ES2753402T3 - Proceso continuo para el fraccionamiento seco de aceites de glicérido - Google Patents
Proceso continuo para el fraccionamiento seco de aceites de glicérido Download PDFInfo
- Publication number
- ES2753402T3 ES2753402T3 ES15766668T ES15766668T ES2753402T3 ES 2753402 T3 ES2753402 T3 ES 2753402T3 ES 15766668 T ES15766668 T ES 15766668T ES 15766668 T ES15766668 T ES 15766668T ES 2753402 T3 ES2753402 T3 ES 2753402T3
- Authority
- ES
- Spain
- Prior art keywords
- glyceride oil
- temperature
- oil
- glyceride
- nucleated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000003921 oil Substances 0.000 title claims abstract description 259
- 125000005456 glyceride group Chemical group 0.000 title claims abstract description 203
- 238000005194 fractionation Methods 0.000 title claims abstract description 38
- 238000010924 continuous production Methods 0.000 title description 8
- 235000019198 oils Nutrition 0.000 claims abstract description 256
- 238000000034 method Methods 0.000 claims abstract description 93
- 230000008569 process Effects 0.000 claims abstract description 82
- 238000002425 crystallisation Methods 0.000 claims abstract description 57
- 230000008025 crystallization Effects 0.000 claims abstract description 57
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 claims abstract description 50
- 239000013078 crystal Substances 0.000 claims abstract description 46
- 238000001816 cooling Methods 0.000 claims abstract description 44
- 239000007788 liquid Substances 0.000 claims abstract description 36
- 235000019482 Palm oil Nutrition 0.000 claims abstract description 32
- 239000002540 palm oil Substances 0.000 claims abstract description 32
- 238000010899 nucleation Methods 0.000 claims abstract description 15
- 230000006911 nucleation Effects 0.000 claims abstract description 15
- 238000007711 solidification Methods 0.000 claims abstract description 6
- 230000008023 solidification Effects 0.000 claims abstract description 6
- 230000008018 melting Effects 0.000 claims description 23
- 238000002844 melting Methods 0.000 claims description 23
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 17
- 229910052740 iodine Inorganic materials 0.000 claims description 17
- 239000011630 iodine Substances 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 9
- 230000009467 reduction Effects 0.000 claims description 4
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 52
- 239000003925 fat Substances 0.000 description 36
- 235000019197 fats Nutrition 0.000 description 36
- 239000007787 solid Substances 0.000 description 16
- 238000001914 filtration Methods 0.000 description 14
- 238000000265 homogenisation Methods 0.000 description 14
- 230000002829 reductive effect Effects 0.000 description 11
- 239000002002 slurry Substances 0.000 description 9
- 238000012546 transfer Methods 0.000 description 9
- 150000003626 triacylglycerols Chemical class 0.000 description 8
- 238000012545 processing Methods 0.000 description 7
- 238000013019 agitation Methods 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 239000012528 membrane Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 238000000926 separation method Methods 0.000 description 6
- 239000002826 coolant Substances 0.000 description 5
- 238000010586 diagram Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000000155 melt Substances 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000010923 batch production Methods 0.000 description 3
- 239000013256 coordination polymer Substances 0.000 description 3
- 239000003599 detergent Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 230000012010 growth Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 235000021003 saturated fats Nutrition 0.000 description 3
- 238000010583 slow cooling Methods 0.000 description 3
- 235000019871 vegetable fat Nutrition 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 239000008157 edible vegetable oil Substances 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 235000021588 free fatty acids Nutrition 0.000 description 2
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005374 membrane filtration Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000014593 oils and fats Nutrition 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000009482 thermal adhesion granulation Methods 0.000 description 2
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 2
- 235000015112 vegetable and seed oil Nutrition 0.000 description 2
- 235000019737 Animal fat Nutrition 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 230000003698 anagen phase Effects 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000007385 chemical modification Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- NNYBQONXHNTVIJ-UHFFFAOYSA-N etodolac Chemical compound C1COC(CC)(CC(O)=O)C2=C1C(C=CC=C1CC)=C1N2 NNYBQONXHNTVIJ-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001640 fractional crystallisation Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 150000002314 glycerols Chemical class 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000011440 grout Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229940063718 lodine Drugs 0.000 description 1
- 235000013310 margarine Nutrition 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 235000021243 milk fat Nutrition 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000001225 nuclear magnetic resonance method Methods 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000013379 physicochemical characterization Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000010900 secondary nucleation Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000000153 supplemental effect Effects 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0075—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of melting or solidifying points
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MYPI2014703630A MY184018A (en) | 2014-12-03 | 2014-12-03 | Continuous process for dry fractionation of glyceride oils |
| PCT/MY2015/000059 WO2016089196A1 (en) | 2014-12-03 | 2015-07-16 | Continuous process for dry fractionation of glyceride oils |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2753402T3 true ES2753402T3 (es) | 2020-04-08 |
Family
ID=54148603
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES15766668T Active ES2753402T3 (es) | 2014-12-03 | 2015-07-16 | Proceso continuo para el fraccionamiento seco de aceites de glicérido |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP3227418B1 (pl) |
| DK (1) | DK3227418T3 (pl) |
| ES (1) | ES2753402T3 (pl) |
| MY (1) | MY184018A (pl) |
| PL (1) | PL3227418T3 (pl) |
| PT (1) | PT3227418T (pl) |
| WO (1) | WO2016089196A1 (pl) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108837551B (zh) * | 2018-07-28 | 2024-04-02 | 湖南懋天世纪新材料有限公司 | 一种超细仲钨酸铵蒸发结晶装置及结晶方法 |
| CN110257169A (zh) * | 2019-06-12 | 2019-09-20 | 深圳精益油脂技术有限公司 | 一种制备低缩水甘油酯及低3-mcpd酯含量的棕榈油的方法 |
| MY203841A (en) * | 2020-03-10 | 2024-07-20 | Liew Heng Wen | Dry fractionation of edible oil |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1120456A (en) * | 1964-12-14 | 1968-07-17 | Ranchers Cotton Oil | Method of separating components of oleaginous mixtures by fractional crystallization |
| DE2901328C2 (de) * | 1979-01-15 | 1985-07-25 | Walter Rau Lebensmittelwerke GmbH & Co. KG, 4517 Hilter | Verfahren zum selektiven Gewinnen von Triglyceriden oder Gemischen von Triglyceriden höherer Fettsäuren in kristalliner Form aus Naturfetten |
| CA1301775C (en) * | 1986-06-04 | 1992-05-26 | Karel Petrus Agnes Maria Van Putte | Fractionation of fat blends |
| DE4132892A1 (de) * | 1991-10-04 | 1993-04-22 | Krupp Maschinentechnik | Stoffgemischfraktionierung |
| WO1998051753A1 (en) * | 1997-05-12 | 1998-11-19 | Wisconsin Alumni Research Foundation | Continuous crystallization system with controlled nucleation for milk fat fractionation |
| DE60140185D1 (de) * | 2001-07-31 | 2009-11-26 | Smet Engineering N V De | Verfahren und Vorrichtung zur Trockenfraktionierung |
| EP1818088A1 (en) * | 2006-01-20 | 2007-08-15 | De Smet Engineering N.V. | Crystallisers useful in fractionation processes for oils and fats |
| GB2496606B (en) * | 2011-11-15 | 2014-01-22 | Desmet Ballestra Engineering S A Nv | Continuous fractionation of triglyceride oils |
-
2014
- 2014-12-03 MY MYPI2014703630A patent/MY184018A/en unknown
-
2015
- 2015-07-16 PT PT157666686T patent/PT3227418T/pt unknown
- 2015-07-16 DK DK15766668T patent/DK3227418T3/da active
- 2015-07-16 PL PL15766668T patent/PL3227418T3/pl unknown
- 2015-07-16 ES ES15766668T patent/ES2753402T3/es active Active
- 2015-07-16 WO PCT/MY2015/000059 patent/WO2016089196A1/en not_active Ceased
- 2015-07-16 EP EP15766668.6A patent/EP3227418B1/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| MY184018A (en) | 2021-03-17 |
| PL3227418T3 (pl) | 2020-06-15 |
| DK3227418T3 (da) | 2019-11-11 |
| WO2016089196A1 (en) | 2016-06-09 |
| PT3227418T (pt) | 2019-11-05 |
| EP3227418A1 (en) | 2017-10-11 |
| EP3227418B1 (en) | 2019-09-04 |
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