ES448305A1 - Procedimiento para la obtencion de un material de separacionpara la cromatografia de capa delgada. - Google Patents
Procedimiento para la obtencion de un material de separacionpara la cromatografia de capa delgada.Info
- Publication number
- ES448305A1 ES448305A1 ES448305A ES448305A ES448305A1 ES 448305 A1 ES448305 A1 ES 448305A1 ES 448305 A ES448305 A ES 448305A ES 448305 A ES448305 A ES 448305A ES 448305 A1 ES448305 A1 ES 448305A1
- Authority
- ES
- Spain
- Prior art keywords
- thin layer
- layer chromatography
- separating material
- thick
- diameter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000463 material Substances 0.000 title abstract 2
- 238000004809 thin layer chromatography Methods 0.000 title abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000000741 silica gel Substances 0.000 abstract 1
- 229910002027 silica gel Inorganic materials 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
- G01N30/92—Construction of the plate
- G01N30/93—Application of the sorbent layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/50—Conditioning of the sorbent material or stationary liquid
- G01N30/52—Physical parameters
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
Procedimiento para la obtención de un material de separación para la cromatografía en capa delgada, por recubrimiento de un material soporte con gel de sílice que puede contener un medio aglutinante y/o indicadores, caracterizado porque se prepara a temperatura sensiblemente ambiente una suspensión de agua y gel de sílice, que está compuesto por partículas con un estrecho margen de tamaño de partículas con un estrecho margen de tamaño de partícula comprendido entre 3 y 8 mym, porque se homogeneiza completamente esta suspensión, se libera de burbujas de aire, se extiende en capas de espesor homogéneo sobre el material soporte de modo que después del secado se obtenga un espesor de capa comprendido entre 100 y 300 mym.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2524065A DE2524065C2 (de) | 1975-05-30 | 1975-05-30 | Trennmaterial für die Dünnschichtchromatographie |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES448305A1 true ES448305A1 (es) | 1978-11-01 |
Family
ID=5947841
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES448305A Expired ES448305A1 (es) | 1975-05-30 | 1976-05-28 | Procedimiento para la obtencion de un material de separacionpara la cromatografia de capa delgada. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4064041A (es) |
| JP (1) | JPS5947260B2 (es) |
| BE (1) | BE842303A (es) |
| CA (1) | CA1065832A (es) |
| CH (1) | CH619868A5 (es) |
| CS (1) | CS189770B2 (es) |
| DE (1) | DE2524065C2 (es) |
| ES (1) | ES448305A1 (es) |
| FR (1) | FR2312778A1 (es) |
| GB (1) | GB1533724A (es) |
| IT (1) | IT1061325B (es) |
| NL (1) | NL7605767A (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2826664C2 (de) | 1978-06-19 | 1987-01-15 | Merck Patent Gmbh, 6100 Darmstadt | Verfahren zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen |
| DE2856056C2 (de) * | 1978-12-23 | 1986-10-16 | Merck Patent Gmbh, 6100 Darmstadt | Verfahren zur Herstellung von wasserfesten Chromatographie-Fertigpräparationen |
| US4292041A (en) * | 1979-11-02 | 1981-09-29 | Merck & Co., Inc. | Surfactant assay |
| HU189133B (en) * | 1982-04-28 | 1986-06-30 | Labor Mueszeripari Muevek,Hu | Special layer plate and/or layer plate system for overpressure multi-layer chromatography |
| DE3427923A1 (de) * | 1984-07-28 | 1986-01-30 | Merck Patent Gmbh, 6100 Darmstadt | Trennmaterial fuer die duennschichtchromatographie |
| LU90565B1 (en) * | 2000-04-14 | 2001-10-15 | Europ Economic Community | Device for the detection of aflatoxins |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL288991A (es) * | 1962-06-09 | |||
| DE1442446C3 (de) * | 1965-06-18 | 1974-03-14 | Merck Patent Gmbh, 6100 Darmstadt | Sorptionsmittel für die Schichtchromatographie: |
| FR1498667A (fr) * | 1966-09-15 | 1967-10-20 | Procédé chromatographique | |
| US3647684A (en) * | 1968-04-17 | 1972-03-07 | Dexter Corp | Adding cationic material to silicic acid sorbent chromatographic sheet for improved performance |
| DE1792083A1 (de) * | 1968-07-19 | 1971-04-29 | Merck Anlagen Gmbh | Zweischichtenplatte und ihre Verwendung zur duennschichtchromatographischen Auftrennung von Aminosaeuren |
| US3922431A (en) * | 1969-02-20 | 1975-11-25 | Edmund Radmacher | Elements for thin-layer chromatography |
| US3782075A (en) * | 1972-04-07 | 1974-01-01 | Du Pont | Completely porous microspheres for chromatographic uses |
| CH565651A5 (es) * | 1973-06-14 | 1975-08-29 | Ciba Geigy Ag |
-
1975
- 1975-05-30 DE DE2524065A patent/DE2524065C2/de not_active Expired
-
1976
- 1976-05-25 FR FR7615775A patent/FR2312778A1/fr active Granted
- 1976-05-27 US US05/690,728 patent/US4064041A/en not_active Expired - Lifetime
- 1976-05-27 GB GB22048/76A patent/GB1533724A/en not_active Expired
- 1976-05-28 BE BE167397A patent/BE842303A/xx not_active IP Right Cessation
- 1976-05-28 CS CS763579A patent/CS189770B2/cs unknown
- 1976-05-28 NL NL7605767A patent/NL7605767A/xx not_active Application Discontinuation
- 1976-05-28 CH CH671976A patent/CH619868A5/de not_active IP Right Cessation
- 1976-05-28 ES ES448305A patent/ES448305A1/es not_active Expired
- 1976-05-28 IT IT49706/76A patent/IT1061325B/it active
- 1976-05-29 JP JP51062850A patent/JPS5947260B2/ja not_active Expired
- 1976-05-31 CA CA253,708A patent/CA1065832A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR2312778B1 (es) | 1980-05-16 |
| JPS5947260B2 (ja) | 1984-11-17 |
| DE2524065C2 (de) | 1988-03-03 |
| JPS524291A (en) | 1977-01-13 |
| US4064041A (en) | 1977-12-20 |
| FR2312778A1 (fr) | 1976-12-24 |
| CH619868A5 (es) | 1980-10-31 |
| CA1065832A (en) | 1979-11-06 |
| DE2524065A1 (de) | 1976-12-09 |
| CS189770B2 (en) | 1979-04-30 |
| BE842303A (nl) | 1976-11-29 |
| IT1061325B (it) | 1983-02-28 |
| GB1533724A (en) | 1978-11-29 |
| NL7605767A (nl) | 1976-12-02 |
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