ES2551514T3 - Método para controlar la degradación de un ingrediente activo químico agrícola - Google Patents
Método para controlar la degradación de un ingrediente activo químico agrícola Download PDFInfo
- Publication number
- ES2551514T3 ES2551514T3 ES09788041.3T ES09788041T ES2551514T3 ES 2551514 T3 ES2551514 T3 ES 2551514T3 ES 09788041 T ES09788041 T ES 09788041T ES 2551514 T3 ES2551514 T3 ES 2551514T3
- Authority
- ES
- Spain
- Prior art keywords
- degradation
- active ingredient
- ciazofamide
- weight
- control
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 230000015556 catabolic process Effects 0.000 title abstract description 6
- 238000006731 degradation reaction Methods 0.000 title abstract description 6
- 239000004480 active ingredient Substances 0.000 title description 7
- 239000003905 agrochemical Substances 0.000 title description 3
- 238000000034 method Methods 0.000 title 1
- -1 polyoxyethylene Polymers 0.000 abstract description 20
- 229920003171 Poly (ethylene oxide) Polymers 0.000 abstract description 9
- 239000003381 stabilizer Substances 0.000 abstract description 3
- 150000005846 sugar alcohols Polymers 0.000 abstract description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 abstract 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 abstract 2
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 229910052915 alkaline earth metal silicate Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 239000010775 animal oil Substances 0.000 abstract 1
- 125000000129 anionic group Chemical group 0.000 abstract 1
- 150000004679 hydroxides Chemical class 0.000 abstract 1
- 150000004760 silicates Chemical class 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 235000015112 vegetable and seed oil Nutrition 0.000 abstract 1
- 239000008158 vegetable oil Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 239000004927 clay Substances 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 230000000855 fungicidal effect Effects 0.000 description 4
- 239000000417 fungicide Substances 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000004321 preservation Methods 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000003242 anti bacterial agent Substances 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- VNDFYDZORAPFSA-UHFFFAOYSA-N 2-(2-phenylethenoxy)ethenylbenzene Chemical compound C=1C=CC=CC=1C=COC=CC1=CC=CC=C1 VNDFYDZORAPFSA-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000002877 alkyl aryl group Chemical group 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Substances O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 229940049964 oleate Drugs 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 229920001515 polyalkylene glycol Polymers 0.000 description 1
- 229920000259 polyoxyethylene lauryl ether Polymers 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 239000004563 wettable powder Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/50—1,3-Diazoles; Hydrogenated 1,3-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
- A01N25/14—Powders or granules wettable
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/22—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients stabilising the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
El uso de al menos un estabilizante seleccionado entre un aceite animal epoxidado; un aceite vegetal epoxidado; un tensioactivo no iónico o aniónico de polioxietileno; un alcohol polihídrico; hidróxidos, carbonatos y bicarbonatos de metales alcalinos; hidróxidos, carbonatos y bicarbonatos de metales alcalino-térreos; soluciones acuosas de silicato; silicatos básicos; y silicatos básicos de metales alcalino-térreos, para controlar la degradación de la Ciazofamida.
Description
E09788041
29-10-2015
es al menos uno de una sal del éster del ácido sulfúrico de alquiléter de polioxietileno, sulfato de alquilaril éter de polioxietileno, sulfato de estiril éter de polioxietileno, sulfato de amonio de estiril éter de polioxietileno, fosfato de alquiléter de polioxietileno, una sal del éster del ácido fosfórico de alquilaril éter de polioxietileno, éster del ácido fosfórico de estirilaril éter de polioxietileno y una sal del éster del ácido fosfórico de estirilaril éter de polioxietileno.
5 (21). La composición descrita en el punto (15), en la que el alcohol polihídrico es al menos uno seleccionado del grupo constituido por un alquilenglicol, un alcohol trihídrico, un dialquilenglicol y un polialquilenglicol. (22). La composición descrita en cualquiera de los puntos (15)-(21), que comprende otro ingrediente activo químico agrícola, además de la Ciazofamida. (23). La composición descrita en el punto (22), en la que el otro ingrediente activo químico agrícola es un
10 compuesto de ingrediente activo de un fungicida. (24). La composición descrita en el punto (23), en la que el compuesto de ingrediente activo de un fungicida es un compuesto de benzanilida o un antibiótico. (25). La composición descrita en el punto (23), en la que el compuesto de ingrediente activo de un fungicida es un compuesto de benzanilida.
15 (26). La composición descrita en el punto (23), en la que el compuesto de ingrediente activo de un fungicida es un antibiótico.
Ejemplos
Después de pesar el 50,0 % en peso de arcilla MK (fabricada por Keiwa Rozai Co., Ltd.) y el 1,6 % en peso de Ciazofamida técnica finamente molida (pureza 94,4 %, diámetro medio de partícula 2,32 µm), se mezclan utilizando un Millser. Además, se le añadió el 47,4 % en peso de la arcilla MK mencionada anteriormente y el 1,0 % en peso de
25 un estabilizante y se volvió a mezclar usando el Millser, obteniendo de este modo un polvo pulverizable que contiene el 1,5 % en peso de Ciazofamida.
30 Después de pesar el 21,2 % en peso de Ciazofamida técnica finamente molida (pureza 94,4 %, diámetro medio de partícula 2,32 µm), el 8 % en peso de un agente dispersante; un condensado del ácido de alquilnaftalenosulfónico sódico-formaldehído (nombre comercial: SUPRAGIL MNS/90), el 2 % en peso de un agente humectante; dialquilnaftalensulfonato de sodio (nombre comercial: SUPRAGIL WP) y el 68,8 % en peso de carbonato de calcio LW-3000 (fabricado por Shimizu Industrial Corporation), se mezclan usando un Millser, obteniendo de este modo un
35 polvo humectable que contiene el 20 % en peso de Ciazofamida.
Después de pesar el 50,0 % en peso de arcilla MK (fabricada por Keiwa Rozai Co., Ltd.) y el 1,6 % en peso
40 Ciazofamida técnica finamente molida (pureza del 94,4 %, diámetro medio de partícula 2,32 µm), se mezclan usando un Millser. Además, se le añadió el 48,4 % en peso de la arcilla MK mencionada anteriormente y se volvió a mezclar usando un Millser, obteniendo de este modo un polvo pulverizable que contiene el 1,5 % en peso de Ciazofamida.
45 El polvo pulverizable obtenido mediante el Ejemplo 1 o Ejemplo Comparativo se sometió a conservación acelerada a 54 ºC durante 14 días, y a continuación se midió el contenido de Ciazofamida en el polvo pulverizable por HPLC (cromatografía líquida de alto rendimiento) y se calculó la relación de degradación ( %) de Ciazofamida mediante la siguiente fórmula: Relación de degradación ( %) = (contenido de la fase inicial -contenido después de la
50 conservación acelerada)/contenido de la fase inicial × 100. Los resultados del ensayo se muestran en la Tabla 1. A este respecto, se midió el contenido de Ciazofamida en el polvo pulverizable conservado a 4 ºC en el momento de medir el contenido de Ciazofamida en el polvo pulverizable después de la conservación acelerada, y el valor se usó como contenido de la fase inicial.
- Tabla 1 (Relación de degradación de la Ciazofamida)
- Estabilizante (1,0 % en peso)
- Relación de degradación (%)
- Ejemplo
- Aceite de soja epoxidado (nombre comercial: NK 800: fabricado por TAKEMOTO OIL & FAT Co., Ltd.) 5
- Lauril éter de polioxietileno (nombre comercial: Noigen ET-143: fabricado por Dai-ichi Kogyo Seiyaku Co., Ltd.)
- 6
- Éster de oleato de polioxietileno (nombre comercial: Noigen ES-149: fabricado por Dai-ichi Kogyo Seiyaku Co., Ltd.)
- 5
- Aceite de ricino de polioxietileno (nombre comercial: Sorpol CA20: fabricado por Toho Chemical Industry Co., Ltd.)
- 7
7
Claims (1)
-
imagen1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2008211054 | 2008-08-19 | ||
| JP2008211054 | 2008-08-19 | ||
| PCT/JP2009/064811 WO2010021404A2 (en) | 2008-08-19 | 2009-08-19 | Method for controlling degradation of agricultural chemical active ingredient |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2551514T3 true ES2551514T3 (es) | 2015-11-19 |
Family
ID=41707535
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES09788041.3T Active ES2551514T3 (es) | 2008-08-19 | 2009-08-19 | Método para controlar la degradación de un ingrediente activo químico agrícola |
Country Status (28)
| Country | Link |
|---|---|
| US (1) | US20110144175A1 (es) |
| EP (1) | EP2320733B1 (es) |
| JP (2) | JP5939557B2 (es) |
| KR (1) | KR101900952B1 (es) |
| CN (1) | CN102123589B (es) |
| AR (1) | AR075264A1 (es) |
| AU (1) | AU2009283423B2 (es) |
| BR (1) | BRPI0917309A2 (es) |
| CA (1) | CA2734374C (es) |
| CL (1) | CL2011000346A1 (es) |
| CY (1) | CY1117391T1 (es) |
| DK (1) | DK2320733T3 (es) |
| EC (1) | ECSP11010833A (es) |
| ES (1) | ES2551514T3 (es) |
| HR (1) | HRP20151373T1 (es) |
| HU (1) | HUE026010T2 (es) |
| MA (1) | MA32638B1 (es) |
| MX (1) | MX2011001818A (es) |
| PL (1) | PL2320733T3 (es) |
| PT (1) | PT2320733E (es) |
| RS (1) | RS54472B1 (es) |
| RU (1) | RU2514646C2 (es) |
| SI (1) | SI2320733T1 (es) |
| SM (1) | SMT201500311B (es) |
| TW (1) | TWI507131B (es) |
| UA (1) | UA104729C2 (es) |
| WO (1) | WO2010021404A2 (es) |
| ZA (1) | ZA201101344B (es) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5675646B2 (ja) * | 2009-12-09 | 2015-02-25 | Ｍｅｉｊｉ Ｓｅｉｋａファルマ株式会社 | 安定化された水性懸濁状農薬用組成物 |
| CN102858168B (zh) | 2010-04-27 | 2018-04-03 | 住友化学株式会社 | 农药组合物及其用途 |
| JP5782678B2 (ja) | 2010-04-27 | 2015-09-24 | 住友化学株式会社 | 有害生物防除組成物およびその用途 |
| KR101812362B1 (ko) | 2010-04-27 | 2017-12-26 | 스미또모 가가꾸 가부시키가이샤 | 유해 생물 방제 조성물 및 그의 용도 |
| PL2563131T3 (pl) | 2010-04-27 | 2017-09-29 | Sumitomo Chemical Company, Limited | Kompozycja szkodnikobójcza i jej zastosowanie |
| JP5712504B2 (ja) | 2010-04-27 | 2015-05-07 | 住友化学株式会社 | 有害生物防除組成物およびその用途 |
| JP5724210B2 (ja) | 2010-04-28 | 2015-05-27 | 住友化学株式会社 | 植物病害防除組成物およびその用途 |
| PL2563135T3 (pl) | 2010-04-28 | 2017-06-30 | Sumitomo Chemical Company, Limited | Kompozycja do kontrolowania chorób roślin i jej zastosowanie |
| NZ603846A (en) | 2010-04-28 | 2014-07-25 | Sumitomo Chemical Co | Plant disease control composition and its use |
| CN102858170B (zh) | 2010-04-28 | 2014-12-10 | 住友化学株式会社 | 杀虫组合物及其用途 |
| JP5789918B2 (ja) | 2010-04-28 | 2015-10-07 | 住友化学株式会社 | 植物病害防除組成物およびその用途 |
| JP5724211B2 (ja) | 2010-04-28 | 2015-05-27 | 住友化学株式会社 | 植物病害防除組成物およびその用途 |
| JP5724212B2 (ja) | 2010-04-28 | 2015-05-27 | 住友化学株式会社 | 植物病害防除組成物およびその用途 |
| CN102640754B (zh) * | 2012-04-01 | 2013-07-31 | 广东中迅农科股份有限公司 | 氰霜唑微胶囊悬浮剂及其制备方法 |
| CN105101799B (zh) * | 2013-04-16 | 2018-01-23 | Upl 有限公司 | 杀真菌组合物 |
| CN103563948B (zh) * | 2013-11-19 | 2015-07-22 | 西安北农华农作物保护有限公司 | 一种含氰霜唑的杀菌组合物 |
| WO2016068013A1 (ja) * | 2014-10-27 | 2016-05-06 | 石原産業株式会社 | 農薬製剤 |
| CN113040153B (zh) * | 2019-12-26 | 2022-03-22 | 江苏龙灯化学有限公司 | 一种稳定的四唑吡氨酯和氰霜唑液体悬浮组合物及其用途 |
| CN116250529B (zh) * | 2021-12-10 | 2025-09-16 | 山东潍坊润丰化工股份有限公司 | 一种含氟啶胺和氰霜唑的悬浮剂及其制备方法 |
| KR102555517B1 (ko) * | 2022-09-14 | 2023-07-13 | 안호영 | 사이퍼메스린계 이성질체를 유효성분으로 하는 산제화된 살충 조성물 및 그 제조 방법 |
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| WO2005014777A2 (en) * | 2002-10-16 | 2005-02-17 | Board Of Regents, The University Of Texas System | Methods and compositions for increasing the efficacy of biologically-active ingredients |
| KR20050047699A (ko) * | 2003-11-18 | 2005-05-23 | 주식회사 엘지생명과학 | 살균성 수성 액상수화제 |
| BRPI0513023A (pt) * | 2004-07-06 | 2008-04-22 | Basf Aktiengeeellschaft | composição pesticida, uso da mesma, e, métodos para combater os organismos que são prejudiciais às plantas, para proteger as safras do ataque ou infestação por organismos prejudiciais e para proteger as sementes do ataque ou infestação por organismos prejudiciais |
| WO2007050090A1 (en) * | 2005-10-28 | 2007-05-03 | Valent U.S.A. Corporation | Herbicidal compositions |
| JP5395483B2 (ja) * | 2008-03-31 | 2014-01-22 | 石原産業株式会社 | 農薬水性懸濁剤組成物 |
| CN101578987A (zh) * | 2009-06-26 | 2009-11-18 | 陕西标正作物科学有限公司 | 一种氰霜唑水乳剂及其制备方法 |
| CN101690484B (zh) * | 2009-08-24 | 2014-04-02 | 陕西标正作物科学有限公司 | 一种烯酰吗啉和氰霜唑复配的悬浮剂及其制备方法 |
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