compensation. . The invention is useful in applications in which quartz resonators are used as sensors, such as: for the determination of the visco-elastic properties of fluids, for the detection of specific chemical species in a gaseous environment or in solution by means of the appropriate coating of the sensor. , among other.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200200306A ES2197796B1 (en) | 2002-01-31 | 2002-01-31 | CHARACTERIZATION SYSTEM OF RESISTANT CRYSTAL SENSORS IN FLUID MEDIA, AND CALIBRATION AND COMPENSATION PROCEDURE OF THE QUARTZ CRYSTAL CAPACITY. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200200306A ES2197796B1 (en) | 2002-01-31 | 2002-01-31 | CHARACTERIZATION SYSTEM OF RESISTANT CRYSTAL SENSORS IN FLUID MEDIA, AND CALIBRATION AND COMPENSATION PROCEDURE OF THE QUARTZ CRYSTAL CAPACITY. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2197796A1 true ES2197796A1 (en) | 2004-01-01 |
| ES2197796B1 ES2197796B1 (en) | 2005-02-16 |
Family
ID=30470524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES200200306A Expired - Fee Related ES2197796B1 (en) | 2002-01-31 | 2002-01-31 | CHARACTERIZATION SYSTEM OF RESISTANT CRYSTAL SENSORS IN FLUID MEDIA, AND CALIBRATION AND COMPENSATION PROCEDURE OF THE QUARTZ CRYSTAL CAPACITY. |
Country Status (1)
| Country | Link |
|---|---|
| ES (1) | ES2197796B1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010149811A1 (en) | 2009-06-23 | 2010-12-29 | Universidad Politécnica De Valencia | Method and device for nanogravimetry in fluid media using piezoelectric resonators |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4447782A (en) * | 1982-03-17 | 1984-05-08 | Transat Corp. | Apparatus for automatic measurement of equivalent circuit parameters of piezoelectric resonators |
| US5117192A (en) * | 1990-01-12 | 1992-05-26 | Leybold Inficon Inc. | Control circuitry for quartz crystal deposition monitor |
| WO1996035103A1 (en) * | 1995-05-04 | 1996-11-07 | Michael Rodahl | A piezoelectric crystal microbalance device |
| ES2153740A1 (en) * | 1998-07-08 | 2001-03-01 | Univ Valencia Politecnica | System for compensating the effects of viscous friction in the measurement of the resonance frequency in a piezometric crystal in a liquid |
-
2002
- 2002-01-31 ES ES200200306A patent/ES2197796B1/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4447782A (en) * | 1982-03-17 | 1984-05-08 | Transat Corp. | Apparatus for automatic measurement of equivalent circuit parameters of piezoelectric resonators |
| US5117192A (en) * | 1990-01-12 | 1992-05-26 | Leybold Inficon Inc. | Control circuitry for quartz crystal deposition monitor |
| WO1996035103A1 (en) * | 1995-05-04 | 1996-11-07 | Michael Rodahl | A piezoelectric crystal microbalance device |
| ES2153740A1 (en) * | 1998-07-08 | 2001-03-01 | Univ Valencia Politecnica | System for compensating the effects of viscous friction in the measurement of the resonance frequency in a piezometric crystal in a liquid |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010149811A1 (en) | 2009-06-23 | 2010-12-29 | Universidad Politécnica De Valencia | Method and device for nanogravimetry in fluid media using piezoelectric resonators |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2197796B1 (en) | 2005-02-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EC2A | Search report published |
Date of ref document: 20040101 Kind code of ref document: A1 |
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| FG2A | Definitive protection |
Ref document number: 2197796B1 Country of ref document: ES |
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| FD2A | Announcement of lapse in spain |
Effective date: 20220526 |