ES2628461T3 - Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa - Google Patents

Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa Download PDF

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ES2628461T3
ES2628461T3 ES11867432.4T ES11867432T ES2628461T3 ES 2628461 T3 ES2628461 T3 ES 2628461T3 ES 11867432 T ES11867432 T ES 11867432T ES 2628461 T3 ES2628461 T3 ES 2628461T3
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biomass
vapors
gases
extraction
vertical reactor
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Martin Hitzl
Michael Renz
Avelino Corma Canos
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Ingelia SL
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Ingelia SL
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/002—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal in combination with oil conversion- or refining processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/008—Controlling or regulating of liquefaction processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/02—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by distillation
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/16—Hydrocarbons
    • C10L1/1616—Hydrocarbons fractions, e.g. lubricants, solvents, naphta, bitumen, tars, terpentine
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/54—Specific separation steps for separating fractions, components or impurities during preparation or upgrading of a fuel
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L9/00—Treating solid fuels to improve their combustion
    • C10L9/08—Treating solid fuels to improve their combustion by heat treatments, e.g. calcining
    • C10L9/086—Hydrothermal carbonization
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Processing Of Solid Wastes (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

La presente invención se refiere a un procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa que comprende alimentar una mezcla acuosa de biomasa desde un tubo de precalentamiento de la mezcla acuosa de biomasa a un reactor vertical con un nivel de flotación definido y una zona de acumulación de vapores y gases en su parte superior, donde dicho procedimiento de extracción de productos bioquímicos se caracteriza por que comprende: (a) calentar hasta o por encima de la temperatura de evaporación de la mezcla acuosa de biomasa en el mismo reactor vertical y/o en una etapa anterior de precalentamiento de la mezcla acuosa de biomasa, incrementando la generación de vapores y/o gases en el nivel de flotación definido del reactor vertical; (b) extraer los vapores y/o gases generados en la etapa anterior y acumulados en la parte superior del reactor vertical; y (c) enfriar los gases y/o condensar los vapores extraídos en la etapa anterior a diferentes niveles de temperatura y presión. Así mismo es objeto de la invención el producto bioquímico obtenible a partir de dicho procedimiento, así como el sistema para llevarlo a cabo.

Description

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Claims (1)

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ES11867432.4T 2011-06-09 2011-12-22 Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa Active ES2628461T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ES201130964A ES2393464B1 (es) 2011-06-09 2011-06-09 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa.
ES201130964P 2011-06-09
PCT/ES2011/070894 WO2012168502A1 (es) 2011-06-09 2011-12-22 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa

Publications (1)

Publication Number Publication Date
ES2628461T3 true ES2628461T3 (es) 2017-08-02

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Family Applications (2)

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ES201130964A Expired - Fee Related ES2393464B1 (es) 2011-06-09 2011-06-09 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa.
ES11867432.4T Active ES2628461T3 (es) 2011-06-09 2011-12-22 Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa

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ES201130964A Expired - Fee Related ES2393464B1 (es) 2011-06-09 2011-06-09 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa.

Country Status (9)

Country Link
US (1) US9556384B2 (es)
EP (1) EP2719748B1 (es)
BR (1) BR112013029833B1 (es)
CA (1) CA2835235C (es)
CO (1) CO6870026A2 (es)
ES (2) ES2393464B1 (es)
MX (1) MX340183B (es)
RU (1) RU2013151820A (es)
WO (1) WO2012168502A1 (es)

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FR3027894B1 (fr) 2014-11-04 2019-05-24 Degremont Procede de carbonisation hydrothermale d'une biomasse, et dispositif s'y rapportant
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EP3372657B1 (de) 2017-03-10 2019-09-25 HTCycle GmbH Vorrichtung zur durchführung einer hydrothermalen karbonisierungsreaktion
CA2972505A1 (en) 2017-07-05 2019-01-05 Decide Nv Process and system for treating municipal solid waste materials and producing multiple products
WO2019161272A1 (en) 2018-02-15 2019-08-22 North Carolina State University Synthesis of micron and nanoscale carbon spheres and structures using hydrothemal carbonization
CN109351297B (zh) * 2018-11-29 2023-10-17 清华大学 一种水热反应系统及其运行方法
DE102018220946A1 (de) 2018-12-04 2020-06-04 Suncoal Industries Gmbh Partikelförmige Kohlenstoffmaterialien und Verfahren zu deren Auftrennung
WO2020169809A2 (de) 2019-02-21 2020-08-27 Suncoal Industries Gmbh Verfahren zur geruchsreduktion partikelförmiger kohlenstoffmaterialien
CN109879325B (zh) * 2019-03-13 2020-04-17 重庆大学 一种从污泥基水热炭中回收磷及金属的方法
US12522627B2 (en) 2019-07-10 2026-01-13 Suncoal Industries Gmbh Method for producing stabilized lignin
GB2586145A (en) * 2019-08-07 2021-02-10 Ibj Tech Ivs Improvements in or relating to heat exchangers
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GB2592086B (en) 2020-06-17 2024-02-21 Coal Products Ltd Fibres
CN113604236B (zh) * 2021-08-13 2022-07-22 中国农业大学 一种生物质连续水热炭化系统
US12325651B2 (en) * 2023-01-23 2025-06-10 United Arab Emirates University Biodesalination using microbial attached growth cultivation

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Also Published As

Publication number Publication date
EP2719748A1 (en) 2014-04-16
ES2393464B1 (es) 2013-11-18
BR112013029833B1 (pt) 2019-10-08
US20140142353A1 (en) 2014-05-22
WO2012168502A1 (es) 2012-12-13
MX340183B (es) 2016-06-28
BR112013029833A2 (pt) 2016-12-06
ES2393464A1 (es) 2012-12-21
CA2835235A1 (en) 2012-12-13
EP2719748A4 (en) 2015-04-01
MX2013012763A (es) 2013-12-16
EP2719748B1 (en) 2017-05-10
US9556384B2 (en) 2017-01-31
RU2013151820A (ru) 2015-05-27
CA2835235C (en) 2018-01-23
CO6870026A2 (es) 2014-02-20

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