ES426730A1 - PROCEDURE FOR THE PRODUCTION OF A MULTIPLICITY OF COMPOSITIONS OF ISOCIANATE. - Google Patents

PROCEDURE FOR THE PRODUCTION OF A MULTIPLICITY OF COMPOSITIONS OF ISOCIANATE.

Info

Publication number
ES426730A1
ES426730A1 ES426730A ES426730A ES426730A1 ES 426730 A1 ES426730 A1 ES 426730A1 ES 426730 A ES426730 A ES 426730A ES 426730 A ES426730 A ES 426730A ES 426730 A1 ES426730 A1 ES 426730A1
Authority
ES
Spain
Prior art keywords
product
mixture
multiplicity
production
methylene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES426730A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Publication of ES426730A1 publication Critical patent/ES426730A1/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyurethanes Or Polyureas (AREA)

Abstract

Process for the production of a multiplicity of isocyanate compositions, from a mixture of methylene-bridged polyphenylpolyisocyanates polyisocyanates containing 40 to 85% of diphenylmethanediisocyanates and produced by phosgenation of a mixture of polyamines, obtained by condensation of aniline and formaldehyde, characterized in that it comprises (a) distilling said polyisocyanate mixture and separating 5 to 70% of the diisocyanate with respect to it, as overhead volatile products (product II), leaving a residue of methylene-bridged polyphenylpolysisocyanates (product I) and (b) subjecting product II to a crystallization process so that a crystallized 4,4'-diphenylmethanediisocyanate (product III) and a mother liquor (product IV) comprising 10 to 55% of 2,4'are obtained. -diphenylmethane diisocyanate and 90 to 45% of 4,4'-diphenylmethane diisocyanate. (Machine-translation by Google Translate, not legally binding)
ES426730A 1973-05-29 1974-05-29 PROCEDURE FOR THE PRODUCTION OF A MULTIPLICITY OF COMPOSITIONS OF ISOCIANATE. Expired ES426730A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2537073A GB1417087A (en) 1973-05-29 1973-05-29 Polyisocyanates

Publications (1)

Publication Number Publication Date
ES426730A1 true ES426730A1 (en) 1976-07-01

Family

ID=10226582

Family Applications (1)

Application Number Title Priority Date Filing Date
ES426730A Expired ES426730A1 (en) 1973-05-29 1974-05-29 PROCEDURE FOR THE PRODUCTION OF A MULTIPLICITY OF COMPOSITIONS OF ISOCIANATE.

Country Status (10)

Country Link
JP (1) JPS5826337B2 (en)
AR (1) AR202214A1 (en)
BE (1) BE815525A (en)
BR (1) BR7404304D0 (en)
DE (1) DE2425658A1 (en)
ES (1) ES426730A1 (en)
FR (1) FR2231709B1 (en)
GB (1) GB1417087A (en)
IT (1) IT1012607B (en)
NL (1) NL7406894A (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1483957A (en) * 1975-05-19 1977-08-24 Ici Ltd Diphenylmethane diisocyanate compositions
US4055548A (en) * 1976-09-17 1977-10-25 The Upjohn Company Storage-stable liquid polyisocyanate composition
DE2815554A1 (en) 1978-04-11 1979-10-25 Basf Ag FLAME RESISTANT SOFT POLYURETHANE FOAM
US4237240A (en) 1979-04-09 1980-12-02 Basf Aktiengesellschaft Process for the manufacture of flexible polyurethane foams with high load-bearing and high energy-absorption capacity
US4287132A (en) 1980-09-29 1981-09-01 Atlantic Richfield Company Preparation of polyisocyanates from polycarbamates
JP2660588B2 (en) * 1989-11-30 1997-10-08 日本ポリウレタン工業株式会社 Method for producing flexible polyurethane foam
JP2875877B2 (en) * 1990-10-23 1999-03-31 三井化学株式会社 Method for producing methylene-crosslinked polyphenylene polyisocyanate
DE4200236A1 (en) * 1992-01-08 1993-07-15 Bayer Ag METHOD FOR ISOLATING POLYISOCYANATE ISOMERS FROM POLYISOCYANATE MIXTURES
EP1475367B1 (en) * 2003-05-08 2010-07-07 Bayer MaterialScience AG Distillation process for separating diisocyanatodiphenylmethane isomers
EP1518874B1 (en) * 2003-09-24 2006-12-13 Basf Aktiengesellschaft Polymeric MDI having low monomer content
WO2010040675A2 (en) * 2008-10-06 2010-04-15 Huntsman International Llc Process for the simultaneous production of different mixtures of diisocyanate isomers of the diphenylmethane series
EP3498689A1 (en) 2017-12-14 2019-06-19 Sulzer Chemtech AG A plant and method for purifying an isomeric monomer, such as 4,4'-methylene diphenyl diisocyanate, from a crude mixture

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2105193C3 (en) * 1971-02-04 1981-07-09 Chemie-Anlagenbau Bischofsheim GmbH, 4500 Osnabrück Process for the separation of an organic polyisocyanate mixture

Also Published As

Publication number Publication date
BE815525A (en) 1974-11-25
AR202214A1 (en) 1975-05-23
DE2425658A1 (en) 1974-12-19
JPS5826337B2 (en) 1983-06-02
BR7404304D0 (en) 1975-09-30
FR2231709B1 (en) 1978-01-20
NL7406894A (en) 1974-12-03
GB1417087A (en) 1975-12-10
FR2231709A1 (en) 1974-12-27
JPS5035142A (en) 1975-04-03
IT1012607B (en) 1977-03-10

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