ES475099A1 - Process for the production of sodium percarbonate - Google Patents
Process for the production of sodium percarbonateInfo
- Publication number
- ES475099A1 ES475099A1 ES475099A ES475099A ES475099A1 ES 475099 A1 ES475099 A1 ES 475099A1 ES 475099 A ES475099 A ES 475099A ES 475099 A ES475099 A ES 475099A ES 475099 A1 ES475099 A1 ES 475099A1
- Authority
- ES
- Spain
- Prior art keywords
- sodium
- solution
- sodium percarbonate
- input solution
- hydrogen peroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VTIIJXUACCWYHX-UHFFFAOYSA-L disodium;carboxylatooxy carbonate Chemical compound [Na+].[Na+].[O-]C(=O)OOC([O-])=O VTIIJXUACCWYHX-UHFFFAOYSA-L 0.000 title abstract 5
- 229940045872 sodium percarbonate Drugs 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 7
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- 238000001556 precipitation Methods 0.000 abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 2
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 abstract 2
- 235000019982 sodium hexametaphosphate Nutrition 0.000 abstract 2
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 abstract 2
- 239000003808 active oxygen stabilizer Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000012452 mother liquor Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/10—Peroxyhydrates; Peroxyacids or salts thereof containing carbon
- C01B15/103—Peroxyhydrates; Peroxyacids or salts thereof containing carbon containing only alkali metals as metals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention relates to a process for the production of compact, coarse sodium percarbonate which comprises reacting hydrogen peroxide at 10 to 20 DEG C, with an input solution containing sodium carbonate and saturated with sodium percarbonate in the presence of 100 to 200 g of sodium chloride per litre of solution, at least one active oxygen stabiliser and from 0.1 to 1.9 g of sodium hexametaphosphate per litre of solution, the ratio of soda to sodium hexametaphosphate in the input solution being from 65:1 to 500:1, hydrogen peroxide being added to the soda input solution or suspension in a quantity which is substantially equivalent to the sodium carbonate dissolved and/or suspended in the input solution at a temperature maintained at substantially one and the same level throughout the entire precipitation process, subsequently reducing the over-saturation of dissolved sodium percarbonate formed by precipitation of the sodium percarbonate during and for up to 60 minutes after addition of the hydrogen peroxide, and separating off and drying the salt obtained. Optionally the mother liquor accumulating is returned to the working stage for the soda input solution.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2800760A DE2800760C2 (en) | 1978-01-09 | 1978-01-09 | Process for the production of sodium percarbonate from a soda solution or suspension |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES475099A1 true ES475099A1 (en) | 1979-04-16 |
Family
ID=6029185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES475099A Expired ES475099A1 (en) | 1978-01-09 | 1978-11-15 | Process for the production of sodium percarbonate |
Country Status (17)
| Country | Link |
|---|---|
| JP (1) | JPS54101798A (en) |
| AT (1) | AT386590B (en) |
| BE (1) | BE873347A (en) |
| CA (1) | CA1106136A (en) |
| CH (1) | CH638464A5 (en) |
| DD (1) | DD141013A5 (en) |
| DE (1) | DE2800760C2 (en) |
| ES (1) | ES475099A1 (en) |
| FR (1) | FR2414022A1 (en) |
| GB (1) | GB2011874B (en) |
| IL (1) | IL56390A (en) |
| IT (1) | IT1160954B (en) |
| PL (1) | PL114221B1 (en) |
| PT (1) | PT68751A (en) |
| SE (1) | SE439152B (en) |
| SU (1) | SU957757A3 (en) |
| ZA (1) | ZA786759B (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5833164B2 (en) * | 1980-07-04 | 1983-07-18 | 花王株式会社 | Hollow granular percarbonate and its manufacturing method |
| JPS58182855U (en) * | 1982-05-31 | 1983-12-06 | マツダ株式会社 | car roof molding |
| JPS58186557U (en) * | 1982-06-04 | 1983-12-12 | 古河電池株式会社 | Storage battery case |
| JPS596285U (en) * | 1982-07-05 | 1984-01-14 | ホーチキ株式会社 | Fire alarm equipment receiver |
| ES2085089T5 (en) † | 1992-10-16 | 2000-01-01 | Solvay Interox Gmbh | SODIC PERCARBONATES STABILIZED BY COATING. |
| DE4306399C2 (en) * | 1993-03-02 | 1995-06-14 | Degussa | Process for the preparation of stabilized sodium percarbonate |
| DE4311944A1 (en) * | 1993-04-10 | 1994-10-13 | Degussa | Coated sodium percarbonate particles, process for their preparation and detergent, cleaning and bleaching compositions containing them |
| US5560896A (en) * | 1993-08-31 | 1996-10-01 | Degussa Aktiengesellschaft | Method for producing granulated sodium percarbonate |
| IT1276685B1 (en) * | 1995-06-08 | 1997-11-03 | Ausimont Spa | PROCESS FOR THE PRODUCTION OF SODIUM PERCARBONATE IN GRANULAR FORM |
| DE19717729A1 (en) * | 1997-04-26 | 1998-10-29 | Degussa | Coated sodium percarbonate particles, process for their preparation and their use |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2328803C3 (en) * | 1973-06-06 | 1982-11-25 | Peroxid-Chemie GmbH, 8023 Höllriegelskreuth | Process for the production of an abrasion-resistant, coarse-grained sodium percarbonate |
| DE2644147C3 (en) * | 1976-09-30 | 1983-05-19 | Degussa Ag, 6000 Frankfurt | Process for the production of a compact, coarse-grained sodium percarbonate |
| DE2644148C3 (en) * | 1976-09-30 | 1983-05-11 | Degussa Ag, 6000 Frankfurt | Continuous process for the production of a compact, coarse-grained sodium percarbonate |
| AT356627B (en) * | 1976-10-22 | 1980-05-12 | Treibacher Chemische Werke Ag | METHOD FOR PRODUCING SODIUM PERCARBONATE |
-
1978
- 1978-01-09 DE DE2800760A patent/DE2800760C2/en not_active Expired
- 1978-10-31 CA CA315,322A patent/CA1106136A/en not_active Expired
- 1978-11-01 SU SU782680502A patent/SU957757A3/en active
- 1978-11-06 PT PT68751A patent/PT68751A/en unknown
- 1978-11-15 ES ES475099A patent/ES475099A1/en not_active Expired
- 1978-11-16 DD DD78209130A patent/DD141013A5/en not_active IP Right Cessation
- 1978-11-24 IT IT69696/78A patent/IT1160954B/en active
- 1978-12-01 ZA ZA00786759A patent/ZA786759B/en unknown
- 1978-12-28 JP JP16133078A patent/JPS54101798A/en active Granted
- 1978-12-28 FR FR7836779A patent/FR2414022A1/en active Granted
-
1979
- 1979-01-08 SE SE7900158A patent/SE439152B/en not_active IP Right Cessation
- 1979-01-08 IL IL56390A patent/IL56390A/en not_active IP Right Cessation
- 1979-01-08 PL PL1979212677A patent/PL114221B1/en unknown
- 1979-01-08 GB GB79653A patent/GB2011874B/en not_active Expired
- 1979-01-08 BE BE6/46728A patent/BE873347A/en not_active IP Right Cessation
- 1979-01-09 AT AT0016279A patent/AT386590B/en not_active IP Right Cessation
- 1979-01-09 CH CH17679A patent/CH638464A5/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6327292B2 (en) | 1988-06-02 |
| SU957757A3 (en) | 1982-09-07 |
| CH638464A5 (en) | 1983-09-30 |
| SE439152B (en) | 1985-06-03 |
| BE873347A (en) | 1979-07-09 |
| JPS54101798A (en) | 1979-08-10 |
| ATA16279A (en) | 1988-02-15 |
| IL56390A0 (en) | 1979-03-12 |
| ZA786759B (en) | 1979-11-28 |
| GB2011874B (en) | 1982-05-26 |
| IT1160954B (en) | 1987-03-11 |
| DE2800760C2 (en) | 1983-01-27 |
| SE7900158L (en) | 1979-07-10 |
| FR2414022A1 (en) | 1979-08-03 |
| PT68751A (en) | 1978-12-01 |
| FR2414022B1 (en) | 1982-11-19 |
| GB2011874A (en) | 1979-07-18 |
| IT7869696A0 (en) | 1978-11-24 |
| PL114221B1 (en) | 1981-01-31 |
| AT386590B (en) | 1988-09-12 |
| CA1106136A (en) | 1981-08-04 |
| DE2800760A1 (en) | 1979-07-19 |
| IL56390A (en) | 1981-09-13 |
| DD141013A5 (en) | 1980-04-09 |
| PL212677A1 (en) | 1979-11-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 20000201 |