ES260154A1 - Procedimiento de preparaciën de derivados 21-acetoxilados de 20-cetoesteroides - Google Patents
Procedimiento de preparaciën de derivados 21-acetoxilados de 20-cetoesteroidesInfo
- Publication number
- ES260154A1 ES260154A1 ES0260154A ES260154A ES260154A1 ES 260154 A1 ES260154 A1 ES 260154A1 ES 0260154 A ES0260154 A ES 0260154A ES 260154 A ES260154 A ES 260154A ES 260154 A1 ES260154 A1 ES 260154A1
- Authority
- ES
- Spain
- Prior art keywords
- diiodo
- dione
- dihydroxy
- keto
- reaction medium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001875 compounds Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- -1 steroid compounds Chemical class 0.000 title abstract 2
- JWMFYGXQPXQEEM-GCOKGBOCSA-N 5α-pregnane Chemical compound C([C@@H]1CC2)CCC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H](CC)[C@@]2(C)CC1 JWMFYGXQPXQEEM-GCOKGBOCSA-N 0.000 abstract 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 239000012429 reaction media Substances 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 239000012453 solvate Substances 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 150000003431 steroids Chemical class 0.000 abstract 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 abstract 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 239000011260 aqueous acid Substances 0.000 abstract 1
- 239000001110 calcium chloride Substances 0.000 abstract 1
- 229910001628 calcium chloride Inorganic materials 0.000 abstract 1
- 229940043430 calcium compound Drugs 0.000 abstract 1
- 150000001674 calcium compounds Chemical class 0.000 abstract 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000292 calcium oxide Substances 0.000 abstract 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 abstract 1
- 229910052740 iodine Inorganic materials 0.000 abstract 1
- 239000011630 iodine Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J5/00—Normal steroids containing carbon, hydrogen, halogen or oxygen, substituted in position 17 beta by a chain of two carbon atoms, e.g. pregnane and substituted in position 21 by only one singly bound oxygen atom, i.e. only one oxygen bound to position 21 by a single bond
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J75/00—Processes for the preparation of steroids in general
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Steroid Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR802089A FR1243528A (fr) | 1959-08-05 | 1959-08-05 | Procédé d'acétoxylation de stéroïdes en 21 par l'intermédiaire de dérivés diiodés |
| FR828677A FR78357E (fr) | 1960-05-31 | 1960-05-31 | Procédé d'acétoxylation de stéroïdes en 21 par l'intermédiaire de dérivés diiodés |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES260154A1 true ES260154A1 (es) | 1960-11-01 |
Family
ID=26184260
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES0260154A Expired ES260154A1 (es) | 1959-08-05 | 1960-08-04 | Procedimiento de preparaciën de derivados 21-acetoxilados de 20-cetoesteroides |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE593768A (fr) |
| CH (1) | CH398571A (fr) |
| ES (1) | ES260154A1 (fr) |
| GB (1) | GB934707A (fr) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4440689A (en) * | 1981-07-22 | 1984-04-03 | Mitsubishi Chemical Industries, Limited | Acyloxysteroids and process for producing same |
-
1960
- 1960-08-04 CH CH885960A patent/CH398571A/fr unknown
- 1960-08-04 GB GB271660D patent/GB934707A/en not_active Expired
- 1960-08-04 ES ES0260154A patent/ES260154A1/es not_active Expired
- 1960-08-04 BE BE593768A patent/BE593768A/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CH398571A (fr) | 1966-03-15 |
| GB934707A (en) | 1963-08-21 |
| BE593768A (fr) | 1961-02-06 |
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