ES463603A1 - Procedimiento para la purificacion de acido fosforico de procedimiento en humedo. - Google Patents
Procedimiento para la purificacion de acido fosforico de procedimiento en humedo.Info
- Publication number
- ES463603A1 ES463603A1 ES463603A ES463603A ES463603A1 ES 463603 A1 ES463603 A1 ES 463603A1 ES 463603 A ES463603 A ES 463603A ES 463603 A ES463603 A ES 463603A ES 463603 A1 ES463603 A1 ES 463603A1
- Authority
- ES
- Spain
- Prior art keywords
- phosphoric acid
- water
- solvent
- organic
- decontaminated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title abstract 18
- 229910000147 aluminium phosphate Inorganic materials 0.000 title abstract 9
- 238000005202 decontamination Methods 0.000 title 1
- 230000003588 decontaminative effect Effects 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 5
- 239000002904 solvent Substances 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- 229910000318 alkali metal phosphate Inorganic materials 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000000356 contaminant Substances 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 150000003016 phosphoric acids Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/234—Purification; Stabilisation; Concentration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procedimiento para la purificación de ácido fosfórico de procedimiento en húmedo, en que el ácido fosfórico a purificar y un disolvente orgánico, que es parcialmente miscible con agua y es capaz de recoger el ácido fosfórico, son conducidos en contracorriente entre si, la solución orgánica de ácido fosfórico, resultante en tal caso, es separada de las impurezas no recogidas por el disolvente, el producto refinado primario es tratado en contracorriente con un disolvente que contiene ácido mineral, caracterizado porque se mezcla con un disolvente anhidro al extracto orgánico de ácido fosfórico formado en el tratamiento del producto refinado, con un contenido de agua mayor de 0 e igual o menor de 10% en paso, en una proporción ponderal tal que la mezcla obtenida tiene un contenido de agua que es mayor que 0 y menor de 50% de la concentración de saturación con agua en el disolvente, y porque esta mezcla se conduce en contracorriente con respecto al ácido fosforito a purificar.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2657190A DE2657190C2 (de) | 1976-12-17 | 1976-12-17 | Verfahren zur Reinigung von Naßverfahrensphosphorsäure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES463603A1 true ES463603A1 (es) | 1978-07-16 |
Family
ID=5995770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES463603A Expired ES463603A1 (es) | 1976-12-17 | 1977-10-27 | Procedimiento para la purificacion de acido fosforico de procedimiento en humedo. |
Country Status (23)
| Country | Link |
|---|---|
| US (1) | US4200620A (es) |
| JP (1) | JPS5383993A (es) |
| AT (1) | AT354978B (es) |
| BE (1) | BE861920A (es) |
| BR (1) | BR7708375A (es) |
| CA (1) | CA1084238A (es) |
| CH (1) | CH631418A5 (es) |
| DD (1) | DD136258A5 (es) |
| DE (1) | DE2657190C2 (es) |
| DK (1) | DK149229C (es) |
| ES (1) | ES463603A1 (es) |
| FI (1) | FI65610C (es) |
| FR (1) | FR2374263A1 (es) |
| GB (1) | GB1554379A (es) |
| IL (1) | IL53618A0 (es) |
| IT (1) | IT1090568B (es) |
| MX (1) | MX146999A (es) |
| NL (1) | NL184945C (es) |
| PH (1) | PH14335A (es) |
| SE (1) | SE429752B (es) |
| SU (1) | SU888812A3 (es) |
| TR (1) | TR19331A (es) |
| ZA (1) | ZA777470B (es) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4197280A (en) * | 1978-10-02 | 1980-04-08 | Stauffer Chemical Company | Wet process phosphoric acid purification |
| DE2909572A1 (de) | 1979-03-12 | 1980-09-25 | Hoechst Ag | Verfahren zur ueberfuehrung von extraktionsrueckstaenden aus der phosphorsaeurereinigung in feste deponieprodukte |
| DE2926943A1 (de) * | 1979-07-04 | 1981-01-29 | Hoechst Ag | Verfahren zur reinigung von nassverfahrensphosphorsaeure |
| US4751066A (en) * | 1986-05-08 | 1988-06-14 | Fmc Corporation | Process for preparing alkali metal phosphate |
| GB9124353D0 (en) * | 1991-11-15 | 1992-01-08 | Albright & Wilson | Immobilisation of metal contaminants from a liquid to a solid metal |
| IL211043A0 (en) * | 2010-02-06 | 2011-04-28 | Aharon Eyal | A method for the separation of a non-volatile strong acid from a salt thereof and compositions produced thereby |
| MX2015009680A (es) * | 2013-01-28 | 2016-04-25 | Solex Water Ltd | Metodos y sistemas para recuperacion de agua. |
| CN114031057B (zh) * | 2021-12-17 | 2022-06-21 | 四川大学 | 湿法磷酸生产工业磷酸及联产聚磷酸铵或固体磷酸的方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE884358C (de) * | 1951-09-20 | 1953-07-27 | Gerardo Collardin | Verfahren zur Reinigung von technischer Phosphorsaeure |
| BE757550A (fr) * | 1969-10-16 | 1971-03-16 | Giulini Gmbh Geb | Procede de preparation de phosphates purs a partir d'acides phosphoriques impurs |
| SE366972B (es) * | 1970-06-12 | 1974-05-13 | Azote & Prod Chim | |
| FR2093372A5 (en) * | 1970-06-12 | 1972-01-28 | Azote & Prod Chim | Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent |
| FR2128968A6 (en) * | 1971-03-10 | 1972-10-27 | Azote & Prod Chim | Purification of wet-process phosphoric acid - by extraction - with part water-misc organic solvent |
| US3956465A (en) * | 1970-06-12 | 1976-05-11 | Azote Et Produits Chimiques S.A. | Solvent purification of wet process phosphoric acid |
| DE2029564C3 (de) * | 1970-06-16 | 1978-06-22 | Giulini Chemie Gmbh, 6700 Ludwigshafen | Verfahren zur Herstellung von reinen Alkaliphosphaten aus Rohphosphorsäure |
| US3684439A (en) * | 1970-09-22 | 1972-08-15 | Monsanto Co | Handling of raffinates from wet phosphoric acid purification |
| DE2321751C3 (de) * | 1973-04-30 | 1981-11-19 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Reinigung von Naßphosphorsäure |
| DE2605106C2 (de) * | 1976-02-10 | 1984-06-14 | Hoechst Ag, 6230 Frankfurt | Verfahren und Vorrichtung zur Herstellung von alkoholischen Phosphorsäurelösungen aus sauren Phosphaten |
-
1976
- 1976-12-17 DE DE2657190A patent/DE2657190C2/de not_active Expired
-
1977
- 1977-09-13 CH CH1116477A patent/CH631418A5/de not_active IP Right Cessation
- 1977-10-27 ES ES463603A patent/ES463603A1/es not_active Expired
- 1977-11-30 SU SU772547802A patent/SU888812A3/ru active
- 1977-12-08 NL NLAANVRAGE7713608,A patent/NL184945C/xx not_active IP Right Cessation
- 1977-12-09 GB GB51348/77A patent/GB1554379A/en not_active Expired
- 1977-12-12 US US05/859,879 patent/US4200620A/en not_active Expired - Lifetime
- 1977-12-13 TR TR19331A patent/TR19331A/xx unknown
- 1977-12-14 PH PH20552A patent/PH14335A/en unknown
- 1977-12-14 IT IT52200/77A patent/IT1090568B/it active
- 1977-12-15 FI FI773803A patent/FI65610C/fi not_active IP Right Cessation
- 1977-12-15 IL IL53618A patent/IL53618A0/xx not_active IP Right Cessation
- 1977-12-15 MX MX171732A patent/MX146999A/es unknown
- 1977-12-15 DD DD77202670A patent/DD136258A5/xx unknown
- 1977-12-15 AT AT898277A patent/AT354978B/de active
- 1977-12-15 SE SE7714259A patent/SE429752B/sv not_active IP Right Cessation
- 1977-12-15 ZA ZA00777470A patent/ZA777470B/xx unknown
- 1977-12-16 JP JP15231677A patent/JPS5383993A/ja active Granted
- 1977-12-16 FR FR7738057A patent/FR2374263A1/fr active Granted
- 1977-12-16 DK DK562677A patent/DK149229C/da not_active IP Right Cessation
- 1977-12-16 BR BR7708375A patent/BR7708375A/pt unknown
- 1977-12-16 CA CA293,219A patent/CA1084238A/en not_active Expired
- 1977-12-16 BE BE183509A patent/BE861920A/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| BE861920A (fr) | 1978-06-16 |
| FI65610C (fi) | 1984-06-11 |
| FI65610B (fi) | 1984-02-29 |
| JPS5383993A (en) | 1978-07-24 |
| ATA898277A (de) | 1979-07-15 |
| DK562677A (da) | 1978-06-18 |
| GB1554379A (en) | 1979-10-17 |
| FR2374263A1 (fr) | 1978-07-13 |
| FI773803A7 (fi) | 1978-06-18 |
| BR7708375A (pt) | 1978-08-08 |
| MX146999A (es) | 1982-09-22 |
| DK149229C (da) | 1986-08-18 |
| FR2374263B1 (es) | 1982-10-08 |
| DD136258A5 (de) | 1979-06-27 |
| NL184945B (nl) | 1989-07-17 |
| NL7713608A (nl) | 1978-06-20 |
| AT354978B (de) | 1980-02-11 |
| NL184945C (nl) | 1989-12-18 |
| ZA777470B (en) | 1978-11-29 |
| CH631418A5 (de) | 1982-08-13 |
| SE7714259L (sv) | 1978-06-18 |
| JPS5734203B2 (es) | 1982-07-21 |
| US4200620A (en) | 1980-04-29 |
| SU888812A3 (ru) | 1981-12-07 |
| CA1084238A (en) | 1980-08-26 |
| IL53618A0 (en) | 1978-03-10 |
| SE429752B (sv) | 1983-09-26 |
| TR19331A (tr) | 1978-12-07 |
| PH14335A (en) | 1981-05-29 |
| DK149229B (da) | 1986-03-24 |
| DE2657190C2 (de) | 1982-11-04 |
| DE2657190A1 (de) | 1978-06-22 |
| IT1090568B (it) | 1985-06-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19930621 |