ES251332A1 - PROCEDIMEINTO PARA LA OBTENCIoN DE UN ALCALOIDE DE INSOQUINUCLIDINA A BASE DE ESPECIES DE CONOPHARYNGIA - Google Patents
PROCEDIMEINTO PARA LA OBTENCIoN DE UN ALCALOIDE DE INSOQUINUCLIDINA A BASE DE ESPECIES DE CONOPHARYNGIAInfo
- Publication number
- ES251332A1 ES251332A1 ES0251332A ES251332A ES251332A1 ES 251332 A1 ES251332 A1 ES 251332A1 ES 0251332 A ES0251332 A ES 0251332A ES 251332 A ES251332 A ES 251332A ES 251332 A1 ES251332 A1 ES 251332A1
- Authority
- ES
- Spain
- Prior art keywords
- solution
- filtration
- benzene
- residue
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KPUSZZFAYGWAHZ-UHFFFAOYSA-N 3-azabicyclo[2.2.2]octane Chemical class C1CC2CCC1NC2 KPUSZZFAYGWAHZ-UHFFFAOYSA-N 0.000 title abstract 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 12
- 239000000243 solution Substances 0.000 abstract 11
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 7
- 238000001914 filtration Methods 0.000 abstract 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 238000001704 evaporation Methods 0.000 abstract 3
- 238000000605 extraction Methods 0.000 abstract 3
- 239000002244 precipitate Substances 0.000 abstract 3
- UCIDWKVIQZIKEK-NXWOVTFFSA-N Tabernanthine Chemical compound N1([C@@H]2[C@H]3C[C@@H](C1)C[C@@H]2CC)CCC1=C3NC2=CC(OC)=CC=C12 UCIDWKVIQZIKEK-NXWOVTFFSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 239000012670 alkaline solution Substances 0.000 abstract 2
- 229930013930 alkaloid Natural products 0.000 abstract 2
- 150000003797 alkaloid derivatives Chemical class 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 2
- 238000010908 decantation Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- UCIDWKVIQZIKEK-UHFFFAOYSA-N tabernanthine Natural products CCC1CC(C2)CC3C1N2CCC1=C3NC2=CC(OC)=CC=C12 UCIDWKVIQZIKEK-UHFFFAOYSA-N 0.000 abstract 2
- 238000005406 washing Methods 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 1
- 239000003463 adsorbent Substances 0.000 abstract 1
- 150000001335 aliphatic alkanes Chemical class 0.000 abstract 1
- -1 aliphatic halogenated hydrocarbon Chemical class 0.000 abstract 1
- 229910001508 alkali metal halide Inorganic materials 0.000 abstract 1
- 150000008045 alkali metal halides Chemical class 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 239000003208 petroleum Substances 0.000 abstract 1
- 238000009738 saturating Methods 0.000 abstract 1
- 238000010792 warming Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D453/00—Heterocyclic compounds containing quinuclidine or iso-quinuclidine ring systems, e.g. quinine alkaloids
- C07D453/02—Heterocyclic compounds containing quinuclidine or iso-quinuclidine ring systems, e.g. quinine alkaloids containing not further condensed quinuclidine ring systems
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
- A61K31/439—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom the ring forming part of a bridged ring system, e.g. quinuclidine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
- Compounds Of Unknown Constitution (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH6270558A CH368186A (de) | 1958-08-08 | 1958-08-08 | Verfahren zur Gewinnung eines Isochinuclidin-Alkaloids aus Conopharyngia-Arten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES251332A1 true ES251332A1 (es) | 1960-03-01 |
Family
ID=4524469
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES0251332A Expired ES251332A1 (es) | 1958-08-08 | 1959-08-07 | PROCEDIMEINTO PARA LA OBTENCIoN DE UN ALCALOIDE DE INSOQUINUCLIDINA A BASE DE ESPECIES DE CONOPHARYNGIA |
Country Status (3)
| Country | Link |
|---|---|
| CH (1) | CH368186A (de) |
| ES (1) | ES251332A1 (de) |
| GB (1) | GB900395A (de) |
-
1958
- 1958-08-08 CH CH6270558A patent/CH368186A/de unknown
-
1959
- 1959-08-07 ES ES0251332A patent/ES251332A1/es not_active Expired
- 1959-08-07 GB GB27008/59A patent/GB900395A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CH368186A (de) | 1963-03-31 |
| GB900395A (en) | 1962-07-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US2874171A (en) | Recovery of ergosterol | |
| US3253023A (en) | Recovery of 3-(3, 4-dihydroxyphenyl)-l-alanine from velvet beans | |
| US2500173A (en) | Extraction of digitalis glycosides | |
| US2348215A (en) | Process for the manufacture of hesperidin | |
| GB900395A (en) | Process for obtaining an isoquinuclidine alkaloid from the plants of the genus conopharyngia | |
| JPS6159720B2 (de) | ||
| US2960500A (en) | Process for the extraction and purification of sapogenins | |
| Black et al. | Manufacture of algal chemicals. II. Laboratory‐scale isolation of mannitol from brown marine algae | |
| US5093243A (en) | Process for the separation and recovery of nosiheptide | |
| US3118909A (en) | Purification of gibberellins | |
| US3019220A (en) | Isolation of sapogenins | |
| US2863909A (en) | Process of extracting 1, 4-dicaffeyl-quinic acid | |
| Beall | A method for the isolation of pregnandiol from human pregnancy urine | |
| US3057878A (en) | Process for making crystalline potassium salt of gibberellic acid | |
| RU2111006C1 (ru) | Способ получения глицирама | |
| GB728961A (en) | Extraction of steroidal sapogenins from plant material | |
| GB1214093A (en) | Purification of deoxycholic acid | |
| US2876228A (en) | Recovery of rescinnamine | |
| GB702072A (en) | Improvements in or relating to the production of hecogenin from plant material | |
| US2720520A (en) | Recovery and/or purification of protoveratrine from veratrum album | |
| US2421142A (en) | Process for obtaining crystalline riboflavin | |
| US3846434A (en) | Process for obtaining a germine adduct from germine values | |
| US2720521A (en) | Recovery and/or purification of protoveratrine from veratrum album | |
| US3051712A (en) | Aj-ix-isodeserpbdic acid lactone | |
| US2521805A (en) | Process for extracting aconitine |