ES2628461T3 - Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa - Google Patents

Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa Download PDF

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Publication number
ES2628461T3
ES2628461T3 ES11867432.4T ES11867432T ES2628461T3 ES 2628461 T3 ES2628461 T3 ES 2628461T3 ES 11867432 T ES11867432 T ES 11867432T ES 2628461 T3 ES2628461 T3 ES 2628461T3
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biomass
vapors
gases
extraction
vertical reactor
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Martin Hitzl
Michael Renz
Avelino Corma Canos
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Ingelia SL
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Ingelia SL
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/002—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal in combination with oil conversion- or refining processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/008—Controlling or regulating of liquefaction processes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/02—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by distillation
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/16—Hydrocarbons
    • C10L1/1616—Hydrocarbons fractions, e.g. lubricants, solvents, naphta, bitumen, tars, terpentine
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L2290/00—Fuel preparation or upgrading, processes or apparatus therefore, comprising specific process steps or apparatus units
    • C10L2290/54—Specific separation steps for separating fractions, components or impurities during preparation or upgrading of a fuel
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L9/00—Treating solid fuels to improve their combustion
    • C10L9/08—Treating solid fuels to improve their combustion by heat treatments, e.g. calcining
    • C10L9/086—Hydrothermal carbonization
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Processing Of Solid Wastes (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

La presente invención se refiere a un procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa que comprende alimentar una mezcla acuosa de biomasa desde un tubo de precalentamiento de la mezcla acuosa de biomasa a un reactor vertical con un nivel de flotación definido y una zona de acumulación de vapores y gases en su parte superior, donde dicho procedimiento de extracción de productos bioquímicos se caracteriza por que comprende: (a) calentar hasta o por encima de la temperatura de evaporación de la mezcla acuosa de biomasa en el mismo reactor vertical y/o en una etapa anterior de precalentamiento de la mezcla acuosa de biomasa, incrementando la generación de vapores y/o gases en el nivel de flotación definido del reactor vertical; (b) extraer los vapores y/o gases generados en la etapa anterior y acumulados en la parte superior del reactor vertical; y (c) enfriar los gases y/o condensar los vapores extraídos en la etapa anterior a diferentes niveles de temperatura y presión. Así mismo es objeto de la invención el producto bioquímico obtenible a partir de dicho procedimiento, así como el sistema para llevarlo a cabo.

Description

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Claims (1)

  1. imagen1
ES11867432.4T 2011-06-09 2011-12-22 Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa Active ES2628461T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
ES201130964P 2011-06-09
ES201130964A ES2393464B1 (es) 2011-06-09 2011-06-09 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa.
PCT/ES2011/070894 WO2012168502A1 (es) 2011-06-09 2011-12-22 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa

Publications (1)

Publication Number Publication Date
ES2628461T3 true ES2628461T3 (es) 2017-08-02

Family

ID=47279177

Family Applications (2)

Application Number Title Priority Date Filing Date
ES201130964A Expired - Fee Related ES2393464B1 (es) 2011-06-09 2011-06-09 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa.
ES11867432.4T Active ES2628461T3 (es) 2011-06-09 2011-12-22 Método para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotérmica de biomasa

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ES201130964A Expired - Fee Related ES2393464B1 (es) 2011-06-09 2011-06-09 Procedimiento para la extracción de productos bioquímicos obtenidos a partir de un proceso de carbonización hidrotermal de biomasa.

Country Status (9)

Country Link
US (1) US9556384B2 (es)
EP (1) EP2719748B1 (es)
BR (1) BR112013029833B1 (es)
CA (1) CA2835235C (es)
CO (1) CO6870026A2 (es)
ES (2) ES2393464B1 (es)
MX (1) MX340183B (es)
RU (1) RU2013151820A (es)
WO (1) WO2012168502A1 (es)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3027894B1 (fr) * 2014-11-04 2019-05-24 Degremont Procede de carbonisation hydrothermale d'une biomasse, et dispositif s'y rapportant
DE102016201801A1 (de) 2015-11-21 2017-05-24 Suncoal Industries Gmbh Partikelförmiges Kohlenstoffmaterial herstellbar aus nachwachsenden Rohstoffen und Verfahren zu dessen Herstellung
DK3372657T3 (da) 2017-03-10 2020-01-27 Htcycle Gmbh Anordning til gennemførelse af en hydrotermisk karboniseringsreaktion
CA2972505A1 (en) 2017-07-05 2019-01-05 Decide Nv Process and system for treating municipal solid waste materials and producing multiple products
US11724941B2 (en) 2018-02-15 2023-08-15 North Carolina State University Synthesis of micron and nanoscale carbon spheres and structures using hydrothemal carbonization
CN109351297B (zh) * 2018-11-29 2023-10-17 清华大学 一种水热反应系统及其运行方法
DE102018220946A1 (de) 2018-12-04 2020-06-04 Suncoal Industries Gmbh Partikelförmige Kohlenstoffmaterialien und Verfahren zu deren Auftrennung
EP3927881A2 (de) 2019-02-21 2021-12-29 SunCoal Industries GmbH Verfahren zur geruchsreduktion partikelförmiger kohlenstoffmaterialien
CN109879325B (zh) * 2019-03-13 2020-04-17 重庆大学 一种从污泥基水热炭中回收磷及金属的方法
EP3997157A1 (de) 2019-07-10 2022-05-18 SunCoal Industries GmbH Verfahren zur herstellung eines stabilisierten lignins mit hoher spezifischer oberfläche
GB2586145A (en) * 2019-08-07 2021-02-10 Ibj Tech Ivs Improvements in or relating to heat exchangers
US12162786B2 (en) * 2019-12-02 2024-12-10 Robert C. Casad, Jr. Methods for valorization of lignin-rich solids from anaerobic digestate
GB2592086B (en) 2020-06-17 2024-02-21 Coal Products Ltd Fibres
CN113604236B (zh) * 2021-08-13 2022-07-22 中国农业大学 一种生物质连续水热炭化系统
US12325651B2 (en) * 2023-01-23 2025-06-10 United Arab Emirates University Biodesalination using microbial attached growth cultivation

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH373118A (de) 1956-12-18 1963-11-15 Ciba Geigy Verfahren zur Herstellung neuer wasserlöslicher Farbstoffe
CA2232015A1 (en) * 1999-10-21 1999-10-22 Hebco International Inc. Process for the selective and safe recovery of residual gases from a pyrolysis reaction of solid carbonizable material
WO2006117002A2 (en) * 2005-04-29 2006-11-09 Scf Technologies A/S Method and apparatus for converting organic material
CA2595484A1 (en) 2006-08-07 2008-02-07 John Allan Fallavollita Process for recovery of holocellulose and near-native lignin from biomass
DE102007056170A1 (de) 2006-12-28 2008-11-06 Dominik Peus Semikontinuierliches Verfahren zur Herstellung von Brennstoff aus Biomasse
ES2710176T3 (es) * 2007-02-08 2019-04-23 Grenol Ip Gmbh Carbonización hidrotermal de biomasa
DE102008004732A1 (de) * 2008-01-16 2009-07-23 Lucia Viviane Sanders Hydrothermale Karbonisierung von Biomasse
BRPI0803545A2 (pt) * 2008-07-31 2010-06-15 Petroleo Brasileiro Sa processo de produção de bio-óleo por co-processamento de biomassa em unidade de coqueamento retardado
ES2339321B1 (es) * 2008-11-17 2011-03-31 Ingelia, S.L. Sistema de control de la presion y temperatura de un reactor o conjunto de reactores quimicos.
MX2011003823A (es) * 2008-11-17 2011-07-28 Ingelia S L Sistema de control de presion y temperatura de al menos un reactor quimico.
ES2339320B1 (es) * 2008-11-17 2011-03-28 Ingelia, S.L. Metodo de carbonizacion hidrotermal con reactor de flujo invertido,eninstalacion.
DE102009008563A1 (de) * 2009-02-12 2010-08-19 Sgs Sanders Geoscience Se Biotechnologisches Verfahren zur Herstellung von Energieträgern
JP2012525507A (ja) 2009-04-30 2012-10-22 イヴ リサーチ インコーポレイテッド コート紙製品をリサイクルするためのプロセスおよび装置
WO2010124381A1 (en) 2009-04-30 2010-11-04 Evegenetics Canada Inc. Preparation of biofuels and other useful products such as 5-(hydroxymethyl)-furfural

Also Published As

Publication number Publication date
MX2013012763A (es) 2013-12-16
BR112013029833B1 (pt) 2019-10-08
BR112013029833A2 (pt) 2016-12-06
US9556384B2 (en) 2017-01-31
US20140142353A1 (en) 2014-05-22
CO6870026A2 (es) 2014-02-20
ES2393464A1 (es) 2012-12-21
CA2835235C (en) 2018-01-23
EP2719748B1 (en) 2017-05-10
EP2719748A1 (en) 2014-04-16
ES2393464B1 (es) 2013-11-18
RU2013151820A (ru) 2015-05-27
CA2835235A1 (en) 2012-12-13
WO2012168502A1 (es) 2012-12-13
MX340183B (es) 2016-06-28
EP2719748A4 (en) 2015-04-01

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